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1522-22-1

Basic Information
CAS No.: 1522-22-1
Name: HEXAFLUOROACETYLACETONE
Article Data: 13
Molecular Structure:
Molecular Structure of 1522-22-1 (HEXAFLUOROACETYLACETONE)
Formula: C5H2F6O2
Molecular Weight: 208.06
Synonyms: 1,1,1,5,5,5-Hexafluoro-2,4-pentandione;1,1,1,5,5,5-Hexafluoro-2,4-pentanedione;1,1,1,5,5,5-Hexafluoroacetylacetone;1,3-Bis(trifluoromethyl)propane-1,3-dione;Hexafluoro-2,4-pentanedione;Hexafluoroacetylacetone;
EINECS: 216-191-0
Density: 1.506 g/cm3
Boiling Point: 70 °C at 760 mmHg
Flash Point: 30.8 °C
Solubility: Not miscible in water.
Appearance: clear colorless to slightly yellow liquid
Hazard Symbols: CorrosiveC, FlammableF, IrritantXi
Risk Codes: 10-20/21/22-34
Safety: 26-36/37/39-45
Transport Information: UN 2920 8/PG 2
PSA: 34.14000
LogP: 1.63930
Synthetic route

1,1,1,5,5,5-hexafluoro-3-pentyn-2-one trimethylsilylethyl ketal

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

Conditions
ConditionsYield
With sulfuric acid In tetrahydrofuran; water at 40 - 50℃; for 7.5h;93%
69962-11-4

1,1,1,5,5,5-hexafluoro-3-trifluoromethyl-pentane-2,4-dione

A

400-49-7

trifluoromethyl 2,2,2-trifluororethyl ketone

B

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

C

76-05-1

trifluoroacetic acid

Conditions
ConditionsYield
With water 1.) 20 deg C, 7 d, 2.) 100 - 110 deg C, 70 h; Title compound not separated from byproducts;
69962-11-4

1,1,1,5,5,5-hexafluoro-3-trifluoromethyl-pentane-2,4-dione

A

400-49-7

trifluoromethyl 2,2,2-trifluororethyl ketone

B

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

C

trifluoroperacetic acid

D

1,1-bis(trifluoroacetyl)-2,2,2-trifluoroethane monohydrate

E

76-05-1

trifluoroacetic acid

Conditions
ConditionsYield
With water at 20℃; for 168h; Product distribution; other temp., other time;
72721-52-9

1,1,1,5,5,5-hexafluoro-3-trifluoroacetyl-pentane-2,4-dione

A

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

B

76-05-1

trifluoroacetic acid

Conditions
ConditionsYield
With water Title compound not separated from byproducts;
72721-52-9

1,1,1,5,5,5-hexafluoro-3-trifluoroacetyl-pentane-2,4-dione

A

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

B

1,1,1,5,5,5-hexafluoro-3-trifluoroacetyl-pentane-2,4-dione enol tautomer

C

76-05-1

trifluoroacetic acid

Conditions
ConditionsYield
With sulfuric acid; phosphorus pentoxide at 20℃; Product distribution; effect of temp. on keto-enol equilibrium;
428-75-1

bis(gem-diol) 1,1,1,5,5,5-hexafluoropentane-2,2,4,4-tetraol

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

Conditions
ConditionsYield
With sulfuric acid In toluene at 80℃;
With sulfuric acid In tert-butyl methyl ether; toluene at 20℃; for 5h;
With sulfuric acid In tetrahydrofuran; toluene at 20℃; for 5h;
421-50-1

1,1,1-trifluoro-2-propanone

383-63-1

ethyl trifluoroacetate,

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

(hexafluoroacetylacetonato)(1,5-cyclooctadiene)rhodium(I)

326-06-7

1-Phenyl-4,4,4-trifluorobutane-1,3-dione

A

(trifluorobenzoylacetonato)(1,5-cyclooctadiene)rhodium(I)

B

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

Conditions
ConditionsYield
In Petroleum ether Kinetics; React. in the temp. range from 14.8-24.8°C (10-fold excess TFBA).; Monitoring by UV.;
661-54-1

3,3,3-trifluoroprop-1-yne

383-63-1

ethyl trifluoroacetate,

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

Conditions
ConditionsYield
Stage #1: 3,3,3-trifluoroprop-1-yne With n-butyllithium In n-heptane; tert-butyl methyl ether at -103 - -28℃; Inert atmosphere; Large scale;
Stage #2: ethyl trifluoroacetate, In n-heptane; tert-butyl methyl ether at -38 - -30℃; for 2h; Inert atmosphere; Large scale; Further stages;
2.6 kg
Stage #1: 3,3,3-trifluoroprop-1-yne With n-butyllithium In tetrahydrofuran; hexane at -30℃; for 0.25h; Inert atmosphere;
Stage #2: ethyl trifluoroacetate, In tetrahydrofuran; hexane at -30℃; for 2h; Inert atmosphere;
Stage #3: With sulfuric acid In tetrahydrofuran at 10℃; for 3.58h;
2.7 g

ferric hydroxide

1522-22-1

1,1,1,5,5,5-hexafluoroacetylacetone

Fe(hexafluoropentanedionate)3

Conditions
ConditionsYield
boat with starting metal compound placed in apparatus for thermoradiometric studies, Ar saturated at 50°C with HHFA, flow rate 0.5-2l/h, temp. rise 4°C/min, duration 50min; sublimation;100%
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  • 1,1,1,5,5,5-Hexafluoropentane-2,4-dione

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    1522-22-1

    1,1,1,5,5,5-Hexafluoropentane-2,4-dione

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Chemistry

Molecular Structure:

Molecular Formula: C5H2F6O2
Molecular Weight: 208.0586
IUPAC Name: 1,1,1,5,5,5-Hexafluoropentane-2,4-dione
Synonyms of 1,1,1,5,5,5-Hexafluoropentane-2,4-dione (CAS NO.1522-22-1): 1,1,1,5,5,5-Hexafluoroacetylacetone ; EINECS 216-191-0 ; Hexafluoroacetylacetone ; 2,4-Pentanedione, 1,1,1,5,5,5-hexafluoro-
CAS NO: 1522-22-1
Product Categories: Halogen compounds 
Index of Refraction: 1.304
Molar Refractivity: 26.18 cm3
Molar Volume: 138 cm3
Surface Tension: 19 dyne/cm
Density: 1.506 g/cm3
Flash Point: 30.8 °C
Enthalpy of Vaporization: 31.16 kJ/mol
Boiling Point: 70 °C at 760 mmHg
Vapour Pressure of 1,1,1,5,5,5-Hexafluoropentane-2,4-dione (CAS NO.1522-22-1): 131 mmHg at 25°C

Safety Profile

Hazard Codes of 1,1,1,5,5,5-Hexafluoropentane-2,4-dione (CAS NO.1522-22-1): CorrosiveC,FlammableF,IrritantXi
Risk Statements: 10-20/21/22-34 
R10: Flammable. 
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed. 
R34: Causes burns.
Safety Statements: 26-36/37/39-45 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection. 
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
RIDADR: UN 2920 8/PG 2
WGK Germany: 3
F: 3
Hazard Note: Flammable/Corrosive
TSCA: T
HazardClass: 8
PackingGroup: II