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168173-56-6

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Basic Information
CAS No.: 168173-56-6
Name: Pyridine, 2-bromo-5-(chloromethyl)- (9CI)
Article Data: 9
Molecular Structure:
Molecular Structure of 168173-56-6 (Pyridine, 2-bromo-5-(chloromethyl)- (9CI))
Formula: C6H5 Br Cl N
Molecular Weight: 206.469
Synonyms: 2-Bromo-5-(chloromethyl)pyridine
Density: 1.631g/cm3
Boiling Point: 285ºC at 760 mmHg
Flash Point: 126.2ºC
PSA: 12.89000
LogP: 2.58290
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Synthetic route
122306-01-8

2-bromo-5-(hydroxymethyl)pyridine

168173-56-6

2-bromo-5-pyridylmethyl chloride

Conditions
ConditionsYield
Stage #1: 2-bromo-5-(hydroxymethyl)pyridine With thionyl chloride at -60℃; for 1h;
Stage #2: With sodium hydrogencarbonate In water; ethyl acetate		91%
With thionyl chloride In dichloromethane91%
With sodium hydroxide; thionyl chloride In water; toluene; acetonitrile
6311-35-9

6-bromonicotinic acid

168173-56-6

2-bromo-5-pyridylmethyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
1.2: 0 - 20 °C
2.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 20 °C / Cooling with ice
View Scheme
149806-06-4

6-bromonicotinaldehyde

168173-56-6

2-bromo-5-pyridylmethyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium tetrahydroborate; ethanol / 20 °C / Inert atmosphere
2: thionyl chloride / 1 h / -60 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium tetrahydroborate
2: thionyl chloride
View Scheme
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / tetrahydrofuran / 2 h / 0 - 20 °C
2: thionyl chloride / dichloromethane / 2 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere
2: thionyl chloride / chloroform / 4 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium tetrahydroborate / ethanol / 24 h / 20 °C / Inert atmosphere
2: thionyl chloride / dichloromethane
View Scheme
168173-56-6

2-bromo-5-pyridylmethyl chloride

143-33-9

sodium cyanide

144873-99-4

(6-bromopyridine-3-yl)acetonitrile

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 48h;90%
168173-56-6

2-bromo-5-pyridylmethyl chloride

C12H16F2N2O3

3-(6-bromopyridin-3-ylmethyl)-4-(2,2-difluoroethylamino)-8-(methoxyimino)-1-oxaspiro[4.5]dec-3-en-2-one

Conditions
ConditionsYield
Stage #1: C12H16F2N2O3 With caesium carbonate In acetonitrile at 0 - 20℃; for 4h;
Stage #2: 2-bromo-5-pyridylmethyl chloride In acetonitrile for 12h; Reflux; regioselective reaction;		80%
168173-56-6

2-bromo-5-pyridylmethyl chloride

4-(2,2-difluoroethylamino)-5,5-dimethylfuran-2(5H)-one

3-(6-bromopyridin-3-ylmethyl)-4-(2,2-difluoroethylamino)-5,5-dimethylfuran-2(5H)-one

Conditions
ConditionsYield
Stage #1: 4-(2,2-difluoroethylamino)-5,5-dimethylfuran-2(5H)-one With caesium carbonate In acetonitrile at 0 - 20℃; for 4h;
Stage #2: 2-bromo-5-pyridylmethyl chloride In acetonitrile for 12h; Reflux; regioselective reaction;		78%
168173-56-6

2-bromo-5-pyridylmethyl chloride

C12H17F2NO3

3-(6-bromopyridin-3-ylmethyl)-4-(2,2-difluoroethylamino)-8-methoxy-1-oxaspiro[4.5]dec-3-en-2-one

Conditions
ConditionsYield
Stage #1: C12H17F2NO3 With caesium carbonate In acetonitrile at 0 - 20℃; for 4h;
Stage #2: 2-bromo-5-pyridylmethyl chloride In acetonitrile for 12h; Reflux; regioselective reaction;		74%
168173-56-6

2-bromo-5-pyridylmethyl chloride

C11H15F2NO2

3-(6-bromopyridin-3-ylmethyl)-4-(2,2-difluoroethylamino)-1-oxaspiro[4.5]dec-3-en-2-one

Conditions
ConditionsYield
Stage #1: C11H15F2NO2 With caesium carbonate In acetonitrile at 0 - 20℃; for 4h;
Stage #2: 2-bromo-5-pyridylmethyl chloride In acetonitrile for 12h; Reflux; regioselective reaction;		70%
106-52-5

N-methyl-4-hydroxypiperidine

168173-56-6

2-bromo-5-pyridylmethyl chloride

C12H17BrN2O

Conditions
ConditionsYield
Stage #1: N-methyl-4-hydroxypiperidine With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h;
Stage #2: 2-bromo-5-pyridylmethyl chloride In N,N-dimethyl-formamide at 0 - 20℃;		50%
1603-91-4

4-methylthiazol-2-ylamine

168173-56-6

2-bromo-5-pyridylmethyl chloride

3-(6-bromo-3-pyridyl)methyl-2-imino-4-methyl-2,3-dihydrothiazole hydrochloride

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    Hangzhou Fenjunchem Co.,Ltd dedicated to the development, production and marketing of chemicals which is specialized in Organic compounds; Active Pharmaceutical Ingredient(s); Nutr

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    Business Type:Trading Company

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  • 168173-56-6

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    Business Type:Lab/Research institutions

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  • Advantage supply 168173-56-6 2-BROMO-5-(CHLOROMETHYL)PYRIDINE

  • Casno:

    168173-56-6

    Advantage supply 168173-56-6 2-BROMO-5-(CHLOROMETHYL)PYRIDINE

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    Advantageous manufacturers Storage:low temperature storage Application:Research and development of pharmaceutical intermediates

    Xi'an Zhenghao Biotechnology Co., Ltd. was established in 2021. It is a high-tech enterprise specializing in the research and development and production of pharmaceutical intermedi

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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  • Pyridine,2-bromo-5-(chloromethyl)-

  • Casno:

    168173-56-6

    Pyridine,2-bromo-5-(chloromethyl)-

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    Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

  • Chemical Co.Ltd

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