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Basic Information
| CAS No.: | 1647-16-1 |
|---|---|
| Name: | 1,9-Decadiene |
| Article Data: | 56 |
| Molecular Structure: | |
|
|
|
| Formula: | C10H18 |
| Molecular Weight: | 138.253 |
| Synonyms: | NSC 102789;a,w-Decadiene |
| EINECS: | 216-711-6 |
| Density: | 0.752 g/cm3 |
| Melting Point: | -69.6°C (estimate) |
| Boiling Point: | 169 °C at 760 mmHg |
| Flash Point: | 41.7 °C |
| Appearance: | clear colorless to slightly yellow liquid |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 10-36/37/38 |
| Safety: | 26-36 |
| Transport Information: | UN 3295 3 |
| PSA: | 0.00000 |
| LogP: | 3.69900 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| at 600℃; under 20 Torr; for 0.0333333h; | A 93% B 31% C 57% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| Mo(NC6H3(CH(CH3)2)2)(CHC(CH3)2C6H5)(NC4H2(CH3)2)(OC10H9BrC10H9BrOSi(CH3)2C(CH3)3) In 1,3,5-trimethyl-benzene under 7600.51 Torr; for 16h; Product distribution / selectivity; Inert atmosphere; Sealed system; | 90% |
| Re2O7/B2O3/Al2O3; tetramethylstannane In toluene under 3750.38 - 4500.45 Torr; for 92.5h; Product distribution / selectivity; | |
| Re2O7/B2O3/Al2O3; tetramethylstannane In toluene under 3750.38 - 4500.45 Torr; Product distribution / selectivity; | |
| With Mo[N(2,6-(i-Pr)2Ph)](CHCMe2Ph)(Me2Pyr)(OBitet) at 20℃; under 15201 Torr; for 20h; Inert atmosphere; | 93 %Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| With 1-hexadecylcarboxylic acid at 340℃; for 6h; Molecular sieve; | A n/a B 88% |
Conditions
| Conditions | Yield |
|---|---|
| With methoxy(cyclooctadiene)rhodium(I) dimer; N,N-Dimethylacrylamide; 3-Methoxybenzoic acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 90℃; for 24h; Inert atmosphere; Glovebox; Sealed tube; chemoselective reaction; | 88% |
Conditions
| Conditions | Yield |
|---|---|
| With nickel(II) iodide; triphenylphosphine In neat (no solvent) for 16h; Reagent/catalyst; Inert atmosphere; Sealed tube; | 85% |
| With bis-triphenylphosphine-palladium(II) chloride; 3,3',5,5'-tetra(tert-butyl)biphenyl-2,2'-diol; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In neat (no solvent) at 132℃; for 3h; Inert atmosphere; | 59% |
| Stage #1: 10-undecenoic acid With bis(1,5-cyclooctadiene)diiridium(I) dichloride; triphenylphosphine; potassium iodide at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: With acetic anhydride at 160℃; for 5h; Inert atmosphere; Schlenk technique; regioselective reaction; |
- 85721-25-1
2-(oct-7-en-1-yl)oxirane
- 1647-16-1
1,10-decadiene
Conditions
| Conditions | Yield |
|---|---|
| With bis(acetylacetonate)nickel(II); diethylzinc In hexane; toluene at 110℃; for 48h; Inert atmosphere; | 85% |
- 94160-13-1
C24H30O4
- 1647-16-1
1,10-decadiene
Conditions
| Conditions | Yield |
|---|---|
| at 330℃; for 8h; | 82% |
- 26118-61-6
1,10-decanediol diacetate
- 1647-16-1
1,10-decadiene
Conditions
| Conditions | Yield |
|---|---|
| at 350℃; for 8h; | 80% |
| at 565℃; | |
| at 600℃; |
- 82176-56-5
tetrabromo-1,1,10,10 decane
- 1647-16-1
1,10-decadiene
Conditions
| Conditions | Yield |
|---|---|
| With n-butyllithium In diethyl ether at -30 - -25℃; | 78% |
- 42236-22-6
n-Decandiyl-dipropionat
- 1647-16-1
1,10-decadiene
Conditions
| Conditions | Yield |
|---|---|
| at 340℃; for 8h; | 78% |
