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499-61-6

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Basic Information
CAS No.: 499-61-6
Name: 2-amino-1-(3,4-dihydroxyphenyl)ethan-1-one
Article Data: 16
Molecular Structure:
Molecular Structure of 499-61-6 (2-amino-1-(3,4-dihydroxyphenyl)ethan-1-one)
Formula: C8H9 N O3
Molecular Weight: 167.164
Synonyms: Acetophenone,2-amino-3',4'-dihydroxy- (6CI,7CI,8CI); 2-Amino-3',4'-dihydroxyacetophenone;Arterenon; Arterenone; Noradrenalone; U 0603
Density: 1.375g/cm3
Melting Point: 235 °C (decomp)
Boiling Point: 435.1°Cat760mmHg
Flash Point: 217°C
PSA: 83.55000
LogP: 0.93950
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Synthetic route
C14H19N4O3(1+)*Cl(1-)

C14H19N4O3(1+)*Cl(1-)

499-61-6

arterenone

Conditions
ConditionsYield
Stage #1: C14H19N4O3(1+)*Cl(1-) With hydrogenchloride In methanol; water at 60 - 65℃; for 3 - 4h;
Stage #2: With hydrogenchloride In isopropyl alcohol		96.3%
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benzene-1,2-diol

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glycine

499-61-6

arterenone

Conditions
ConditionsYield
Stage #1: benzene-1,2-diol With zinc(II) chloride In 1,2-dichloro-ethane at 10 - 15℃; for 0.5h;
Stage #2: glycine In 1,2-dichloro-ethane at 70℃; for 20h; Time;		78.8%
Stage #1: benzene-1,2-diol With zinc(II) chloride In 1,2-dichloro-ethane at 10 - 70℃; for 0.5h;
Stage #2: glycine In 1,2-dichloro-ethane for 20h; Concentration; Reflux;		76.82%
99-40-1

2-chloro-3',4'-dihydroxyacetophenone

499-61-6

arterenone

Conditions
ConditionsYield
With ammonium hydroxide
Multi-step reaction with 2 steps
1: H2O; NaN3
2: palladium; aq.-ethanolic HCl / Hydrogenation
View Scheme
70216-33-0

N-(2-(3,4-dimethoxyphenyl)-2-oxoethyl)benzamide

499-61-6

arterenone

Conditions
ConditionsYield
With mineral acid
13062-58-3

2-dibenzylamino-1-(3,4-dihydroxy-phenyl)-ethanone

499-61-6

arterenone

Conditions
ConditionsYield
With water; palladium under 7355.08 Torr; Hydrogenation;
165947-83-1

2-azido-1-(3,4-dihydroxy-phenyl)-ethanone

499-61-6

arterenone

Conditions
ConditionsYield
With hydrogenchloride; palladium Hydrogenation;
187101-62-8

2,5-bis-(3,4-dimethoxy-phenyl)-pyrazine

499-61-6

arterenone

Conditions
ConditionsYield
With hydrogen iodide; acetic acid
40869-57-6

2-amino-1-(3,4-dimethoxy-phenyl)-ethanone

499-61-6

arterenone

Conditions
ConditionsYield
With hydrogenchloride

1-(3,4-dihydroxy-phenyl)-2-nitro-ethanone

A

138-65-8

Norepinephrine

B

499-61-6

arterenone

Conditions
ConditionsYield
bei der Reduktion;

1-(3,4-dihydroxy-phenyl)-2-nitro-ethanone

499-61-6

arterenone

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