1,1-Dimethylnaphthalen-2(1H)-one

Base Information

Chemical Name:1,1-Dimethylnaphthalen-2(1H)-one
CAS No.:23230-52-6
Molecular Formula:C12H12O
Molecular Weight:172.227
Hs Code.:
DSSTox Substance ID:DTXSID30511775
Wikidata:Q82370739
Mol file:23230-52-6.mol

Synonyms:23230-52-6;1,1-Dimethylnaphthalen-2(1H)-one;SCHEMBL4235643;DTXSID30511775;1,1-dimethyl-1h-naphthalen-2-one

Suppliers and Price of 1,1-Dimethylnaphthalen-2(1H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,1-Dimethylnaphthalen-2(1H)-one

Chemical Property:

PSA：17.07000
LogP:2.56010
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:172.088815002
Heavy Atom Count:13
Complexity:250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(=O)C=CC2=CC=CC=C21)C

Technology Process of 1,1-Dimethylnaphthalen-2(1H)-one

There total 1 articles about 1,1-Dimethylnaphthalen-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135-19-3
β-naphthol

: 74-88-4
methyl iodide

: 93-04-9
2-Methoxynaphthalene

: 1076-26-2
1-methyl-2-naphthol

: 1130-80-9
2-methoxy-1-methylnaphthalene

: 23230-52-6
1,1-dimethyl-1,2-dihydronaphthalen-2-one

Guidance literature:: With aluminum oxide; sodium methylate; at 50 ℃; for 48h; Yield given. Yields of byproduct given;
DOI:10.1039/c39800000325

Reference yield:

: 23230-52-6
1,1-dimethyl-1,2-dihydronaphthalen-2-one

: 573-98-8
dimethyl-1,2 naphtalene

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaBH₄/CeCl₃

2: 64 percent / Zn-Cu / diethyl ether

With sodium tetrahydroborate; cerium(III) chloride; copper; zinc; In diethyl ether;
DOI:10.1021/ja00315a038

Reference yield:

: 23230-52-6
1,1-dimethyl-1,2-dihydronaphthalen-2-one

: 88105-36-6
1,1-dimethyl-2-phenyl-3,4-methano-1,2,3,4-tetrahydronaphthalen-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / NaBH₄/CeCl₃

2: 29 percent / Zn-Cu / diethyl ether

3: 50 percent / pyridinium chlorochromate / CH₂Cl₂

4: 34 percent

With sodium tetrahydroborate; cerium(III) chloride; copper; pyridinium chlorochromate; zinc; In diethyl ether; dichloromethane;
DOI:10.1021/ja00315a038