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13019-22-2

Basic Information
CAS No.: 13019-22-2
Name: 9-Decen-1-ol
Article Data: 46
Molecular Structure:
Molecular Structure of 13019-22-2 (9-Decen-1-ol)
Formula: C10H20 O
Molecular Weight: 156.268
Synonyms: 9-Decenol;Decylenic alcohol;NSC 103158;Rosalva;Trepanol;w-Decen-1-ol;
EINECS: 235-878-6
Density: 0.876 g/mL at 25 °C(lit.)
Melting Point: -13 °C
Boiling Point: 234-238 °C(lit.)
Flash Point: 210 °F
Solubility: Insoluble in water; soluble in alcohol.
Appearance: colorless liquid
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: A skin irritant. A flammable liquid. When heated to decomposition it emits acrid smoke and irritating fumes. See also ALCOHOL, DENATURED; ALCOHOLS, C6-12; ALCOHOLS, C9-11; ALCOHOLS, C12-13, ETHOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED; ALCOHOLS, C12-16, ETHOXYLATED; ALCOHOLS, C14-15, ETHOXYLATED; ALCOHOLS, C16-18, ETHOXYLATED; ALCOHOLS, C8-10, ETHOXYLATED PROPOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED PROPOXYLATED; ALCOHOLS, N.O.S..
PSA: 20.23000
LogP: 2.89540
Synthetic route
25601-41-6

methyl 9-decenoate

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
Stage #1: methyl 9-decenoate With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 5.5h; Cooling;
Stage #2: With sodium hydroxide In tetrahydrofuran; water at 20℃; Reagent/catalyst; Concentration; Solvent; Temperature; Time;
98.3%
With lithium aluminium tetrahydride In tetrahydrofuran at 15 - 20℃; for 5.5h; Inert atmosphere;98.3%
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene at 15 - 20℃; for 2h; Sealed tube; Cooling with ice; Inert atmosphere;97.14%
67136-13-4

1-(tetrahydro-2-pyranyloxy)-9-decene

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With copper dichloride In methanol at 20℃; Hydrolysis;95%
With CuCl2*2H2O In methanol at 20℃; for 1.25h;95%
91717-85-0

decane-1,2,10-triol

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With rhenium(VII) oxide; triphenylphosphine at 165℃; for 1h;90%
112-47-0

1,10-Decanediol

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With 1-hexadecylcarboxylic acid at 340℃; for 5h; Temperature; Reagent/catalyst; Molecular sieve;88%
With 1-hexadecylcarboxylic acid; stearic acid at 330 - 350℃; under 700 Torr; for 150h;80%
112-47-0

1,10-Decanediol

A

1647-16-1

1,10-decadiene

B

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With 1-hexadecylcarboxylic acid at 340℃; for 6h; Molecular sieve;A n/a
B 88%
39770-05-3

9-decenal

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With manganese; water; 2,4,6-collidine hydrochloride In tetrahydrofuran at 20℃; chemoselective reaction;84%
67233-91-4

trans-9-decenoic acid ethyl ester

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With styrene; [RuCl2(N,N'-(ethane-1,2-diyl)bis(1-(2-(diphenylphosphaneyl)phenyl)methanimine))]; potassium methanolate; hydrogen at 80℃; under 37503.8 Torr; for 5h; Time; Inert atmosphere; Autoclave; chemoselective reaction;84%
With styrene; [RuCl2(N,N'-(ethane-1,2-diyl)bis(1-(2-(diphenylphosphaneyl)phenyl)methanimine))]; potassium methanolate; hydrogen at 80℃; under 37503.8 Torr; for 5h; Inert atmosphere; Autoclave;84%
14436-32-9

dec-9-enoic acid

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 1h; Inert atmosphere;80%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃;64%
With nonan-1-al; samarium diiodide; samarium(III) trifluoromethanesulfonate In tetrahydrofuran; methanol; potassium hydroxide at 20℃; for 0.0833333h; Reduction;96 % Chromat.

