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102-87-4

Basic Information
CAS No.: 102-87-4
Name: 1-Dodecanamine,N,N-didodecyl-
Molecular Structure:
Molecular Structure of 102-87-4 (1-Dodecanamine,N,N-didodecyl-)
Formula: C36H75N
Molecular Weight: 521.99
Synonyms: Tridodecylamine(6CI,8CI);Adogen 360;Alamine 304;Alamine 304-1;Armeen 312;N,N-Didodecyl-1-dodecanamine;NSC 35134;Tri-n-dodecylamine;Trilaurylamine;Tris(dodecyl)amine;
EINECS: 203-063-4
Density: 0.828 g/cm3
Melting Point: 16 °C
Boiling Point: 544.6 °C at 760 mmHg
Flash Point: 256.6 °C
Solubility: Not miscible or difficult to mix with water.
Appearance: clear slightly yellow liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36
Transport Information:
PSA: 3.24000
LogP: 13.05110
Synthetic route
124-22-1

n-Dodecylamine

A

3007-31-6

N,N-didodecylamine

B

102-87-4

tridodecylamine

Conditions
ConditionsYield
With Co2Rh2/C In toluene at 180℃; under 760.051 Torr; for 6h; Temperature; Time; Solvent; Autoclave; Inert atmosphere;A 86%
B 5%
With ruthenium trichloride; triphenylphosphine In tetrahydrofuran at 235℃; for 8h;A 26 % Chromat.
B 52%
With ruthenium trichloride; triphenylphosphine In tetrahydrofuran at 235℃; for 8h; Title compound not separated from byproducts;A 67 % Chromat.
B 30 % Chromat.
With tris(triphenylphosphine)ruthenium(II) chloride In methanol at 180℃; for 7h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
2437-25-4

undecyl cyanide

A

3007-31-6

N,N-didodecylamine

B

102-87-4

tridodecylamine

Conditions
ConditionsYield
With hydrogen; silica gel; copper at 160℃; under 33002.6 Torr; for 2.69444h; Product distribution; Rate constant; other temperatures, other catalysts;A 84%
B n/a
With methanol; hydrogen at 249.9℃; under 37503 Torr; for 25h;A 15%
B 60 % Chromat.
With methanol; hydrogen; aluminum oxide; copper-chromium powder at 249.9℃; under 37503 Torr; for 25h;A 48 % Chromat.
B 5 % Chromat.
124-22-1

n-Dodecylamine

143-15-7

1-dodecylbromide

102-87-4

tridodecylamine

Conditions
ConditionsYield
With sodium carbonate In ethanol for 144h; Heating;22.6%
4292-19-7

1-Iodododecane

3007-31-6

N,N-didodecylamine

102-87-4

tridodecylamine

Conditions
ConditionsYield
at 160 - 170℃;
4292-19-7

1-Iodododecane

A

3007-31-6

N,N-didodecylamine

B

102-87-4

tridodecylamine

Conditions
ConditionsYield
With ammonia; water
3007-31-6

N,N-didodecylamine

112-52-7

1-chlorododecane

102-87-4

tridodecylamine

Conditions
ConditionsYield
at 160 - 170℃;
67-56-1

methanol

111-82-0

methyl n-dodecanoate

A

124-22-1

n-Dodecylamine

B

112-18-5

N,N-dimethylaminododecane

C

7311-30-0

N-methyldodecylamine

D

3007-31-6

N,N-didodecylamine

E

2915-90-4

N-methyldidodecylamine

F

102-87-4

tridodecylamine

Conditions
ConditionsYield
With ammonia; hydrogen; copper-chromium powder; titanium(IV) oxide at 250℃; under 37503 Torr; Product distribution; other catalyst; var. temp., pressure, and reagents ratio;A 31.9 % Chromat.
B 20.0 % Chromat.
C 30.7 % Chromat.
D 2.5 % Chromat.
E 2.0 % Chromat.
F 2.0 % Chromat.
111-82-0

methyl n-dodecanoate

A

124-22-1

n-Dodecylamine

B

3007-31-6

N,N-didodecylamine

C

102-87-4

tridodecylamine

Conditions
ConditionsYield
With methanol; ammonia; hydrogen; copper-chromium powder; titanium(IV) oxide at 250℃; under 37503 Torr;A 31.9 % Chromat.
B 2.5 % Chromat.
C 2.0 % Chromat.
112-53-8

