4-[(Methylamino)carbonyl]benzoic acid

Base Information

• Chemical Name: 4-[(Methylamino)carbonyl]benzoic acid
• CAS No.: 23754-45-2
• Molecular Formula: C9H9NO3
• Molecular Weight: 179.175
• Hs Code.: 2921490090
• Mol file: 23754-45-2.mol

Synonyms:4-[(METHYLAMINO)CARBONYL]BENZOIC ACID;p-carboxybenzoylmethylamide;4-(methylcarbamoyl)benzoic acid;N-methyl-terephthalamic acid;

Chemical Property of 4-[(Methylamino)carbonyl]benzoic acid

Chemical Property:

• PSA: 66.40000
• LogP: 1.13530
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

4-[(Methylamino)carbonyl]benzoicAcid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 43
• Safety Statements: 36/37

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[(Methylamino)carbonyl]benzoic acid

There total 8 articles about 4-[(Methylamino)carbonyl]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methyl 4-(methylaminocarbonyl)benzoate (23754-46-3) → 4-(Methylaminocarbonyl)benzoic acid (23754-45-2)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1080/14756366.2021.1941920

Reference yield: 78.0%

N-methyl-p-methylbenzamide (18370-11-1) → 4-(Methylaminocarbonyl)benzoic acid (23754-45-2)

Guidance literature:

With potassium permanganate; In water; at 40 ℃; for 4h;

DOI:10.1016/j.bmcl.2014.12.085

Reference yield:

oxalyl dichloride (79-37-8) + Monomethyl terephthalate (1679-64-7) → methyl 4-(methylaminocarbonyl)benzoate (23754-46-3) + 4-(Methylaminocarbonyl)benzoic acid (23754-45-2)

Guidance literature:

With pyridine; In methanol; dichloromethane; benzene;

upstream raw materials:

methyl 4-(methylaminocarbonyl)benzoate

oxalyl dichloride

Monomethyl terephthalate

p-Toluic acid

Downstream raw materials:

C₂₇H₃₂N₆O₄

N-methyl-4-[(7-quinolin-3-yl-2,3-dihydro-1,4-benzoxazepin-4(5H)-yl)carbonyl]benzamide

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