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30438-74-5

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Basic Information
CAS No.: 30438-74-5
Name: 1-chloro-N,N-diMethylMethanaMine
Article Data: 13
Molecular Structure:
Molecular Structure of 30438-74-5 (1-chloro-N,N-diMethylMethanaMine)
Formula: C3H8 Cl N
Molecular Weight: 93.5562
Synonyms: Trimethylamine,chloro- (6CI,7CI,8CI); (Chloromethyl)dimethylamine; (Dimethylamino)methylchloride; 1-Chloro-N,N-dimethylmethanamine; 1-Chloro-N,N-dimethylmethylamine;Chlorotrimethylamine; Dimethyl(chloromethyl)amine;N-(Chloromethyl)dimethylamine; NSC 97326
Density: 0.967g/cm3
Melting Point: 140-145 °C
Boiling Point: 70.3°Cat760mmHg
Flash Point: °C
PSA: 3.24000
LogP: 0.74430
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Synthetic route
80202-60-4

N-<(trimethylsiloxy)methyl>dimethylamine

A

107-46-0

Hexamethyldisiloxane

B

30438-74-5

N-(chloromethyl)dimethylamine

Conditions
ConditionsYield
With chloro-trimethyl-silane In diethyl ether at 20 - 40℃;A 97%
B 95%
51-80-9

bis-(dimethylamino)methane

30438-74-5

N-(chloromethyl)dimethylamine

Conditions
ConditionsYield
With acetyl chloride In diethyl ether for 2h; Ambient temperature;95%
With hydrogenchloride; N,N-dimethyl-formamide
With tetrachloromethane; chlorine
With benzoyl chloride In diethyl ether
With chloromethyl methyl ether In acetonitrile
75-77-4

chloro-trimethyl-silane

1446511-97-2

C10H28N2O3Si2

A

141-62-8

decamethyltetrasiloxane

B

30438-74-5

N-(chloromethyl)dimethylamine

Conditions
ConditionsYield
In benzene at 40℃; for 20h; Inert atmosphere; Schlenk technique;A 86%
B n/a
...Expand
1446511-97-2

C10H28N2O3Si2

1529-47-1

chlorotrimethylgermane

A

1446512-01-1

C10H30Ge2O3Si2

B

30438-74-5

N-(chloromethyl)dimethylamine

Conditions
ConditionsYield
In benzene at 40℃; for 15h; Inert atmosphere; Schlenk technique;A 57%
B n/a
...Expand
76-86-8

Triphenylsilyl chloride

1446511-97-2

C10H28N2O3Si2

A

7065-59-0

3,3,5,5-tetramethyl-1,1,1,7,7,7-hexaphenyl-tetrasiloxane

B

30438-74-5

N-(chloromethyl)dimethylamine

Conditions
ConditionsYield
In benzene at 40℃; for 20h; Inert atmosphere; Schlenk technique;A 45%
B n/a
...Expand
1446511-97-2

C10H28N2O3Si2

1626-24-0

chlorotriphenylgermane

A

1446512-05-5

C40H42Ge2O3Si2

B

30438-74-5

N-(chloromethyl)dimethylamine

Conditions
ConditionsYield
In benzene at 40℃; for 20h; Inert atmosphere; Schlenk technique;A 33%
B n/a
...Expand
30438-74-5

N-(chloromethyl)dimethylamine

79-39-0

Methacrylamide

N-(dimethylaminomethyl)methacrylamide hydrochloride

Conditions
ConditionsYield
In dichloromethane at 20 - 25℃; Product distribution; Further Variations:; Solvents; Alkylation;98%
4769-97-5

4-nitro-1H-indoIe

30438-74-5

N-(chloromethyl)dimethylamine

7150-46-1

4-nitrogramine

Conditions
ConditionsYield
In acetic acid96%
943983-35-5

2-isobutyl-3-(diethoxyphosphorylmethyl)furan

30438-74-5

N-(chloromethyl)dimethylamine

2-isobutyl-3-(diethoxyphosphorylmethyl)-5-(dimethylaminomethyl)furan hydrochloride

Conditions
ConditionsYield
In acetonitrile at 80℃; for 6h;95%
30438-74-5

N-(chloromethyl)dimethylamine

103559-83-7

hexaphenylcarbodiphosphorane

<1-Triphenylphosphonio-2-dimethylamino-ethyliden-triphenylphosphoran>-chlorid

Conditions
ConditionsYield
In benzene for 2h;90%
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