3-(3-Methoxyphenyl)-1-propene

Base Information

• Chemical Name: 3-(3-Methoxyphenyl)-1-propene
• CAS No.: 24743-14-4
• Molecular Formula: C10H12O
• Molecular Weight: 148.205
• Hs Code.: 2909309090
• European Community (EC) Number: 675-444-7
• DSSTox Substance ID: DTXSID30374887
• Nikkaji Number: J141.462C
• Wikidata: Q82163463
• Mol file: 24743-14-4.mol

Synonyms:3-(3-Methoxyphenyl)-1-propene;24743-14-4;3-Allylanisole;1-methoxy-3-prop-2-enylbenzene;1-allyl-3-methoxybenzene;MFCD06201195;Benzene, 1-methoxy-3-(2-propenyl)-;3-allyl anisole;m-methoxy-allylbenzene;SCHEMBL2091147;DTXSID30374887;GLXYYHFXAQWLEP-UHFFFAOYSA-N;AC1287;AKOS006346305;1-methoxy-3-(prop-2-en-1-yl)benzene;DS-10170;SY039006;CS-0158005;FT-0735693;EN300-698354;A919294

Chemical Property of 3-(3-Methoxyphenyl)-1-propene

Chemical Property:

• Vapor Pressure: 0.284mmHg at 25°C
• Melting Point: 124-126 °C
• Boiling Point: 57oC/0.1mm
• Flash Point: 75.9oC
• PSA: 9.23000
• Density: 0.938g/cm3
• LogP: 2.42370
• Storage Temp.: 2-8°C
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 148.088815002
• Heavy Atom Count: 11
• Complexity: 120

Purity/Quality:

97% ^*data from raw suppliers

3-(3-Methoxyphenyl)-1-propene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC(=C1)CC=C

Technology Process of 3-(3-Methoxyphenyl)-1-propene

There total 22 articles about 3-(3-Methoxyphenyl)-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(3-methoxyphenyl)magnesium bromide (36282-40-3) + allyl bromide (106-95-6) → 1-allyl-3-methoxybenzene (24743-14-4)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 24h;

DOI:10.1021/jo035795h

Reference yield: 95.0%

3-methoxyphenyl bromide (2398-37-0) + allyl bromide (106-95-6) → 1-allyl-3-methoxybenzene (24743-14-4)

Guidance literature:

3-methoxyphenyl bromide; With iodine; magnesium; In diethyl ether; Inert atmosphere; Reflux;

allyl bromide; In diethyl ether; at 0 - 20 ℃; for 2.08333h; Inert atmosphere;

DOI:10.1021/jo4014996

Reference yield: 91.0%

2-Methoxy-4-allylphenyl-diethylphosphat (26057-16-9) → 1-allyl-3-methoxybenzene (24743-14-4)

Guidance literature:

With ammonia; sodium; In ethanol;

upstream raw materials:

(3-methoxyphenyl)magnesium bromide

allyl bromide

3-allylphenol

dimethyl sulfate

Downstream raw materials:

3-allylphenol

1,2-epoxy-3-(m-methoxyphenyl)propane

(E)-1-methoxy-3-(prop-1-en-1-yl)benzene

3-(3-methoxyphenyl)propan-1-ol