CAS No.19130-96-2,1-Deoxynojirimycin Suppliers

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Basic Information

Molecular Structure:
CAS No.:	19130-96-2
Name:	1-Deoxynojirimycin
Article Data:	102

Formula:	C₆H₁₃NO₄
Molecular Weight:	163.174
Synonyms:	UNII-FZ56898FLE;1,5-Deoxy-1,5-imino-D-mannitol;
EINECS:	606-239-2
Density:	1.456 g/cm³
Melting Point:	195-196 °C
Boiling Point:	361.1 °C at 760 mmHg
Flash Point:	197.3 °C
Solubility:	soluble in water
Appearance:	white crystalline solid
Hazard Symbols:	Xi
Risk Codes:	R36/37/38
Safety:	24/25
PSA:	92.95000
LogP:	-2.63800

Synthetic route

: 69567-11-9, 76738-52-8, 126836-30-4
2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogenchloride; 20% palladium hydroxide-activated charcoal; hydrogen In methanol; water for 14h;	100%
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In ethanol; water at 20℃; under 3000.3 Torr; for 20h; pH=Ca. 2;	93%
Stage #1: 2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol With hydrogenchloride In ethanol for 0.25h; pH=Ca. 2; Inert atmosphere; Stage #2: With palladium 10% on activated carbon; hydrogen In ethanol under 3000.3 Torr; for 20h; Inert atmosphere;	93%

: 157363-86-5
N-benzyl-3,4-di-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogen; palladium In acetic acid for 15h;	100%
With hydrogen; acetic acid; palladium for 18h;	100%
With palladium 10% on activated carbon; hydrogen In acetic acid at 20℃; for 19h;	98%

: 1190302-84-1
(2R,4aR,7S,8R,8aR)-tert-butyl 8-hydroxy-7-(methoxymethyl)-2-phenyltetrahydro-4H-[1,3]dioxino[5,4-b]pyridine-5(4aH)-carboxylate

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogenchloride In ethanol for 18h; Reflux; Inert atmosphere;	100%

: 132198-14-2
N-Benzhydryl-1-deoxynojirimycin

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogen; palladium dihydroxide In methanol under 3102.9 Torr; for 24h;	99%
With hydrogen; palladium dihydroxide	90%
With hydrogen; palladium on activated charcoal In methanol	50%

: 4-benzyloxy-2-hydroxymethylpiperidine-3,5-diol

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With palladium 10% on activated carbon; hydrogen In tetrahydrofuran; water at 20℃; under 760.051 Torr; for 48h;	98%
With hydrogen; palladium dihydroxide In methanol for 24h;

: 15218-38-9
nojirimycin

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogen; platinum(IV) oxide In ethanol; water under 750.06 Torr; for 18h; Ambient temperature;	97%

: (2R,3R,4R,5S)-3-benzoyloxy-1-benzyloxycarbonyl-4,5-diacetoxy-2-(hydroxymethyl)piperidine

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogenchloride In methanol for 12h; Heating;	94%

: 1017587-22-2
(2R,3R,4R,5S)-(3,4-dibenzyloxy-N-tert-butoxycarbonyl-5-hydroxy-2-piperidinyl)methanol

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethanol at 20℃; for 48h;	92%

: 1,3,6-Tri-O-benzyl-5-(benzyloxycarbonylamino)-5-deoxy-α,β-D-gluco-furanose

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With hydrogen; palladium dihydroxide In acetic acid; tert-butyl alcohol under 3750.3 Torr; for 48h; Ambient temperature;	91%

: 149302-60-3
N-bentyl-2,3,4,6-tetra-O-benzyl-1-deoxynojirimycin

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

Conditions

Conditions	Yield
With 10 wt% Pd(OH)2 on carbon; hydrogen In ethanol; chloroform at 20℃; for 20h;	91%

Raw Materials

57-04-5

Downstream Products

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Chemistry

Molecular structure of 1-Deoxynojirimycin (CAS NO.19130-96-2) is:

Product Name: 1-Deoxynojirimycin
CAS Registry Number: 19130-96-2
IUPAC Name: (2R,3R,4R,5S)-2-(hydroxymethyl)piperidine-3,4,5-triol
Molecular Weight: 163.17172 [g/mol]
Molecular Formula: C₆H₁₃NO₄
XLogP3-AA: -2.3
H-Bond Donor: 5
H-Bond Acceptor: 5
Flash Point: 163.7 °C
Enthalpy of Vaporization: 64.97 kJ/mol
Boiling Point: 347 °C at 760 mmHg
Vapour Pressure: 9.72E-06 mmHg at 25°C
Melting Point: 195-196 °C
Product Categories: Miscellaneous Natural Products; All Inhibitors; Glycosidase Inhibitors; Inhibitors; Miscellaneous Enzyme

Uses

1-Deoxynojirimycin (CAS NO.19130-96-2) is an alpha-glucosidase inhibitor with antiviral action.

Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
rat	LD50	oral	> 5gm/kg (5000mg/kg)	BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY) KIDNEY, URETER, AND BLADDER: URINE VOLUME INCREASED SKIN AND APPENDAGES (SKIN): HAIR: OTHER	International Journal of Toxicology. Vol. 16(Suppl,

Specification

1-Deoxynojirimycin , its cas register number is 19130-96-2. It also can be called 1,5-Deoxy-1,5-imino-D-mannitol ; 1-Deoxymannojirimycin ; UNII-FZ56898FLE ; 3,4,5-Piperidinetriol, 2-(hydroxymethyl)-, (2R-(2alpha,3beta,4alpha,5beta))- .It is a white crystalline solid.