1,2-Bis(p-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol

Base Information

• Chemical Name: 1,2-Bis(p-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol
• CAS No.: 2443-45-0
• Molecular Formula: C28H26O4
• Molecular Weight: 426.512
• DSSTox Substance ID: DTXSID40471270
• Nikkaji Number: J254.686H
• Mol file: 2443-45-0.mol

Synonyms:1,2-bis(p-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol;2443-45-0;SCHEMBL7763666;DTXSID40471270;BDZVJQHQHIFHSH-UHFFFAOYSA-N

Chemical Property of 1,2-Bis(p-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol

Chemical Property:

• XLogP3: 4.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 7
• Exact Mass: 426.18310931
• Heavy Atom Count: 32
• Complexity: 504

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C(C2=CC=CC=C2)(C(C3=CC=CC=C3)(C4=CC=C(C=C4)OC)O)O

Technology Process of 1,2-Bis(p-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol

There total 5 articles about 1,2-Bis(p-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

4-Methoxybenzophenone (611-94-9) → 1,2-bis(4-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol (2443-45-0)

Guidance literature:

4-Methoxybenzophenone; With iron(III)-acetylacetonate; phenyltriisopropoxytitanium(IV); In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1246/cl.2011.492

Reference yield: 40.0%

4-Methoxybenzophenone (611-94-9) → 1-(4-methoxyphenyl)-1-phenylmethanol (720-44-5) + 1,2-bis(4-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol (2443-45-0)

Guidance literature:

With triethylamine; cadmium(II) sulphide; In methanol; for 6h; Irradiation;

DOI:10.1021/j100365a002

Reference yield:

4-Methoxybenzophenone (611-94-9) + ethanol (64-17-5) → 1-(4-methoxyphenyl)-1-phenylmethanol (720-44-5) + 1,2-bis(4-methoxyphenyl)-1,2-diphenyl-1,2-ethanediol (2443-45-0)

Guidance literature:

upstream raw materials:

4-Methoxybenzophenone

1,2-bis(4-methoxyphenyl)-1,2-ethanedione

ethanol

Downstream raw materials:

2,2-bis-(p-methoxyphenyl)-1,2-diphenylethanone

2,2-bis-(4-methoxy-phenyl)-1,2-diphenyl-ethanol

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