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Cas Database |
| Name |
Propanoic acid,2-(phenylmethoxy)-, (2R)- |
EINECS | N/A | ||||||||
| CAS No. | 100836-85-9 | Density | 1.15g/cm3 | ||||||||
| PSA | 46.53000 | LogP | 1.67630 | ||||||||
| Solubility | Insoluble in water. | Melting Point |
52-55 °C |
||||||||
| Formula | C10H12 O3 | Boiling Point | 328.2°Cat760mmHg | ||||||||
| Molecular Weight | 180.203 | Flash Point | 130.4°C | ||||||||
| Transport Information | N/A | Appearance | N/A | ||||||||
| Safety |
|
Risk Codes | 36/37/38-43 | ||||||||
| Molecular Structure |
|
Hazard Symbols |
|
||||||||
| Synonyms |
Propanoicacid, 2-(phenylmethoxy)-, (R)-; (R)-(+)-O-Benzyllactic acid;R-2-Benzyloxypropionic acid |
Article Data | 40 |
Propanoic acid,2-(phenylmethoxy)-, (2R)- Synthetic route
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| With lithium hydroxide; water In tetrahydrofuran | 98% |
- 115458-99-6
(R)-2-(benzyloxy) methyl propionate
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| With potassium hydroxide In methanol; water at 20℃; for 0.5h; | 94% |
| With sodium hydroxide In methanol | 89% |
| With methanol; lithium hydroxide at 20℃; for 5h; | 78% |
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| With 2,6-di-tert-butyl-pyridine; 2.6-dimethylphenol; C32H12BF24(1-)*C44H30N2O2P(1+) In toluene at -40℃; for 24h; Inert atmosphere; enantioselective reaction; | 86% |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: benzyl alcohol With sodium at 80 - 90℃; for 2h; Stage #2: (S)-2-chloropropanoic acid at 55℃; for 3h; Stage #3: With hydrogenchloride In tert-butyl methyl ether; water pH=1.5 - 6.5; | 84% |
- 1220352-28-2
(2S,4R)-3-[(R)-2-benzyloxypropanoyl]-2-trifluoromethyl-4-phenyl-1,3-oxazolidine
A
- 100836-85-9
(R)-2-benzyloxypropionic acid
B
- 203176-56-1
(2S,4R)-2-trifluoromethyl-4-phenyl-1,3-oxazolidine
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: (2S,4R)-3-[(R)-2-benzyloxypropanoyl]-2-trifluoromethyl-4-phenyl-1,3-oxazolidine With lithium aluminium tetrahydride In diethyl ether at -10℃; for 2h; Inert atmosphere; Stage #2: With water; sodium hydroxide In diethyl ether Inert atmosphere; Further stages; | A 82% B 57% |
C
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| With water; dihydrogen peroxide; lithium hydroxide In tetrahydrofuran at 0℃; for 1.5h; | A 7% B n/a C n/a |
- 33106-32-0, 74431-49-5, 100836-85-9, 6625-78-1
2-(benzyloxy)propanoic acid
A
- 33106-26-2, 33106-64-8, 70448-03-2, 87037-69-2
2-benzyloxypropanol
B
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| Yield given. Yields of byproduct given; |
- 105544-95-4
[(4R,5S)-5-((R)-1-Benzyloxy-ethyl)-2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy]-tert-butyl-diphenyl-silane
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| Multistep reaction; | |
| Multi-step reaction with 4 steps 1: tetrabutylammonium fluoride / tetrahydrofuran / 2 h / 0 °C 2: acetic acid / H2O / 10 h / 80 °C 3: NaIO4 / acetone; H2O / 3 h / 24 °C 4: CrO3 / acetic acid; pyridine / 3 h / 23 °C View Scheme |
- 87604-62-4
(2S,3R)-3-Benzyloxy-butane-1,2-diol
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| With ruthenium trichloride; sodium periodate In tetrachloromethane; water; acetonitrile for 2h; Ambient temperature; Yield given; |
- 82939-03-5
N-<(R)-α-benzyloxypropionyl>-cyclo-(β-alanylprolyl)
- 100836-85-9
(R)-2-benzyloxypropionic acid
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In methanol for 5h; Ambient temperature; |
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(R)-(+)-2-BENZYLOXYPROPIONIC ACID
