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1103738-29-9

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Basic Information
CAS No.: 1103738-29-9
Name: 4-Iodo-1-chloro-2-(4-ethoxybenzyl)benzene
Article Data: 15
Molecular Structure:
Molecular Structure of 1103738-29-9 (4-Iodo-1-chloro-2-(4-ethoxybenzyl)benzene)
Formula: C15H14ClIO
Molecular Weight: 372.633
Synonyms: Benzene, 1-chloro-2-[(4-ethoxyphenyl)methyl]-4-iodo-; 1-Chloro-2-(4-Ethoxybenzyl)-4-Iodobenzene; 4-(5-Iodo-2-chlorobenzyl)phenyl ethyl ether; 4-Iodo-1-chloro-2-(4-ethoxybenzyl)benzene
Density: 1.531±0.06 g/cm3(Predicted)
Boiling Point: 411.2±40.0 °C(Predicted)
Appearance: off-white solid
PSA: 9.23000
LogP: 4.93410
Related products
Synthetic route
1103738-26-6

(2-chloro-5-iodo-phenyl)-(4-ethoxyphenyl)methanone

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
With triethylsilane; boron trifluoride diethyl etherate In acetonitrile at 5 - 20℃; for 17.5h;97.4%
With triethylsilane; boron trifluoride diethyl etherate In acetonitrile at 5 - 20℃; for 17.508h; Inert atmosphere;97.4%
Stage #1: (2-chloro-5-iodo-phenyl)-(4-ethoxyphenyl)methanone With sodium tetrahydroborate In tetrahydrofuran for 0.5h; Inert atmosphere;
Stage #2: With aluminum (III) chloride at 10℃; for 0.5h; Reflux;		91.2%
793695-85-9

2-bromomethyl-1-chloro-4-iodo-benzene

588-96-5

4-bromoethoxybenzene

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
Stage #1: 4-bromoethoxybenzene With iodine; magnesium; methoxybenzene at 47℃; for 3.2h;
Stage #2: 2-bromomethyl-1-chloro-4-iodo-benzene With copper(l) iodide at -18 - 20℃; for 16.2h; Temperature;		95.9%
281652-58-2

2-chloro-5-iodobenzoylchloride

103-73-1

Phenetole

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
Stage #1: 2-chloro-5-iodobenzoylchloride; Phenetole With aluminum (III) chloride In dichloromethane at -5 - 15℃;
Stage #2: at 25 - 30℃; for 26h;		67%
Stage #1: Phenetole With aluminum (III) chloride In dichloromethane at -3 - 5℃; for 0.5h;
Stage #2: 2-chloro-5-iodobenzoylchloride In dichloromethane at 0 - 25℃; for 12h;
Stage #3: In dichloromethane at 30℃; for 16h;		67%
Stage #1: 2-chloro-5-iodobenzoylchloride; Phenetole With aluminum (III) chloride In dichloromethane at 0 - 5℃; for 2h;
Stage #2: In dichloromethane at 25 - 30℃; for 26h;		67%
aq sodium bicarbonate

aq sodium bicarbonate

boron trifluoride-diethyletherate

boron trifluoride-diethyletherate

1103738-26-6

(2-chloro-5-iodo-phenyl)-(4-ethoxyphenyl)methanone

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
With triethylsilane In acetonitrile
...Expand
281652-58-2

2-chloro-5-iodobenzoylchloride

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane / 2.33 h / -7 - 9 °C / Inert atmosphere
2: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 17.5 h / 5 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride / dichloromethane / 0.12 h / -7 - 9 °C / Inert atmosphere
1.2: 2.22 h / 3 - 5 °C
2.1: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 17.5 h / 5 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: aluminum (III) chloride / dichloromethane / 2 h / 5 - 15 °C / Industrial scale
2: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 2.5 h / 20 - 30 °C / Industrial scale
View Scheme
Multi-step reaction with 2 steps
1: aluminum (III) chloride; water / dichloromethane / 2 h / 5 - 15 °C / Industrial scale
2: triethylsilane; boron trifluoride diethyl etherate / acetonitrile / 2.5 h / 20 - 30 °C / Industrial scale
View Scheme
19094-56-5

2-chloro-5-iodobenzoic acid

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 20.93 h
2: aluminum (III) chloride / dichloromethane / 2.33 h / -7 - 9 °C / Inert atmosphere
3: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 17.5 h / 5 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16 h / 10 - 25 °C
2.1: aluminum (III) chloride / dichloromethane / -5 - 15 °C
2.2: polymethylhydrosiloxane (PMHS) / 26 h / 25 - 30 °C
View Scheme
Multi-step reaction with 2 steps
1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 16.17 h / 10 - 25 °C
2.1: aluminum (III) chloride / dichloromethane / 0.5 h / -3 - 5 °C
2.2: 12 h / 0 - 25 °C
2.3: polymethylhydrosiloxane (PMHS) / 16 h / 30 °C
View Scheme
103-73-1

Phenetole

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: oxalyl chloride / dichloromethane; N,N-dimethyl-formamide / 4 h / 20 °C
1.2: 3 h / 0 - 20 °C
2.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 0 - 20 °C
View Scheme
462-06-6

fluorobenzene

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 39 - 42 °C
1.2: Reflux
2.1: sodium hydroxide / 50 - 65 °C
3.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / Inert atmosphere
3.2: 0.5 h / 10 °C / Reflux
View Scheme
915095-86-2

(2-chloro-5-iodophenyl)(4-fluorophenyl)methanone

1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydroxide / 50 - 65 °C
2.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h / Inert atmosphere
2.2: 0.5 h / 10 °C / Reflux
View Scheme
1103738-29-9

1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene

C30H33NO6

C41H39ClO6

Conditions
ConditionsYield
Stage #1: 1-chloro-2-(4-ethoxybenzyl)-4-iodobenzene With TurboGrignard In tetrahydrofuran at -5 - 0℃; for 1h;
Stage #2: C30H33NO6 In tetrahydrofuran; toluene at -5 - 0℃;		91%
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