1-dodecyl alcohol

A

102-87-4

tridodecylamine

B

didodecylamine; dodecylamine

didodecylamine; dodecylamine

Conditions
ConditionsYield
With aluminium silicate; ammonia at 350℃;

tridodecyl-amine; compound with 2,4,6-trichloro-phenol

A

102-87-4

tridodecylamine

B

88-06-2

2,4,6-Trichlorophenol

Conditions
ConditionsYield
In tetrachloromethane at 25℃; Equilibrium constant;

tridodecyl-amine; compound with 2,4,6-trichloro-phenol

A

102-87-4

tridodecylamine

B

88-06-2

2,4,6-Trichlorophenol

Conditions
ConditionsYield
In tetrachloromethane at 25℃; Equilibrium constant;
102-87-4

tridodecylamine

20587-64-8

tridodecylamine oxide

Conditions
ConditionsYield
With dihydrogen peroxide In methanol; water85%
102-87-4

tridodecylamine

2437-25-4

undecyl cyanide

Conditions
ConditionsYield
With ammonium hydroxide; 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione at 60℃; for 6h;84%
With ammonium hydroxide; 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione at 60℃; for 6h;84%
937802-88-5

C22H17Cl2N2O5S(1-)*K(1+)

102-87-4

tridodecylamine

937802-92-1

C22H18Cl2N2O5S*C36H75N

Conditions
ConditionsYield
With hydrogenchloride In methanol; water at 70℃; for 0.25h;83%
102-87-4

tridodecylamine

N,N-didodecylformamide

Conditions
ConditionsYield
With manganese(IV) oxide; oxygen In chlorobenzene at 100℃; under 4500.45 Torr; for 4h; Autoclave; Green chemistry;80%
102-87-4

tridodecylamine

4-bromomethyl-4'-methacrylamidocarbonylazobenzene

C54H91N4O2(1+)*Br(1-)

Conditions
ConditionsYield
In ethanol for 10h; Reflux;73.5%
102-87-4

tridodecylamine

C46H28N6O8

europium(III) nitrate

C46H24N6O8(4-)*Eu(3+)*C36H75N*H(1+)

Conditions
ConditionsYield
In methanol at 20℃; for 4h; Inert atmosphere;67.3%
1120-71-4

1,3-propanesultone

102-87-4

tridodecylamine

103982-08-7

tridodecylammonium 3-propanesulfonate

Conditions
ConditionsYield
In toluene at 110℃; for 3h;62%
102-87-4

tridodecylamine

1670-14-0

benzamidine monohydrochloride

100-52-7

benzaldehyde

5-decyl-2,4-diphenylpyrimidine

Conditions
ConditionsYield
With di-tert-butyl peroxide; iodine In chlorobenzene at 150℃; for 8h;62%
With di-tert-butyl peroxide; iodine In chlorobenzene at 150℃; for 8h; Sealed tube;62%

C24H19N2O5S(1-)*K(1+)

102-87-4

tridodecylamine

C24H20N2O5S*C36H75N

Conditions
ConditionsYield
With hydrogenchloride; water61%
74-83-9

methyl bromide

102-87-4

tridodecylamine

29920-02-3

tridodecylmethylammonium chloride

Conditions
ConditionsYield
In ethanol at 90 - 95℃; for 183h;52%
98-01-1

furfural

102-87-4

tridodecylamine

696-62-8

para-iodoanisole

C32H57NO2

Conditions
ConditionsYield
With Wilkinson’s catalyst; 1,3-bis-(diphenylphosphino)propane; water In tetrahydrofuran at 140℃; for 12h; Inert atmosphere; Sealed tube;52%
102-87-4

tridodecylamine

70-11-1

α-bromoacetophenone

3-decyl-N,N-didodecyl-5-phenylfuran-2-amine

Conditions
ConditionsYield
With [2,2]bipyridinyl; iron(III) chloride; di-tert-butyl peroxide In toluene at 135℃; for 14h; Sealed tube;40%

zinc perchlorate

102-87-4

tridodecylamine

1439241-70-9

C44H28N6O4

europium(III) nitrate

2C44H26N6O4(2-)*Eu(3+)*Zn(2+)*2ClO4(1-)*C36H75N*H(1+)

