Methyl 4-chloro-2-methoxybenzoate

Base Information

• Chemical Name: Methyl 4-chloro-2-methoxybenzoate
• CAS No.: 78955-90-5
• Molecular Formula: C9H9ClO3
• Molecular Weight: 200.622
• Hs Code.: 2918990090
• Mol file: 78955-90-5.mol

Synonyms:NSC 300574;Methyl 4-chloro-2-methoxybenzoate;4-Chloro-2-methoxybenzoicacid methyl ester;

Chemical Property of Methyl 4-chloro-2-methoxybenzoate

Chemical Property:

• Vapor Pressure: 0.00648mmHg at 25°C
• Refractive Index: 1.519
• Boiling Point: 271.4 °C at 760 mmHg
• Flash Point: 113.6 °C
• PSA: 35.53000
• Density: 1.228 g/cm³
• LogP: 2.13520
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

Methyl4-chloro-2-methoxybenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of Methyl 4-chloro-2-methoxybenzoate

There total 6 articles about Methyl 4-chloro-2-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

→ methyl 4-chloro-2-methoxybenzoate (78955-90-5) + (4-chloro-2-methoxy-phenyl)methanol (90296-27-8)

Guidance literature:

Reference yield: 96.0%

methanol (67-56-1) + 2-methoxy-4-chlorobenzoic acid (57479-70-6) → methyl 4-chloro-2-methoxybenzoate (78955-90-5)

Guidance literature:

With sulfuric acid; Heating / reflux;

Reference yield: 95.0%

4-chlorosalicylic acid (5106-98-9) + methyl iodide (74-88-4) → methyl 4-chloro-2-methoxybenzoate (78955-90-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 75 ℃; for 18h;

DOI:10.1016/j.bmcl.2007.09.103

upstream raw materials:

4-chlorosalicylic acid

dimethyl sulfate

methyl iodide

methanol

Downstream raw materials:

2-methoxy-4-chlorobenzoic acid

8-Allyl-2-(4-chloro-2-methoxy-phenyl)-chromen-4-one

(4-chloro-2-methoxy-phenyl)methanol

1-(4-chloro-2-methoxy-phenyl)-2-diazo-ethanone

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