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Basic Information
| CAS No.: | 35692-30-9 |
|---|---|
| Name: | (p-Chlorophenyl)Trimethoxysilane |
| Article Data: | 3 |
| Molecular Structure: | |
|
|
|
| Formula: | C9H13ClO3Si |
| Molecular Weight: | 232.739 |
| Synonyms: | (4-chloro-phenyl)-trimethoxy-silane;trimethoxy(4-chlorophenyl)silane; |
| Density: | 1.13±0.1 g/cm3(Predicted) |
| Boiling Point: | 214.6±23.0 °C(Predicted) |
| PSA: | 27.69000 |
| LogP: | 1.42510 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With tris(dibenzylideneacetone)dipalladium (0); N-ethyl-N,N-diisopropylamine; tris-(o-tolyl)phosphine In N,N-dimethyl-formamide at 20℃; silylation; |
- 681-84-5
tetramethylorthosilicate
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
Conditions
| Conditions | Yield |
|---|---|
| In tetrahydrofuran at -30 - 20℃; for 13h; Inert atmosphere; | |
| In tetrahydrofuran at -30 - 20℃; for 13h; |
- 603-76-9
1-methylindole
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
- 5905-11-3
2-(4-chlorophenyl)-1-methyl-2-phenyl-1H-indole
Conditions
| Conditions | Yield |
|---|---|
| With tetrabutyl ammonium fluoride; palladium diacetate; acetic acid; silver(l) oxide In tetrahydrofuran; ethanol at 20℃; Inert atmosphere; regioselective reaction; | 93% |
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride In tetrahydrofuran at 60℃; for 1.5h; Hiyama coupling; Inert atmosphere; | 92% |
Conditions
| Conditions | Yield |
|---|---|
| With potassium fluoride; 5,11,17,23-tetra-t-butyl-25,26,27,28-tetrahydroxycalix-4-arene; copper(ll) bromide; magnesium chloride for 8h; Inert atmosphere; Heating; | 92% |
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
- 98-09-9
benzenesulfonyl chloride
- 2051-62-9
4'-biphenyl chloride
Conditions
| Conditions | Yield |
|---|---|
| With tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride In N,N-dimethyl-formamide; acetonitrile at 100℃; for 3h; Hiyama Coupling; Inert atmosphere; Green chemistry; | 86% |
- 20414-85-1, 22132-97-4, 52720-03-3, 121123-21-5
S-methyl-S-(p-tolyl)sulfoximine
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
- 56158-16-8
N-(4-chloro)phenyl-S-(4-methyl)phenyl-S-methylsulfoximine
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) iodide; tetrabutyl ammonium fluoride; oxygen In dichloromethane at 20℃; for 12h; Schlenk technique; Green chemistry; | 84% |
- 221044-05-9
N-(2-pyrimidyl)indole
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
- 1310708-95-2
2-(4-chlorophenyl)-1-(pyrimidin-2-yl)-1H-indole
Conditions
| Conditions | Yield |
|---|---|
| With copper (II)-fluoride; silver hexafluoroantimonate; [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In water at 140℃; for 20h; Hiyama Coupling; Inert atmosphere; Green chemistry; | 81% |
| With copper (II)-fluoride; oxygen; cobalt(III) acetylacetonate In toluene at 160℃; under 760.051 Torr; for 24h; Hiyama Coupling; Sealed tube; | 63% |
- 22133-00-2
(3-chlorophenyl)(imino)(methyl)-λ6-sulfanone
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) iodide; tetrabutyl ammonium fluoride; oxygen In dichloromethane at 20℃; for 12h; Schlenk technique; Green chemistry; | 80% |
- 201230-82-2
carbon monoxide
- 35692-30-9
(4-chlorophenyl)trimethoxysilane
- 62-53-3
aniline
- 6833-15-4
4-chlorobenzanilide
Conditions
| Conditions | Yield |
|---|---|
| With copper (II)-fluoride; bis(triphenylphosphine)palladium(II) dichloride In acetonitrile at 80℃; under 760.051 Torr; for 24h; Hiyama Coupling; Schlenk technique; | 80% |
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(p-Chlorophenyl)Trimethoxysilane