1-((dec-9-en-1-yloxy)methyl)-4-methoxybenzene

13019-22-2

9-Decen-1-ol

Conditions
ConditionsYield
With ammonium peroxydisulfate; 9-(2-mesityl)-10-methylacridinium perchlorate In dichloromethane; water at 20 - 30℃; for 2h; Irradiation; Green chemistry;80%
Stage #1: 1-((dec-9-en-1-yloxy)methyl)-4-methoxybenzene With sodium hydrogencarbonate; bis-[(trifluoroacetoxy)iodo]benzene; meso-2,5-bis(methoxycarbonyl)-2,5-dimethylpyrrolidine-1-oxyl In dichloromethane at 20℃; for 2h;
Stage #2: With water In dichloromethane chemoselective reaction;
79%
100189-71-7

((dec-9-en-1-yloxy)methyl)benzene

A

13019-22-2

9-Decen-1-ol

B

1275582-65-4

9-bromo-decane-1-ol

Conditions
ConditionsYield
With triphenylphosphine hydrobromide In acetonitrile for 12h; Reflux;A 63%
B 8%
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 CAS 13019-22-2

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Chemistry

Molecular Formula: C10H20O
Molar mass: 156.2652 g/mol
EINECS: 235-878-6
Density: 0.839 g/cm3
Flash Point: 98.9 °C
Index of Refraction: 1.445
Boiling Point: 236 °C at 760 mmHg
Vapour Pressure: 0.00879 mmHg at 25°C
Melting point: -13 °C
Appearance: Colourless liquid
Product categories: Acyclic;Alkenes;omega-Functional Alkanols, Carboxylic Acids, Amines & Halides;Organic Building Blocks
Structure of 9-Decen-1-OL (13019-22-2):
      
XLogP3-AA: 3.6
H-Bond Donor: 1
H-Bond Acceptor: 1
Systematic Name: Dec-9-en-1-ol 
SMILES: OCCCCCCCC\C=C 
InChI: InChI=1/C10H20O/c1-2-3-4-5-6-7-8-9-10-11/h2,11H,1,3-10H2 
InChIKey: QGFSQVPRCWJZQK-UHFFFAOYAX 
Std. InChI: InChI=1S/C10H20O/c1-2-3-4-5-6-7-8-9-10-11/h2,11H,1,3-10H2 
Std. InChIKey: QGFSQVPRCWJZQK-UHFFFAOYSA-N

Toxicity Data With Reference

1.    

skn-rbt 100%

    FCTXAV    Food and Cosmetics Toxicology. 12 (1974),405.

Carcinogenicity of 9-Decen-1-OL (13019-22-2) hasn't been listed as a carcinogen by NTP, IARC,ACGIH, or CA Prop 65. You can see actual entry in RTECS for complete information.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

A skin irritant. A flammable liquid. When heated to decomposition it emits acrid smoke and irritating fumes. See also ALCOHOL, DENATURED; ALCOHOLS, C6-12; ALCOHOLS, C9-11; ALCOHOLS, C12-13, ETHOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED; ALCOHOLS, C12-16, ETHOXYLATED; ALCOHOLS, C14-15, ETHOXYLATED; ALCOHOLS, C16-18, ETHOXYLATED; ALCOHOLS, C8-10, ETHOXYLATED PROPOXYLATED; ALCOHOLS, C12-15, ETHOXYLATED PROPOXYLATED; ALCOHOLS, N.O.S..
Hazard Note: Irritant
Hazard Codes: Xi
Risk Statements:
36:  Irritating to the eyes
37:  Irritating to the respiratory system
38:  Irritating to the skin
Safety Statements:
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36:  Wear suitable protective clothing

Specification

 9-Decen-1-OL (13019-22-2) also can be called omega-Decenol ; .omega.-Decen-1-ol ; .omega.-Decenol ; Anapterin and Decylenic alcohol .It is hazardous,so the first aid measures and others should be known.Such as: When on the skin:  should  flush skin with plenty of water immediatelyfor at least 15 minutes while removing contaminated clothing.Or in the eyes: Flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids..While ,it's Inhaled: Remove from exposure and move to fresh air immediately.Then you have the ingesting of the product : Do not induce vomiting.If victim is conscious and alert, give 2-4 cupfuls of milk or water.
In addition, 9-Decen-1-OL (13019-22-2) can be stable under normal temperature and pressure conditions.It is not compatible with strong oxidizing agents, and you must not take it with incompatible materials.And also prevent it to broken down into hazardous decomposition products: irritating and toxic fumes and gases, carbon dioxide, carbon monoxide.