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Basic Information
| CAS No.: | 40682-54-0 |
|---|---|
| Name: | ([1-PHENYL-METH-(E)-YLIDENE]-AMINO)-ACETIC ACID ETHYL ESTER |
| Article Data: | 36 |
| Molecular Structure: | |
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|
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| Formula: | C11H13 N O2 |
| Molecular Weight: | 191.23 |
| Synonyms: | Glycine,N-benzylidene-, ethyl ester (7CI); Benzylideneglycine ethyl ester; Ethyl(benzylideneamino)acetate; Ethyl N-benzylideneglycinate; N-Benzylideneglycineethyl ester; NSC 617266 |
| Density: | 1.01g/cm3 |
| Boiling Point: | 274.1°C at 760 mmHg |
| Flash Point: | 113.9°C |
| PSA: | 38.66000 |
| LogP: | 1.66860 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With magnesium sulfate In dichloromethane at 20℃; | 100% |
| With diethyl ether | |
| In ethanol Heating; |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: glycine ethyl ester hydrochloride With ammonia In dichloromethane; water Stage #2: benzaldehyde With magnesium sulfate In dichloromethane at 20℃; Inert atmosphere; | 100% |
| With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 10h; | 98% |
| With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 8h; Time; | 94% |
- 40682-54-0
ethyl N-benzylideneglycinate
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydride In tetrahydrofuran Ambient temperature; |
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 82 percent / dimethylsulfoxide / 2 h 2: NaH / tetrahydrofuran / Ambient temperature View Scheme |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: ethyl 2-aminoacetate hydrochloride With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 1h; Stage #2: benzaldehyde In dichloromethane at 20℃; |
- 40682-54-0
ethyl N-benzylideneglycinate
- 70591-46-7
(S)-5-methoxycarbonylmethyl-6,6-dimethyl-2-cyclohexen-1-one
Conditions
| Conditions | Yield |
|---|---|
| With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 3h; | 100% |
- 40682-54-0
ethyl N-benzylideneglycinate
Conditions
| Conditions | Yield |
|---|---|
| With tetrakis(acetonitrile)copper(I) perchlorate; (R,R,R)-[2-(4,5-diphenyl-4,5-dihydro-1,3-oxazol-2-yl)ferrocenyl]diphenylphosphine; potassium carbonate In dichloromethane at 20℃; for 10h; Inert atmosphere; stereoselective reaction; | 98% |
- 40682-54-0
ethyl N-benzylideneglycinate
- 107-13-1
acrylonitrile
Conditions
| Conditions | Yield |
|---|---|
| With copper(I) tetrafluoroborate; C42H32F6N3O2P; triethylamine In dichloromethane Molecular sieve; Inert atmosphere; | 98% |
| With tetrakis(acetonitrile)copper(I)tetrafluoroborate; C42H32F6N3O2P; triethylamine In dichloromethane at 0℃; Molecular sieve; Inert atmosphere; stereoselective reaction; | 98% |
- 40682-54-0
ethyl N-benzylideneglycinate
- 100-39-0
benzyl bromide
- 78843-66-0
3-Phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester
Conditions
| Conditions | Yield |
|---|---|
| With sodium carbonate; potassium carbonate; N-benzyl-N,N,N-triethylammonium chloride In acetonitrile for 10h; Ambient temperature; | 97% |
- 40682-54-0
ethyl N-benzylideneglycinate
- 343830-62-6
1-benzyl-(Z)-3-(benzylidene)indolin-2-one
Conditions
| Conditions | Yield |
|---|---|
| With C24H29F6N4O2S(1+)*Br(1-); potassium carbonate In diethyl ether at 20℃; for 4h; stereoselective reaction; | 97% |
- Total:15 Page 1 of 1 1
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([1-PHENYL-METH-(E)-YLIDENE]-AMINO)-ACETIC ACID ETHYL ESTER
