1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-4-[[(trifluoroMethyl)sulfonyl]oxy]-, phenylMethyl ester

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-4-[[(trifluoroMethyl)sulfonyl]oxy]-, phenylMethyl ester
CAS No.:286961-24-8
Molecular Formula:C14H14F3NO5S
Molecular Weight:365.33
Hs Code.:
Mol file:286961-24-8.mol

Synonyms:4-trifluoromethanesulfonyloxy-3,6-dihydro-2H-pyridine-1-carboxylic acid benzyl ester;

Suppliers and Price of 1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-4-[[(trifluoroMethyl)sulfonyl]oxy]-, phenylMethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of 1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-4-[[(trifluoroMethyl)sulfonyl]oxy]-, phenylMethyl ester

Chemical Property:

Boiling Point:443.5±45.0 °C(Predicted)
PKA:-3.60±0.40(Predicted)
PSA：81.29000
Density:1.48±0.1 g/cm3(Predicted)
LogP:3.79770

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-4-[[(trifluoroMethyl)sulfonyl]oxy]-, phenylMethyl ester

There total 6 articles about 1(2H)-Pyridinecarboxylic acid, 3,6-dihydro-4-[[(trifluoroMethyl)sulfonyl]oxy]-, phenylMethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 19099-93-5
benzyl 4-oxo-1-piperidinecarboxylate

: 286961-24-8
benzyl 1,2,3,6-tetrahydro-4-(trifluoromethylsulphonyloxy)-pyridine-1-carboxylate

Guidance literature:: benzyl 4-oxo-1-piperidinecarboxylate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.666667h;

N,N-phenylbistrifluoromethane-sulfonimide; In tetrahydrofuran; at -78 - 24 ℃; for 4.16667h;
DOI:10.1021/acs.joc.6b01709