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| CAS No.: | 682-09-7 |
|---|---|
| Name: | Trimethylolpropane diallyl ether |
| Molecular Structure: | |
|
|
|
| Formula: | C12H22 O3 |
| Molecular Weight: | 214.305 |
| Synonyms: | 1-Butanol,2,2-bis[(2-propenyloxy)methyl]- (9CI); 1-Butanol, 2,2-bis[(allyloxy)methyl]-(6CI,7CI,8CI); 2,2-Bis(allyloxymethyl)-1-butanol; Diallyl trimethylolpropaneether; Neoallyl T 20; T 20; TMPDE 80; Trimethylolpropane diallyl ether;Trimethylpropane diallyl ether |
| EINECS: | 211-661-1 |
| Density: | 0.955 |
| Boiling Point: | 135 ºC (13 mmHg) |
| Flash Point: | >110 ºC |
| Solubility: | Practically insoluble in water |
| Hazard Symbols: |
|
| Risk Codes: | R36/37/38 |
| Safety: | Mildly toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating fumes. See also ETHERS and ALLYL COMPOUNDS. |
| PSA: | 38.69000 |
| LogP: | 1.78030 |
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- 77-99-6
1,1,1-tri(hydroxymethyl)propane
- 107-05-1
3-chloroprop-1-ene
- 682-09-7
trimethylol propane diallyl ether
| Conditions | Yield |
|---|---|
| With sodium hydroxide In water at 90℃; Inert atmosphere; |
- 682-09-7
trimethylol propane diallyl ether
- 144900-28-7
2,4,4-trimethyl-1-pentyl hypophosphorous acid
- 1189189-14-7
[3-(2-hydroxymethyl-2-{3-[hydroxy-(2,4,4-trimethylpentyl)phosphinoyl]propoxymethyl}butoxy)propyl]-(2,4,4-trimethylpentyl)phosphinic acid
| Conditions | Yield |
|---|---|
| With di-tert-amyl peroxide at 140℃; for 6h; Inert atmosphere; | 100% |
| Conditions | Yield |
|---|---|
| With potassium methanolate at 120℃; for 20.9h; Inert atmosphere; | 98.2% |
| Conditions | Yield |
|---|---|
| With potassium methanolate at 120℃; for 21.7667h; Inert atmosphere; | 97.9% |
- 682-09-7
trimethylol propane diallyl ether
| Conditions | Yield |
|---|---|
| With phosphorus trichloride In acetonitrile at -15 - 20℃; for 4h; Inert atmosphere; | 88% |
- 682-09-7
trimethylol propane diallyl ether
| Conditions | Yield |
|---|---|
| With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; for 12h; | 56% |
| Conditions | Yield |
|---|---|
| Stage #1: trimethylol propane diallyl ether With sodium In toluene at 110℃; for 4h; Stage #2: 1-bromo-octane In toluene for 6 - 10h; Heating / reflux; | 55% |
- 682-09-7
trimethylol propane diallyl ether
- 459-64-3
4-methoxybenzenediazonium tetrafluoroborate
- 1147550-11-5
ammonium thiocyanate
| Conditions | Yield |
|---|---|
| copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 35% |
- 682-09-7
trimethylol propane diallyl ether
- 1147550-11-5
ammonium thiocyanate
- 459-44-9
4-methylbenzenediazonium tetrafluoroborate
| Conditions | Yield |
|---|---|
| copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 35% |
- 682-09-7
trimethylol propane diallyl ether
- 1147550-11-5
ammonium thiocyanate
- 369-57-3
benzenediazonium tetrafluoroborate
| Conditions | Yield |
|---|---|
| copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃; | 31% |
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Chemistry
IUPAC Name: 2,2-Bis(prop-2-enoxymethyl)butan-1-ol (682-09-7)
Synonyms:1,1,1-Trimethylolpropane diallyl ether ; 1,1,1-(Trihydroxymethyl)propane diallyl ether ; 2-Ethyl-2-(hydroxymethyl)-1 3-propanediol diallyl ether ; 2,2-Bis(allyloxymethyl)-1-butanol ;Ttrimethylolpropane diallyl ether
CAS: 682-09-7
MF: C12H22O3
MW: 214.3
MS: 
EINECS: 211-661-1
Mol File: 682-09-7.mol
Surface Tension: 31.6 dyne/cm
Density: 0.943 g/cm3
Flash Point: 133.7 °C
Enthalpy of Vaporization: 62.34 kJ/mol
Boiling Point: 297.5 °C at 760 mmHg
Vapour Pressure: 0.000136 mmHg at 25°C
Refractive index: n20/D 1.458(lit.)
Uses
Trimethylolpropane diallyl ether (682-09-7) is used as an organic intermediate.
Toxicity Data With Reference
| 1. | orl-rat LD50:6500 mg/kg | IHFCAY Industrial Hygiene Foundation of America, Chemical and Toxicological Series, Bulletin. 6 (1967),1. |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Hazard Codes: Xi
Risk Statements: 36/37/38
36/37/38: Trimethylolpropane diallyl ether (682-09-7) is irritating to eyes, respiratory system and skin.
Safety Statements: 26-36
26: Trimethylolpropane diallyl ether (682-09-7) used, in case of contact with eyes,please rinse immediately with plenty of water and seek medical advice.
36: Wear suitable protective clothing .
WGK Germany : 2
RTECS: TY6667000