Benzenemethanamine, a-2-propenyl-N-propyl-

Base Information

• Chemical Name: Benzenemethanamine, a-2-propenyl-N-propyl-
• CAS No.: 226723-82-6
• Molecular Formula: C13H19N
• Molecular Weight: 189.301
• Mol file: 226723-82-6.mol

Synonyms:

Chemical Property of Benzenemethanamine, a-2-propenyl-N-propyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanamine, a-2-propenyl-N-propyl-

There total 3 articles about Benzenemethanamine, a-2-propenyl-N-propyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

propylamine (107-10-8,42939-71-9) + allyltributylstanane (24850-33-7) + benzaldehyde (100-52-7) → (1-Phenyl-but-3-enyl)-propyl-amine (226723-82-6)

Guidance literature:

propylamine; benzaldehyde; With 4 A molecular sieve; In dichloromethane; at 20 ℃; for 15h;

allyltributylstanane; With magnesium oxide; tantalum pentachloride; In dichloromethane; at -40 ℃; for 3h;

DOI:10.1021/jo0356659

Reference yield: 50.0%

N-benzylidenepropylamine (6852-55-7) + allyl-trimethyl-silane (762-72-1) → (1-Phenyl-but-3-enyl)-propyl-amine (226723-82-6)

Guidance literature:

With bis(η3-allyl-μ-chloropalladium(II)); tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane; for 139h; Ambient temperature;

DOI:10.1021/jo9901081

Reference yield:

N-benzylidene-propylamine (27845-48-3) + allyl bromide (106-95-6) → (1-Phenyl-but-3-enyl)-propyl-amine (226723-82-6)

Guidance literature:

With samarium; Yield given. Multistep reaction; 1) THF, room temperature, 1 h, 2) room temperature, 1-2 h;

DOI:10.1080/00397919608004559

upstream raw materials:

N-benzylidene-propylamine

allyl bromide

N-benzylidenepropylamine

allyl-trimethyl-silane