CAS No.682-09-7,Trimethylolpropane diallyl ether Suppliers

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Basic Information

Molecular Structure:
CAS No.:	682-09-7
Name:	Trimethylolpropane diallyl ether
Article Data:	4

Formula:	C12H22 O3
Molecular Weight:	214.305
Synonyms:	1-Butanol,2,2-bis[(2-propenyloxy)methyl]- (9CI); 1-Butanol, 2,2-bis[(allyloxy)methyl]-(6CI,7CI,8CI); 2,2-Bis(allyloxymethyl)-1-butanol; Diallyl trimethylolpropaneether; Neoallyl T 20; T 20; TMPDE 80; Trimethylolpropane diallyl ether;Trimethylpropane diallyl ether
EINECS:	211-661-1
Density:	0.955
Boiling Point:	135 ºC (13 mmHg)
Flash Point:	>110 ºC
Solubility:	Practically insoluble in water
Hazard Symbols:
Risk Codes:	R36/37/38
Safety:	Mildly toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating fumes. See also ETHERS and ALLYL COMPOUNDS.
PSA:	38.69000
LogP:	1.78030

Synthetic route

: 77-99-6
1,1,1-tri(hydroxymethyl)propane

: 107-05-1
3-chloroprop-1-ene

: 682-09-7
trimethylol propane diallyl ether

Conditions

Conditions	Yield
With sodium hydroxide In water at 90℃; Inert atmosphere;

: 682-09-7
trimethylol propane diallyl ether

: 144900-28-7
2,4,4-trimethyl-1-pentyl hypophosphorous acid

: 1189189-14-7
[3-(2-hydroxymethyl-2-{3-[hydroxy-(2,4,4-trimethylpentyl)phosphinoyl]propoxymethyl}butoxy)propyl]-(2,4,4-trimethylpentyl)phosphinic acid

Conditions

Conditions	Yield
With di-tert-amyl peroxide at 140℃; for 6h; Inert atmosphere;	100%

: 3234-28-4
1,2-epoxytetradecane

: 682-09-7
trimethylol propane diallyl ether

: C37H74O5

Conditions

Conditions	Yield
With potassium methanolate at 120℃; for 20.9h; Inert atmosphere;	98.2%

: 682-09-7
trimethylol propane diallyl ether

: C33H34O2

: C45H56O5

Conditions

Conditions	Yield
With potassium methanolate at 120℃; for 21.7667h; Inert atmosphere;	97.9%

: 682-09-7
trimethylol propane diallyl ether

: (2,2-bis((allyloxy)methyl)butan-1-yl)dichlorophosphite

Conditions

Conditions	Yield
With phosphorus trichloride In acetonitrile at -15 - 20℃; for 4h; Inert atmosphere;	88%

: 682-09-7
trimethylol propane diallyl ether

: 3,5-bis(2-bromo-2-methylpropanoyloxy) benzoic acid

: C27H36Br2O8

Conditions

Conditions	Yield
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; for 12h;	56%

: 111-83-1
1-bromo-octane

: 682-09-7
trimethylol propane diallyl ether

: 3,3-diallyloxymethyl-5-oxa-tridecane

Conditions

Conditions	Yield
Stage #1: trimethylol propane diallyl ether With sodium In toluene at 110℃; for 4h; Stage #2: 1-bromo-octane In toluene for 6 - 10h; Heating / reflux;	55%

: 682-09-7
trimethylol propane diallyl ether

: 459-64-3
4-methoxybenzenediazonium tetrafluoroborate

: 1147550-11-5
ammonium thiocyanate

: 2-allyloxymethyl-2-[3-(4-methoxy-phenyl)-2-thiocyanato-propoxymethyl]-butan-1-ol

Conditions

Conditions	Yield
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃;	35%

...Expand

: 682-09-7
trimethylol propane diallyl ether

: 1147550-11-5
ammonium thiocyanate

: 459-44-9
4-methylbenzenediazonium tetrafluoroborate

: 2-allyloxymethyl-2-(2-thiocyanato-3-p-tolyl-propoxymethyl)-butan-1-ol

Conditions

Conditions	Yield
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃;	35%

...Expand

: 682-09-7
trimethylol propane diallyl ether

: 1147550-11-5
ammonium thiocyanate

: 369-57-3
benzenediazonium tetrafluoroborate

: 2-[(allyloxy)methyl]-2-[(3-phenyl-2-thiocyanatopropoxy)methyl]butan-1-ol

Conditions

Conditions	Yield
copper(II) bis(tetrafluoroborate) In water; acetone at 10 - 15℃;	31%

...Expand

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Chemistry

IUPAC Name: 2,2-Bis(prop-2-enoxymethyl)butan-1-ol (682-09-7)
Synonyms:1,1,1-Trimethylolpropane diallyl ether ; 1,1,1-(Trihydroxymethyl)propane diallyl ether ; 2-Ethyl-2-(hydroxymethyl)-1 3-propanediol diallyl ether ; 2,2-Bis(allyloxymethyl)-1-butanol ;Ttrimethylolpropane diallyl ether ; 1-Butanol,2,2-bis[(2-propenyloxy)methyl]- ; 2,2-Bis[(2-propenyloxy)methyl]-1-butano ; 2,2-Bis[(2-propenyloxy)methyl]-1-Butanol
CAS: 682-09-7
MF: C₁₂H₂₂O₃
MW: 214.3
MS:
EINECS: 211-661-1
Mol File: 682-09-7.mol
Surface Tension: 31.6 dyne/cm
Density: 0.943 g/cm³
Flash Point: 133.7 °C
Enthalpy of Vaporization: 62.34 kJ/mol
Boiling Point: 297.5 °C at 760 mmHg
Vapour Pressure: 0.000136 mmHg at 25°C
Refractive index: n20/D 1.458(lit.)

Uses

Trimethylolpropane diallyl ether (682-09-7) is used as an organic intermediate.

Toxicity Data With Reference

orl-rat LD50:6500 mg/kg

IHFCAY Industrial Hygiene Foundation of America, Chemical and Toxicological Series, Bulletin. 6 (1967),1.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Hazard Codes: Xi
Risk Statements: 36/37/38
36/37/38: Trimethylolpropane diallyl ether (682-09-7) is irritating to eyes, respiratory system and skin.
Safety Statements: 26-36
26: Trimethylolpropane diallyl ether (682-09-7) used, in case of contact with eyes,please rinse immediately with plenty of water and seek medical advice.
36: Wear suitable protective clothing .
WGK Germany : 2
RTECS: TY6667000