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Basic Information
CAS No.: 116751-24-7
Name: 3-Hydroxy-2,4,5-trifluorobenzoic acid
Molecular Structure:
Molecular Structure of 116751-24-7 (3-Hydroxy-2,4,5-trifluorobenzoic acid)
Formula: C7H3F3O3
Molecular Weight: 192.094
Synonyms: 2,4,5-Trifluoro-3-hydroxybenzoic acid;2,4,5-Trifluoro-3-hydroxybenzoicacid;
Density: 1.699 g/cm3
Melting Point: 144-145 °C
Boiling Point: 292.6 °C at 760 mmHg
Flash Point: 130.8 °C
Appearance: white to light yellow-beige powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-37/39
PSA: 57.53000
LogP: 1.50770
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Synthetic route
652-03-9

3,4,5,6-tetrafluorophthalic acid

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
Stage #1: 3,4,5,6-tetrafluorophthalic acid With sodium hydroxide In water at 90℃; for 9h;
Stage #2: With hydrogenchloride; tri-n-propylamine In water at 140℃; under 7500.75 Torr; for 7h; pH=1; Temperature;		90.35%
28749-88-4

3,4,6-trifluoro-5-hydroxyphthalic acid

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
In water90%
In water90%
28889-41-0

4-methoxy-3,5,6-trifluorophthalic acid

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
In water74%
In water74%

2-bromo-3,4,6-trifluoro-5-hydroxy-benzoic acid

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
With sodium hydroxide; zinc In water at 25℃; for 2h;1.92 g

triisopropyl(2,3,6-trifluorophenoxy)silane

124-38-9

carbon dioxide

A

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

B

156839-10-0

2,3,5-trifluoro-4-hydroxybenzoic acid

Conditions
ConditionsYield
Stage #1: triisopropyl(2,3,6-trifluorophenoxy)silane With 2,2,6,6-tetramethylpiperidinyl-lithium In diethyl ether
Stage #2: carbon dioxide In diethyl ether
Stage #3: With hydrogenchloride Title compound not separated from byproducts;
...Expand
124-38-9

carbon dioxide

1,2,4-trifluoro-3-(methoxymethoxy)benzene

A

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

B

156839-10-0

2,3,5-trifluoro-4-hydroxybenzoic acid

Conditions
ConditionsYield
Stage #1: 1,2,4-trifluoro-3-(methoxymethoxy)benzene With n-butyllithium In tetrahydrofuran
Stage #2: carbon dioxide In tetrahydrofuran; hexane
Stage #3: With hydrogenchloride In water Title compound not separated from byproducts;
Stage #1: 1,2,4-trifluoro-3-(methoxymethoxy)benzene With lithium diisopropyl amide In tetrahydrofuran
Stage #2: carbon dioxide In tetrahydrofuran
Stage #3: With hydrogenchloride In water Title compound not separated from byproducts;
...Expand
851341-31-6

1-bromo-2,3,5-trifluoro-4-(methoxymethoxy)benzene

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 2,2,6,6-tetramethylpiperidine; potassium tert-butoxide; N,N,N',N'',N''-pentamethylenediamine / butyllithium / tetrahydrofuran; hexane / 0.75 h / -125 °C
1.2: tetrahydrofuran; hexane
2.1: HCl / H2O
3.1: 1.92 g / NaOH; zinc powder / H2O / 2 h / 25 °C
View Scheme

2-bromo-3,4,6-trifluoro-5-methoxymethoxy-benzoic acid

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: HCl / H2O
2: 1.92 g / NaOH; zinc powder / H2O / 2 h / 25 °C
View Scheme
113798-74-6

2,3,6-trifluorophenol

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 82 percent / imidazole / dimethylformamide / 20 h / 25 °C
2.1: lithium 2,2,6,6-tetramethylpiperidide / diethyl ether
2.2: diethyl ether
2.3: hydrochloric acid
View Scheme
Multi-step reaction with 5 steps
1.1: 87 percent / N-bromosuccinimide / CHCl3 / 2 h / 0 °C
2.1: 88 percent / N-ethyldiisopropylamine / CH2Cl2 / 2 h / 25 °C
3.1: 2,2,6,6-tetramethylpiperidine; potassium tert-butoxide; N,N,N',N'',N''-pentamethylenediamine / butyllithium / tetrahydrofuran; hexane / 0.75 h / -125 °C
3.2: tetrahydrofuran; hexane
4.1: HCl / H2O
5.1: 1.92 g / NaOH; zinc powder / H2O / 2 h / 25 °C
View Scheme
Multi-step reaction with 2 steps
1.1: 87 percent / N-ethyldiisopropylamine / CH2Cl2 / 25 °C
2.1: lithium diisopropylamide / tetrahydrofuran
2.2: tetrahydrofuran
2.3: HCl / H2O
View Scheme
192446-70-1

4-bromo-2,3,6-trifluorophenol

116751-24-7

2,4,5-trifluoro-3-hydroxybenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: 88 percent / N-ethyldiisopropylamine / CH2Cl2 / 2 h / 25 °C
2.1: 2,2,6,6-tetramethylpiperidine; potassium tert-butoxide; N,N,N',N'',N''-pentamethylenediamine / butyllithium / tetrahydrofuran; hexane / 0.75 h / -125 °C
2.2: tetrahydrofuran; hexane
3.1: HCl / H2O
4.1: 1.92 g / NaOH; zinc powder / H2O / 2 h / 25 °C
View Scheme
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