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CAS No.: | 22117-85-7 |
---|---|
Name: | 2-Methoxy-5-sulfamoylbenzoic acid |
Article Data: | 19 |
Molecular Structure: | |
Formula: | C8H9NO5S |
Molecular Weight: | 231.229 |
Synonyms: | o-Anisicacid, 5-sulfamoyl- (8CI);2-Methoxy-5-sulfonamidobenzoic acid;5-(Aminosulfonyl)-2-methoxybenzoic acid; |
EINECS: | 244-789-1 |
Density: | 1.492 g/cm3 |
Melting Point: | 220 °C |
Boiling Point: | 482.5 °C at 760 mmHg |
Flash Point: | 245.6 °C |
Hazard Symbols: | Xi |
Risk Codes: | 36/37/38 |
Safety: | 26-36/37/39 |
PSA: | 115.07000 |
LogP: | 1.82190 |
methyl 2-methoxy-5-sulfamoyl-benzoate
2-methoxy-5-sulfamoylbenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol | 98.3% |
Stage #1: methyl 2-methoxy-5-sulfamoyl-benzoate With sodium hydroxide; water In methanol at 20℃; for 1h; Stage #2: With hydrogenchloride In methanol; water | 98.3% |
Stage #1: methyl 2-methoxy-5-sulfamoyl-benzoate With sodium hydroxide; water In methanol at 20℃; for 1h; Stage #2: With hydrogenchloride In methanol; water | 98.3% |
5-chlorosulfonyl-2-anisic acid
2-methoxy-5-sulfamoylbenzoic acid
Conditions | Yield |
---|---|
With ammonia In tetrahydrofuran for 0.5h; Ambient temperature; | 94.6% |
With ammonia |
2-Methoxybenzoic acid
2-methoxy-5-sulfamoylbenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 84.9 percent / chlorosulfuric acid / 0.67 h / 60 - 70 °C 2: 94.6 percent / NH3 / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 24h; | 95% |
2-methoxy-5-sulfamoylbenzoic acid
copper(II) acetate monohydrate
Conditions | Yield |
---|---|
In ethanol; water at 20℃; for 72h; | 70% |
2-methoxy-5-sulfamoylbenzoic acid
(S)-N-[[3-[3-fluoro-4-[4-morpholinyl]phenyl]-2-oxo-5-oxazolidinyl]methyl]amine
5-(aminosulfonyl)-N-(S)-[[3-[3-fluoro-4-(morpholin-4-yl)phenyl]-2-oxooxazolidin-5-yl]methyl]-2-methoxy benzamide
Conditions | Yield |
---|---|
Stage #1: 2-methoxy-5-sulfamoylbenzoic acid With chloroformic acid ethyl ester; triethylamine In dichloromethane at 0 - 20℃; for 0.5h; Stage #2: (S)-N-[[3-[3-fluoro-4-[4-morpholinyl]phenyl]-2-oxo-5-oxazolidinyl]methyl]amine In dichloromethane at 0 - 20℃; for 4h; | 55% |
2-methoxy-5-sulfamoylbenzoic acid
2-[4-(3-trifluoromethylphenyl)piperazin-1-yl]ethan-1-amine
Conditions | Yield |
---|---|
With triethylamine; isobutyl chloroformate In 1,4-dioxane for 6h; Ambient temperature; | 40% |
2-methoxy-5-sulfamoylbenzoic acid
2--5-methoxytetralin
Conditions | Yield |
---|---|
With chloroformic acid ethyl ester; triethylamine In acetone at 0℃; for 2h; | 32% |
2-methoxy-5-sulfamoylbenzoic acid
3,5-Bis-(trifluoromethyl)aniline
N-[3,5-bis(trifluoromethyl)phenyl]-2-methoxy-5-sulfamoyl-benzamide
Conditions | Yield |
---|---|
24.2% |
1-hydroxy-pyrrolidine-2,5-dione
2-methoxy-5-sulfamoylbenzoic acid
N-hydroxysuccinimido diphenyl phosphate
N-ethyl-2-aminomethylpyrrole
N-[(1-ethyl-2-pyrrolidinyl)methyl]-2-methoxy-5-sulfamoylbenzamide
Conditions | Yield |
---|---|
With triethylamine In acetonitrile | 24% |
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Chemical Name: 2-Methoxy-5-sulfamoylbenzoic acid
IUPAC NAME: 2-methoxy-5-sulfamoylbenzoic acid
CAS No.: 22117-85-7
EINECS: 244-789-1
Molecular Formula: C8H9NO5S
Molecular Weight: 231.23g/mol
Structure:
The synonyms of 2-methoxy-5-sulfamoylbenzoic acid(22117-85-7): 5-sulphamoyl-o-anisic acid;2-Methoxy-5-Sufamoyl Benzoic Acid;5-Aminosulfonyl-2-Methoxybenzoic Acid;5-(Aminosulphonyl)-2-methoxybenzoic acid;2-METHOXY-5-SULFAMOYLBENZOIC ACID;2-METHOXY-5-SULFONYLBENZOIC ACID;2-METHOXY-5-SULPHAMOYLBENZOIC ACID;3-CARBOXY-4-METHOXY-BENZENE SULFONAMIDE;
Density: 1.492 g/cm3
Flash Point: 245.6 °C
Boiling Point: 482.5 °C at 760 mmHg