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1533519-84-4

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Basic Information
CAS No.: 1533519-84-4
Name: 4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione
Article Data: 3
Molecular Structure:
Molecular Structure of 1533519-84-4 (4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione)
Formula: C15H13N3S
Molecular Weight: 267.354
Synonyms: 4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione;lesinurad int.4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione;4-(4-Cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazole-3-thiol;Sodium 2-((4-(4-cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazol-3-yl)thio)acetate;4-(4-cyclopropylnaphthalen-1-yl)-2,4-dihydro-3H-1,2,4-triazole-3-thione;Lesinurad Impurity 21;4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione (for Lesinurad)
EINECS: 943-285-5
Density: 1.41±0.1 g/cm3(Predicted)
Boiling Point: 435.2±38.0 °C(Predicted)
PSA: 69.51000
LogP: 3.58660
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Synthetic route
1533519-86-6

N-(4-cyclopropylnaphthalen-1-yl)-2-formylhydrazine-1-thiocarboxamide

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4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
With water; sodium hydroxide In N,N-dimethyl-formamide at 30℃; for 16h; Solvent; Temperature; Reagent/catalyst;90%
With potassium hydrogencarbonate In water; N,N-dimethyl-formamide at 90 - 140℃;

C12H8ClN3S

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cyclopropylmagnesium bromide

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
In tetrahydrofuran for 2h;89.89%
878671-94-4

1-amino-4-cyclopropylnaphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
2: N,N-dimethyl-formamide / 50 - 55 °C
3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 4 steps
1: toluene; water
2: potassium hydroxide
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 3 steps
1.1: potassium carbonate / water; N,N-dimethyl-formamide / 3.5 h / 15 °C
1.2: 1 h / 0 °C
1.3: 2 h
2.1: ethyl acetate / 2 h / 60 °C
3.1: sodium hydroxide; water / N,N-dimethyl-formamide / 16 h / 30 °C
View Scheme
90-11-9

1-Bromonaphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C
2: nitric acid / 0 - 20 °C
3: palladium on activated charcoal; hydrogen
4: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
5: N,N-dimethyl-formamide / 50 - 55 °C
6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 6 steps
1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C
2: nitric acid / 0 - 20 °C
3: hydrazine hydrate / methanol / Reflux
4: potassium hydroxide / dichloromethane
5: N,N-dimethyl-formamide / 50 - 55 °C
6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 7 steps
1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C
2: nitric acid / 0 - 20 °C
3: palladium on activated charcoal; hydrogen
4: toluene; water
5: potassium hydroxide
6: N,N-dimethyl-formamide / 50 - 55 °C
7: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
25033-19-6

1-cyclopropyl-naphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: nitric acid / 0 - 20 °C
2: palladium on activated charcoal; hydrogen
3: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
4: N,N-dimethyl-formamide / 50 - 55 °C
5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 5 steps
1: nitric acid / 0 - 20 °C
2: hydrazine hydrate / methanol / Reflux
3: potassium hydroxide / dichloromethane
4: N,N-dimethyl-formamide / 50 - 55 °C
5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 6 steps
1: nitric acid / 0 - 20 °C
2: palladium on activated charcoal; hydrogen
3: toluene; water
4: potassium hydroxide
5: N,N-dimethyl-formamide / 50 - 55 °C
6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
878671-93-3

1-cyclopropyl-4-nitronaphthalene

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: palladium on activated charcoal; hydrogen
2: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 4 steps
1: hydrazine hydrate / methanol / Reflux
2: potassium hydroxide / dichloromethane
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 5 steps
1: palladium on activated charcoal; hydrogen
2: toluene; water
3: potassium hydroxide
4: N,N-dimethyl-formamide / 50 - 55 °C
5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
1533519-87-7

1-amino-4-cyclopropylnaphthalene oxalate

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium hydroxide
2: N,N-dimethyl-formamide / 50 - 55 °C
3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
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(1-cyclopropylnaphthalen-4-yl)isothiocyanate

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N,N-dimethyl-formamide / 50 - 55 °C
2: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
Multi-step reaction with 2 steps
1: ethyl acetate / 2 h / 60 °C
2: sodium hydroxide; water / N,N-dimethyl-formamide / 16 h / 30 °C
View Scheme
1533519-92-4

1-amino-4-cyclopropylnaphthalene hydrochloride

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium hydroxide / dichloromethane
2: N,N-dimethyl-formamide / 50 - 55 °C
3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
1533519-91-3

tert-butyl 4-cyclopropylnaphthalen-1-ylcarbamate

1533519-84-4

4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrogenchloride / ethanol
2: potassium hydroxide / dichloromethane
3: N,N-dimethyl-formamide / 50 - 55 °C
4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C
View Scheme
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    Product name: 4-(4-Cyclopropylnaphthalen-1-yl)-1H-1,2,4-Triazole-5(4H)-Thione CAS No.：1533519-84-4 Molecule Formula：C15H13N3S Molecule Weight：267.35 Purity: 98.0% Package: 25kg/drum Description：White or off-white powder Manufacture Standards：E

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    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

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    High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

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    China (Mainland)  |  Contact Details

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    1533519-84-4

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     China (Mainland)  |  Contact Details

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