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| CAS No.: | 13710-19-5 |
|---|---|
| Name: | N-(3-Chloro-ortho-tolyl) anthranilic acid |
| Article Data: | 16 |
| Molecular Structure: | |
|
|
|
| Formula: | C14H12ClNO2 |
| Molecular Weight: | 261.708 |
| Synonyms: | N-(3-Chloro-o-tolyl)anthranilicacid;N-(2-Methyl-3-chlorophenyl)anthranilic acid;GEA 6414;Migea;Tolfedine;Anthranilicacid, N-(3-chloro-o-tolyl)- (7CI,8CI);Clotam;Tolfine; |
| EINECS: | 237-264-3 |
| Density: | 1.333 g/cm3 |
| Melting Point: | 210-214 °C |
| Boiling Point: | 405.4 °C at 760 mmHg |
| Flash Point: | 199 °C |
| Solubility: | Soluble in water (slightly), acetone (~10 mg/ml), DMSO (52 mg/ml at 25°C), methanol (~10 mg/ml) and ethanol (50 mg/ml). |
| Hazard Symbols: |
 Xn
|
| Risk Codes: | 22 |
| Transport Information: | UN 2811 6.1/PG 3 |
| PSA: | 49.33000 |
| LogP: | 4.16320 |
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| Conditions | Yield |
|---|---|
| Stage #1: ortho-chlorobenzoic acid With sodium hydroxide for 1h; Reflux; Stage #2: 3-chloro-2-methylbenzenamine With aluminum oxide; sodium hydroxide for 3h; Reflux; | 88.6% |
| With copper(l) iodide; potassium carbonate; potassium iodide In water at 55 - 100℃; for 12h; Reagent/catalyst; Inert atmosphere; | 60% |
| Conditions | Yield |
|---|---|
| With copper(l) iodide; potassium carbonate; potassium iodide In water at 55 - 100℃; for 6h; Reagent/catalyst; Inert atmosphere; | 83.1% |
| Conditions | Yield |
|---|---|
| With copper(l) iodide; potassium carbonate; potassium iodide In water at 55 - 100℃; for 4h; Reagent/catalyst; Inert atmosphere; | 82% |
| With copper; potassium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; Schlenk technique; Inert atmosphere; |
| Conditions | Yield |
|---|---|
| With N-ethylmorpholine;; copper diacetate In N,N-dimethyl-formamide at 145℃; for 4h; Ullmann-Goldberg condensation; | 40% |
| With N-ethylmorpholine;; copper diacetate In N,N-dimethyl-formamide at 145℃; for 3h; |
- 87-60-5
3-chloro-2-methylbenzenamine
- 88-65-3
2-bromobenzoic-acid
A
- 13710-22-0
N-(3-chlorotolyl)-anthranilic acid
B
- 13710-19-5
tolfenamic Acid
| Conditions | Yield |
|---|---|
| With potassium hydroxide; sodium carbonate In pentan-1-ol; water |
| Conditions | Yield |
|---|---|
| With potassium acetate; copper diacetate; copper at 140℃; Inert atmosphere; |
- 13710-19-5
tolfenamic Acid
| Conditions | Yield |
|---|---|
| With water; potassium hydroxide In ethanol at 95℃; for 16h; Inert atmosphere; | 192 mg |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: phenylsilane; 1,2,2,3,4,4-hexamethylphosphetane 1-oxide / m-xylene / 5 h / 120 °C / Inert atmosphere 2: potassium hydroxide; water / ethanol / 16 h / 95 °C / Inert atmosphere View Scheme |
| Conditions | Yield |
|---|---|
| In methanol at 20℃; | 100% |
| Conditions | Yield |
|---|---|
| In methanol at 20℃; | 100% |
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Chemistry
Product Name: N-(3-Chloro-ortho-tolyl) anthranilic acid
The MF of N-(3-Chloro-ortho-tolyl) anthranilic acid(13710-19-5) is C14H12ClNO2.
The MW of N-(3-Chloro-ortho-tolyl) anthranilic acid(13710-19-5) is 261.7.
Synonyms: CLOTAM;LABOTEST-BB LT00772313;2-(3-CHLORO-O-TOLUIDINO)BENZOIC ACID;2 (3-CHLORO-2-METHYLANILINO)BENZOIC ACID;gea6414;2-[(3-CHLORO-2-METHYLPHENYL)AMINO]BENZOIC ACID;TOLFENAMIC ACID;2-((3-chloro-2-methylphenyl)amino)-benzoicaci
Product Categories: Active Pharmaceutical Ingredients
Mol File: 13710-19-5.mol
EINECS: 237-264-3
Surface Tension: 55.7 dyne/cm
Density: 1.333 g/ml
Flash Point: 199 °C
Enthalpy of Vaporization: 69.28 kJ/mol
Boiling Point: 405.4 °C at 760 mmHg
Vapour Pressure: 2.66E-07 mmHg at 25°C
mp: 210-214°C
Merck: 9513
CAS DataBase Reference: 13710-19-5(CAS DataBase Reference)
Uses
Toxicity Data With Reference
| 1. | orl-rat LD50:225 mg/kg | TOIZAG Toho Igakkai Zasshi. Journal of Medical Society of Toho University. 28 (1981),99. | ||
| 2. | ipr-rat LD50:238 mg/kg | TOIZAG Toho Igakkai Zasshi. Journal of Medical Society of Toho University. 29 (1983),851. | ||
| 3. | scu-rat LD50:246 mg/kg | IYKEDH Iyakuhin Kenkyu. Study of Medical Supplies. 14 (1983),838. | ||
| 4. | orl-mus LD50:280 mg/kg | IYKEDH Iyakuhin Kenkyu. Study of Medical Supplies. 14 (1983),838. | ||
| 5. | ipr-mus LD50:185 mg/kg | IYKEDH Iyakuhin Kenkyu. Study of Medical Supplies. 14 (1983),838. | ||
| 6. | scu-mus LD50:267 mg/kg | IYKEDH Iyakuhin Kenkyu. Study of Medical Supplies. 14 (1983),838. |
Safety Profile
Safety information of N-(3-Chloro-ortho-tolyl) anthranilic acid(13710-19-5):
Hazard Codes:
Xn Risk Statements: 22
R22: Harmful if swallowed ;
RIDADR: UN 2811 6.1/PG 3
WGK Germany: 3
RTECS: CB2687500