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Basic Information
| CAS No.: | 4875-10-9 |
|---|---|
| Name: | 2-NITROTHIOPHENOL |
| Molecular Structure: | |
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| Formula: | C6H5 N O2 S |
| Molecular Weight: | 155.177 |
| Synonyms: | Benzenethiol,o-nitro- (6CI,7CI,8CI); 2-Nitrobenzenethiol; 2-Nitrothiophenol;o-Mercaptonitrobenzene; o-Nitrobenzenethiol; o-Nitrothiophenol |
| Density: | 1.362g/cm3 |
| Melting Point: | 56 °C |
| Boiling Point: | 262.5°Cat760mmHg |
| Flash Point: | 112.6°C |
| PSA: | 84.62000 |
| LogP: | 2.40670 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate In tetrahydrofuran | 100% |
| With triisopropoxyborohydride In tetrahydrofuran at 0℃; for 0.25h; | 92% |
| With triphenylphosphine; 2-hydroxyethanethiol In tetrahydrofuran; water at 50℃; for 21h; Inert atmosphere; | 90% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium tetrahydroborate; zirconium(IV) chloride In tetrahydrofuran at 35℃; for 0.5h; Reduction; | A 10% B 90% |
| With sodium tetrahydroborate; zirconium(IV) chloride In tetrahydrofuran at 35℃; for 0.166667h; Reduction; | A 80% B 20% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium sulfide In N,N-dimethyl-formamide for 62h; Ambient temperature; | 87% |
| With thiourea In ethanol Heating; | 60% |
| With ethanol; sodium disulfide |
- 108732-56-5
4-o-nitrophenylthio-1,2-naphthoquinone
A
- 83-72-7
2-Hydroxy-1,4-naphthoquinone
B
- 4875-10-9
2-nitrothiophenol
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In ethanol; water for 0.0333333h; | A 80% B n/a |
Conditions
| Conditions | Yield |
|---|---|
| In hydrogenchloride | 61% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium sulfide In N,N-dimethyl-formamide for 62h; Ambient temperature; | A 60% B 25% |
| With sodium sulfide In dimethyl sulfoxide at 50℃; for 0.5h; Product distribution; further reagents, further solvent, further substituted o-chloronitrobenzenes, further times and temp.; | A 10% B 50% |
- 67-56-1
methanol
- 3406-02-8
bis(phenylsulfonyl)methane
- 124-41-4
sodium methylate
A
- 4875-10-9
2-nitrothiophenol
B
- 73622-50-1
Bis(phenylsulfonyl)(phenylthio)methane
Conditions
| Conditions | Yield |
|---|---|
| anschliessendes Behandeln mit <2-Nitro-phenyl>-phenyl-disulfid; |
...Expand
- 64-17-5
ethanol
- 28215-02-3
(2-nitro-phenyl)-phenyl disulfide
- 3111-52-2
potassium thiophenolate
A
- 1155-00-6
bis(2-nitrophenyl)disulfide
B
- 4875-10-9
2-nitrothiophenol
C
- 882-33-7
diphenyldisulfane
...Expand
- 22024-99-3
2-nitrobenzenesulfenyl bromide
- 4875-10-9
2-nitrothiophenol
Conditions
| Conditions | Yield |
|---|---|
| With phosphorus tribromide Verduennen mit Aether und anschliessendes Versetzen mit Wasser; |
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2-NITROTHIOPHENOL
Chemistry
The molecular formula of 2-NITROTHIOPHENOL(4875-10-9) is C6H5NO2S and its formula weight is 155.17.
The chemical synonyms of 2-NITROTHIOPHENOL(4875-10-9) are 2-NITROTHIOPHENOL;2-Nitro-benzenethiol;o-Nitrothiophenol;o-Nitromercaptobenzene;2-Nitrobenzene-1-thiol
The molecular structure of 2-NITROTHIOPHENOL(4875-10-9):
The chemical synonyms of 2-NITROTHIOPHENOL(4875-10-9) are 2-NITROTHIOPHENOL;2-Nitro-benzenethiol;o-Nitrothiophenol;o-Nitromercaptobenzene;2-Nitrobenzene-1-thiol
The molecular structure of 2-NITROTHIOPHENOL(4875-10-9):