2-Propynoic acid, 3-(1-cyclohexen-1-yl)-, methyl ester

Base Information

Chemical Name:2-Propynoic acid, 3-(1-cyclohexen-1-yl)-, methyl ester
CAS No.:27944-90-7
Molecular Formula:C10H12O2
Molecular Weight:164.204
Hs Code.:
DSSTox Substance ID:DTXSID40394430
Nikkaji Number:J570.578I
Wikidata:Q82193812
Mol file:27944-90-7.mol

Synonyms:methyl 3-(cyclohexen-1-yl)prop-2-ynoate;27944-90-7;2-Propynoic acid, 3-(1-cyclohexen-1-yl)-, methyl ester;DTXSID40394430;AKOS024287084;3-(1-Cyclohexenyl)propiolic acid methyl ester

Suppliers and Price of 2-Propynoic acid, 3-(1-cyclohexen-1-yl)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propynoic acid, 3-(1-cyclohexen-1-yl)-, methyl ester

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:164.083729621
Heavy Atom Count:12
Complexity:262

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C#CC1=CCCCC1

Technology Process of 2-Propynoic acid, 3-(1-cyclohexen-1-yl)-, methyl ester

There total 7 articles about 2-Propynoic acid, 3-(1-cyclohexen-1-yl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 28075-50-5
cyclohex-1-en-1-yl trifluoromethane sulfonate

: 922-67-8
propynoic acid methyl ester

: 27944-90-7
methyl 3-(1-cyclohexen-1-yl)-2-propynoate

Guidance literature:: propynoic acid methyl ester; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃;

With zinc dibromide; In tetrahydrofuran; hexane; at -78 - 0 ℃;

cyclohex-1-en-1-yl trifluoromethane sulfonate; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; at 23 ℃;
DOI:10.1021/ol030010f

Reference yield: 57.0%

: 931-49-7
1-ethenylcyclohexene

: 79-22-1
methyl chloroformate

: 27944-90-7
methyl 3-(1-cyclohexen-1-yl)-2-propynoate

Guidance literature:: 1-ethenylcyclohexene; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃;

methyl chloroformate; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/j.tet.2014.09.038