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Basic Information
CAS No.: 10484-56-7
Name: 2-BUTOXYNAPHTHALENE
Article Data: 17
Molecular Structure:
Molecular Structure of 10484-56-7 (2-BUTOXYNAPHTHALENE)
Formula: C14H16 O
Molecular Weight: 200.28
Synonyms: 2-Butoxynaphthalene;Butyl b-naphthyl ether; Fragarol; b-Naphthol butyl ether
Density: 1.016g/cm3
Melting Point: 35-36℃
Boiling Point: 315.3°Cat760mmHg
Flash Point: 123.5°C
PSA: 9.23000
LogP: 4.01870
Synthetic route
109-65-9

1-bromo-butane

135-19-3

β-naphthol

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With potassium hydroxide; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate Ambient temperature;98%
With potassium carbonate In acetonitrile at 125℃; for 1h; Microwave irradiation;95%
93-04-9

2-Methoxynaphthalene

71-36-3

butan-1-ol

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With bismuth(lll) trifluoromethanesulfonate In water; 1,2-dichloro-ethane at 110℃; for 24h; Schlenk technique; Inert atmosphere;98%
463934-14-7

2-(but-3-en-1-yloxy)naphthalene

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With iron(III) chloride; lithium aluminium tetrahydride; hydrogen In tetrahydrofuran at 18℃; under 750.075 Torr; for 20h; Inert atmosphere; Sealed tube;65%
135-19-3

β-naphthol

71-36-3

butan-1-ol

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With Nafion NR50 at 115℃; for 35h; Inert atmosphere; Large scale reaction;97%
With sulfuric acid
135-19-3

β-naphthol

n-butyl halide

n-butyl halide

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 80℃;
109-69-3

n-Butyl chloride

135-19-3

β-naphthol

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With 2,6-dimethylpyridine; tetrabutyl-ammonium chloride; potassium carbonate In water for 8h; Heating;97%
1112-67-0

tetrabutyl-ammonium chloride

135-19-3

β-naphthol

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With potassium carbonate at 150 - 160℃; for 6h;27%
135-19-3

β-naphthol

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h / 20 °C / Inert atmosphere; Cooling with ice
2: hydrogen; iron(III) chloride; lithium aluminium tetrahydride / tetrahydrofuran / 20 h / 18 °C / 750.08 Torr / Inert atmosphere; Sealed tube
View Scheme
109-65-9

1-bromo-butane

875-83-2

sodium 2-naphtholate

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With ethanol
109-65-9

1-bromo-butane

135-19-3

β-naphthol

1.) Amberlite IRA-900(Cl(1-))

1.) Amberlite IRA-900(Cl(1-))

10484-56-7

2-butoxynaphthalene

Conditions
ConditionsYield
With sodium hydroxide 1.) EtOH; 2.) THF, 65 deg C; Multistep reaction;
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