Conditions
ConditionsYield
Stage #1: tridodecylamine; C44H28N6O4; europium(III) nitrate In methanol at 20℃; for 4h;
Stage #2: zinc perchlorate In methanol at 20℃; for 1h; Concentration;
36.9%

iron(II) tetrafluoroborate

102-87-4

tridodecylamine

1439241-70-9

C44H28N6O4

europium(III) nitrate

2C44H26N6O4(2-)*C36H76N(1+)*Eu(3+)*Fe(2+)*2BF4(1-)

Conditions
ConditionsYield
Stage #1: tridodecylamine; C44H28N6O4; europium(III) nitrate In methanol at 20℃; for 1h;
Stage #2: iron(II) tetrafluoroborate In methanol at 20℃; for 1h;
35.8%

hydroxygallium naphthalocyaninetetrasulfonic acid

102-87-4

tridodecylamine

4C36H75N*C48H25GaN8O13S4

Conditions
ConditionsYield
In methanol; water32%
102-87-4

tridodecylamine

S,S'-diethyl-S,S'-dimethyl-S,S'-cis-ethene-1,2-diyl-bis-sulfonium; bis-tetrafluoroborate

C41H85NS(2+)*2BF4(1-)

102-87-4

tridodecylamine

74-88-4

methyl iodide

29710-98-3

tri-n-dodecylmethylammonium iodide

Conditions
ConditionsYield
for 24h; Heating;
102-87-4

tridodecylamine

2486-89-7

tri-n-dodecylammonium chloride

Conditions
ConditionsYield
With hydrogenchloride In water
102-87-4

tridodecylamine

2305-34-2

tridodecylamine; nitrate

Conditions
ConditionsYield
With nitric acid In water
102-87-4

tridodecylamine

88-06-2

2,4,6-Trichlorophenol

tridodecyl-amine; compound with 2,4,6-trichloro-phenol

Conditions
ConditionsYield
In tetrachloromethane at 25℃; Equilibrium constant;
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Specification

The 1-Dodecanamine,N,N-didodecyl-, with the CAS registry number 102-87-4, is also known as Tri-n-dodecylamine. Its EINECS registry number is 203-063-4. This chemical's molecular formula is C36H75N and molecular weight is 521.9874. Its IUPAC name is called N,N-didodecyldodecan-1-amine. This chemical is clear slightly yellow liquid.

Physical properties of 1-Dodecanamine,N,N-didodecyl-: (1)ACD/LogP: 17.60; (2)# of Rule of 5 Violations: 2; (3)ACD/LogD (pH 5.5): 14.52; (4)ACD/LogD (pH 7.4): 15.24; (5)ACD/BCF (pH 5.5): 1000000; (6)ACD/BCF (pH 7.4): 1000000; (7)ACD/KOC (pH 5.5): 10000000; (8)ACD/KOC (pH 7.4): 10000000; (9)#H bond acceptors: 1; (10)#Freely Rotating Bonds: 33; (11)Index of Refraction: 1.459; (12)Molar Refractivity: 172.55 cm3; (13)Molar Volume: 630 cm3; (14)Surface Tension: 31.2 dyne/cm; (15)Density: 0.828 g/cm3; (16)Flash Point: 256.6 °C; (17)Enthalpy of Vaporization: 82.33 kJ/mol; (18)Boiling Point: 544.6 °C at 760 mmHg; (19)Vapour Pressure: 6.41E-12 mmHg at 25°C.

Uses of 1-Dodecanamine,N,N-didodecyl-: it can be used to produce tridodecylamine oxide. This reaction will need reagent H2O2 and solvent H2O, methanol. The yield is about 85%.

When you are using this chemical, please be cautious about it as the following:
This chemical may cause inflammation to the skin or other mucous membranes. It is irritating to eyes, respiratory system and skin. In case of contact with eyes, you should rinse immediately with plenty of water and seek medical advice. Whenever you will contact it, please wear suitable protective clothing.

You can still convert the following datas into molecular structure:
(1)Canonical SMILES: CCCCCCCCCCCCN(CCCCCCCCCCCC)CCCCCCCCCCCC
(2)InChI: InChI=1S/C36H75N/c1-4-7-10-13-16-19-22-25-28-31-34-37(35-32-29-26-23-20-17-14-11-8-5-2)36-33-30-27-24-21-18-15-12-9-6-3/h4-36H2,1-3H3
(3)InChIKey: SWZDQOUHBYYPJD-UHFFFAOYSA-N