2-Methoxy-4-[[(4-methoxyphenyl)imino]methyl]phenol

Base Information

• Chemical Name: 2-Methoxy-4-[[(4-methoxyphenyl)imino]methyl]phenol
• CAS No.: 24033-07-6
• Molecular Formula: C15H15NO3
• Molecular Weight: 257.289
• European Community (EC) Number: 653-641-9
• DSSTox Substance ID: DTXSID00419815
• Nikkaji Number: J1.469.106E
• Wikidata: Q82231017
• ChEMBL ID: CHEMBL4229093
• Mol file: 24033-07-6.mol

Synonyms:CBMicro_013156;24033-07-6;2-methoxy-4-{[(4-methoxyphenyl)imino]methyl}phenol;SCHEMBL8319294;CHEMBL4229093;DTXSID00419815;KDIGZGCAYQKYEH-UHFFFAOYSA-N;SMSF0004395;STK092399;AKOS000483477;CB04536;BIM-0013425.P001;N-(3-Methoxy-4-Hydroxybenzylidene)-p-Methoxyaniline;2-methoxy-4-{(E)-[(4-methoxyphenyl)imino]methyl}phenol;2-METHOXY-ALPHA-(4-METHOXYPHENYLIMINO)-PARA-CRESOL

Chemical Property of 2-Methoxy-4-[[(4-methoxyphenyl)imino]methyl]phenol

Chemical Property:

• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 257.10519334
• Heavy Atom Count: 19
• Complexity: 287

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)N=CC2=CC(=C(C=C2)O)OC

Technology Process of 2-Methoxy-4-[[(4-methoxyphenyl)imino]methyl]phenol

There total 5 articles about 2-Methoxy-4-[[(4-methoxyphenyl)imino]methyl]phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-methoxy-aniline (104-94-9) + vanillin (121-33-5,8014-42-4) → 4-methoxy-N-(4-hydroxy-3-methoxybenzylidene)aniline (24033-07-6,1123671-37-3)

Guidance literature:

for 2h; Ambient temperature;

Reference yield: 93.0%

→ 4-methoxy-N-(4-hydroxy-3-methoxybenzylidene)aniline (24033-07-6,1123671-37-3)

Guidance literature:

Reference yield:

2-methoxy-4-((E)-phenylethenyl)phenol (3391-75-1,18486-72-1) + p-methoxy-phenylazide (2101-87-3) → 4-methoxy-N-(4-hydroxy-3-methoxybenzylidene)aniline (24033-07-6,1123671-37-3) + 4-methoxy-N-[(E)-phenylmethylidene]aniline (1613-90-7)

Guidance literature:

With iron(II) chloride; In acetonitrile; at 100 ℃; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.orglett.9b03160

upstream raw materials:

4-methoxy-aniline

vanillin

2-methoxy-4-((E)-phenylethenyl)phenol

p-methoxy-phenylazide

Downstream raw materials:

2-methoxy-4-[4-(4-methoxy-phenyl)-3-phenyl-4,5-dihydro-[1,2,4]oxadiazol-5-yl]-phenol

3-methoxy-4-hydroxybenzoic acid

bis(4-methoxyphenyl)diazene

C₂₂H₂₂N₂O₄

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