N,N-diethylethanamine dihydrofluoride

Base Information

• Chemical Name: N,N-diethylethanamine dihydrofluoride
• CAS No.: 23588-89-8
• Molecular Formula: C6H15N.2FH
• Mol file: 23588-89-8.mol

Synonyms:

Chemical Property of N,N-diethylethanamine dihydrofluoride

Chemical Property:

• Vapor Pressure: 56.1mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-diethylethanamine dihydrofluoride

There total 40 articles about N,N-diethylethanamine dihydrofluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

triethylamine tris(hydrogen fluoride) (73602-61-6,23588-89-8,29585-72-6,94527-74-9) + triethylamine (121-44-8) → triethylammonium dihydrofluoride (23588-89-8,29585-72-6,94527-74-9)

Guidance literature:

DOI:10.1016/S0022-1139(02)00204-X

Reference yield: 88.0%

2,2,3,3-tetrafluoropropanol (76-37-9) + perfluoropropanoyl fluoride (422-61-7) → triethylamine tris(hydrogen fluoride) (73602-61-6,23588-89-8,29585-72-6,94527-74-9) + 1H,1H,3H-perfluoropropyl perfluoropropionate

Guidance literature:

With triethylamine; at 5 - 20 ℃; for 5h;

Reference yield: 81.0%

2,2,3,3,4,4,4-heptafluorobutanol (375-01-9) + Trifluoromethanesulfonyl fluoride (335-05-7) + triethylamine (121-44-8) → 2,2,3,3,4,4,4-heptafluorobutyl trifluoromethanesulfonate (6401-01-0) + triethylamine hydrofluoride (23588-89-8,29585-72-6,94527-74-9)

Guidance literature:

In dichloromethane;

DOI:10.1021/jo01023a511

upstream raw materials:

perfluoro(2-propoxypropionyl) fluoride

2,2,3,3-tetrafluoropropanol

perfluoropropanoyl fluoride

2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptanoyl fluoride

Downstream raw materials:

triethylammonium dihydrofluoride

tert-butyl 4-hydroxy-2-oxopyrrolidine-1-carboxylate

trans-[Pt(H)(F)(PCy₃)2]

[(PdMe)2(μ-κ2(P,P)Cy2PCH2PCy2)2(μ-F)][FHF]