Boranediamine, 1-chloro-N,N,N',N'-tetrakis(1-methylethyl)-

Base Information

Chemical Name:Boranediamine, 1-chloro-N,N,N',N'-tetrakis(1-methylethyl)-
CAS No.:28049-80-1
Molecular Formula:C12H28BClN2
Molecular Weight:246.632
Hs Code.:
Mol file:28049-80-1.mol

Synonyms:

Suppliers and Price of Boranediamine, 1-chloro-N,N,N',N'-tetrakis(1-methylethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Boranediamine, 1-chloro-N,N,N',N'-tetrakis(1-methylethyl)-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Boranediamine, 1-chloro-N,N,N',N'-tetrakis(1-methylethyl)-

There total 1 articles about Boranediamine, 1-chloro-N,N,N',N'-tetrakis(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 10294-34-5
boron trichloride

: 108-18-9
diisopropylamine

: 28049-80-1
bis(diisopropylamino)chloroborane

: 819-79-4
diisopropylamine hydrochloride

Guidance literature:: In light petroleum; -78°C; sepn. of (C3H7)2NH*HCl ppt.;
DOI:10.1039/jr9620001786

Reference yield: 98.0%

: 28049-80-1
bis(diisopropylamino)chloroborane

: 98-86-2
acetophenone

: 959925-19-0
C₆H₅C(CH₂)OB(N(CH(CH₃)2)2)2

Guidance literature:: With potassium hexamethyldisilazane; In tetrahydrofuran; byproducts: KCl; under Ar atm. to soln. KHDMS in THF ketone in THF was added dropwise at 0°C for 30 min, soln. chlorobis(dialkylamino)borane in THF was added and stirred at room temp. for 2 h; soln. was cenrifugated, ppt. was filtered, volatiles were removed in vacuo;
DOI:10.1021/om700676w