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10128-71-9

Basic Information
CAS No.: 10128-71-9
Name: 3-HYDROXY-4-PYRIDINECARBOXYLIC ACID
Article Data: 18
Molecular Structure:
Molecular Structure of 10128-71-9 (3-HYDROXY-4-PYRIDINECARBOXYLIC ACID)
Formula: C6H5NO3
Molecular Weight: 139.111
Synonyms: 3-hydroxypyridine-4-carboxylate;3-Hydroxyisonicotinic acid;3-Hydroxypyridine-4-carboxylicacid;3-Hydroxy-4-pyridinecarboxylic acid;
Density: 1.485 g/cm3
Melting Point: 317-319 °C(dec.)
Boiling Point: 519.3 °C at 760 mmHg
Flash Point: 267.9 °C
Solubility: Soluble in methanol. Slightly soluble in water.
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37/39
PSA: 70.42000
LogP: 0.48540
Synthetic route
7579-20-6

3-Aminopyridine-4-carboxylic acid

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
Stage #1: 3-Aminopyridine-4-carboxylic acid With sulfuric acid; sodium nitrite In water at 10 - 80℃;
Stage #2: With water; acetic acid at 65℃;
Stage #3: With ammonia In water pH=~ 4.5;
91%
With sulfuric acid; sodium nitrite In water at 80℃; for 0.25h;88%
Stage #1: 3-Aminopyridine-4-carboxylic acid With sulfuric acid; sodium nitrite In water at 8 - 85℃; for 0.833333h;
Stage #2: With ammonium hydroxide; acetic acid In water at 0℃;
78%
92404-81-4

furo<2,3-c>pyridinium 3-hydroxypyridine-4-nitrolate

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
With hydrogenchloride for 16h; Heating;80%
92404-80-3

3-hydroxy-4-(1'-chloro-1'-hydroximinomethyl)pyridinium nitrate

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
With hydrogenchloride for 16h; Heating;80%
15031-12-6

5-ethoxyoxazole

79-10-7

acrylic acid

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
In ethanol for 48h;30%
at 4 - 20℃;
88912-27-0

3-chloro-isonicotinic acid

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
With potassium hydroxide
3-amino-pyridine-carboxylic acid-(4)

3-amino-pyridine-carboxylic acid-(4)

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite Diazotization;
sodium-salt of pyridin-3-ol

sodium-salt of pyridin-3-ol

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
With carbon dioxide; potassium acetate at 190 - 240℃; under 44130.5 Torr;
55-22-1

pyridine-4-carboxylic acid

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
With sulfuric acid; quinolinium dichromate(VI); acetic acid at 50℃; for 24h; Kinetics;
With sulfuric acid; quinolinium dichromate(VI); acetic acid In water at 49.85℃; for 48h; Kinetics; Further Variations:; Solvents; Temperatures;
Multi-step reaction with 2 steps
1: thionyl chloride / 180 - 220 °C / im Rohr und Zersetzen des Reaktionsprodukts mit Wasser
2: KOH-solution
View Scheme
With quinolinium dichromate In water; acetic acid at 49.84℃; for 48h; Kinetics; Mechanism; Solvent; Temperature; Inert atmosphere;
19539-50-5

furo<2,3-c>pyridine

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 41 percent / sulfuric acid, fuming nitric acid (d,1.50); / 1.5 h
2: 80 percent / 10percent HCl / 16 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 24 percent / 1.) sulfuric acid, fuming nitric acid (d,1.50); 2.) amberlite IRA-47 / 1.5 h
2: 80 percent / 10percent HCl / 16 h / Heating
View Scheme
109-00-2

3-HYDROXYPYRIDINE

124-38-9

carbon dioxide

10128-71-9

3-hydroxyisonicotinic acid

Conditions
ConditionsYield
Stage #1: 3-HYDROXYPYRIDINE With n-butyllithium
Stage #2: carbon dioxide
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Chemistry

Empirical Formula: C6H5NO3
Molecular Weight: 139.1088
Nominal Mass: 139 Da
Average Mass: 139.1088 Da
Monoisotopic Mass: 139.026943 Da 
Index of Refraction: 1.626
Molar Refractivity: 33.15 cm3
Molar Volume: 93.6 cm3
Surface Tension: 78.3 dyne/cm
Density: 1.485 g/cm3
Flash Point: 267.9 °C
Melting point: 317-319(dec.)
Enthalpy of Vaporization: 83.39 kJ/mol
Boiling Point: 519.3 °C at 760 mmHg
Vapour Pressure: 1.3E-11 mmHg at 25 °C
Structure of 3-Hydroxypyridine-4-carboxylic acid (CAS NO.10128-71-9):
                        
IUPAC Name: 3-Hydroxypyridine-4-carboxylic acid
Canonical SMILES: C1=CN=CC(=C1C(=O)O)O
InChI: InChI=1S/C6H5NO3/c8-5-3-7-2-1-4(5)6(9)10/h1-3,8H,(H,9,10)
InChIKey: JEHGATQUCUYHJL-UHFFFAOYSA-N
Product Category of 3-Hydroxypyridine-4-carboxylic acid (CAS NO.10128-71-9): Pharmacetical;Pyridines

Safety Profile

Hazard Codes of 3-Hydroxypyridine-4-carboxylic acid (CAS NO.10128-71-9): IrritantXi
Risk Statements: 36/37/38 
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.
Hazard Note: Irritant
HazardClass: IRRITANT

Specification

 3-Hydroxypyridine-4-carboxylic acid , its cas register number is 10128-71-9. It also can be called 3-Hydroxyisonicotinic acid ; and 3-Hydroxy-4-pyridinecarboxylic acid .