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Basic Information
CAS No.: 52314-67-7
Name: 3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride
Article Data: 22
Molecular Structure:
Molecular Structure of 52314-67-7 (3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride)
Formula: C8H9Cl3O
Molecular Weight: 227.518
Synonyms: 2,2-Dimethyl-3-(2,2-dichloroethenyl)cyclopropanecarbonylchloride;2,2-Dimethyl-3-(2,2-dichlorovinyl)cyclopropanecarbonyl chloride;3-(2,2-Dichloroethenyl)-2,2-dimethylcyclopropanecarbonyl chloride;3-(2,2-Dichlorovinyl)-2,2-dimethyl-1-cyclopropanecarbonyl chloride;3-(2,2-Dichlorovinyl)-2,2-dimethylcyclopropanecarbonyl chloride;
EINECS: 257-840-8
Density: 1.424 g/cm3
Boiling Point: 242.4 °C at 760 mmHg
Flash Point: 98.9 °C
Solubility: 123.2mg/L at 25℃
PSA: 17.07000
LogP: 3.34300
Synthetic route
55701-05-8

3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylic acid

52314-67-7

permethric acid chloride

Conditions
ConditionsYield
With phosgene; triethylamine at 100℃; for 2h;96.1%
With thionyl chloride Heating;
With thionyl chloride Heating;
Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 73.4 percent / 1 M aq. NaOH / tetrahydrofuran / 36 h / Heating
2: SOCl2 / Heating
View Scheme
79-37-8

oxalyl dichloride

55701-05-8

3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylic acid

52314-67-7

permethric acid chloride

ethyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate ester

ethyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate ester

55701-05-8

3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylic acid

52314-67-7

permethric acid chloride

Conditions
ConditionsYield
With potassium hydroxide; thionyl chloride In ethanol; dichloromethane; water; N,N-dimethyl-formamide
59609-49-3

ethyl 3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate

55701-05-8

3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylic acid

52314-67-7

permethric acid chloride

Conditions
ConditionsYield
With potassium hydroxide; thionyl chloride In methanol; benzene
52314-67-7

permethric acid chloride

62-53-3

aniline

N-phenyl-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxamide

Conditions
ConditionsYield
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h;99%
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction;98%
52314-67-7

permethric acid chloride

m-phenoxybenzaldehyde-13C6

permethrin-13C6

Conditions
ConditionsYield
Stage #1: m-phenoxybenzaldehyde-13C6 With sodium tetrahydroborate In d(4)-methanol for 0.0833333h;
Stage #2: permethric acid chloride In d(4)-methanol at 60℃; under 2327.23 Torr; for 0.166667h; Microwave irradiation;
98.1%
52314-67-7

permethric acid chloride

83582-60-9

4-Hydroxy-4-(3-phenoxyphenyl)butyronitril

3-(2,2-Dichloro-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid 3-cyano-1-(3-phenoxy-phenyl)-propyl ester

Conditions
ConditionsYield
With pyridine In toluene at 25℃;98%
773837-37-9

sodium cyanide

52314-67-7

permethric acid chloride

m-phenoxybenzaldehyde-D5

(D5-)alpha-cypermethrin

Conditions
ConditionsYield
In water-d2 at 40℃; under 2068.65 Torr; for 0.133333h; Microwave irradiation;97.4%
52314-67-7

permethric acid chloride

143-33-9

sodium cyanide

3-(Naphthalen-2-yloxy)-benzaldehyde

3-(2,2-Dichloro-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid cyano-[3-(naphthalen-2-yloxy)-phenyl]-methyl ester

Conditions
ConditionsYield
With tetrabutylammomium bromide In water; toluene at 25℃; for 6h;97%
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Specification

The CAS register number of Cyclopropanecarbonylchloride, 3-(2,2-dichloroethenyl)-2,2-dimethyl- is 52314-67-7. It also can be called as 2,2-Dimethyl-3-(2,2-dichloroethenyl)cyclopropanecarbonylchloride and the IUPAC name about this chemical is 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane-1-carbonyl chloride. The molecular formula about this chemical is C8H9Cl3O and the molecular weight is 227.52.

Physical properties about Cyclopropanecarbonylchloride, 3-(2,2-dichloroethenyl)-2,2-dimethyl- are: (1)ACD/LogP: 3.27; (2)ACD/LogD (pH 5.5): 3.27; (3)ACD/LogD (pH 7.4): 3.27; (4)ACD/BCF (pH 5.5): 181.28; (5)ACD/BCF (pH 7.4): 181.28; (6)ACD/KOC (pH 5.5): 1439.24; (7)ACD/KOC (pH 7.4): 1439.24; (8)#H bond acceptors: 1; (9)#Freely Rotating Bonds: 2; (10)Polar Surface Area: 17.07Å2; (11)Index of Refraction: 1.58; (12)Molar Refractivity: 53.23 cm3; (13)Molar Volume: 159.7 cm3; (14) Polarizability: 21.1x10-24cm3; (15)Surface Tension: 47.2 dyne/cm; (16)Enthalpy of Vaporization: 47.93 kJ/mol; (17)Boiling Point: 242.4 °C at 760 mmHg; (18)Vapour Pressure: 0.0341 mmHg at 25°C.

Uses of Cyclopropanecarbonylchloride, 3-(2,2-dichloroethenyl)-2,2-dimethyl-: it can be used to produce 3-(2,2-dichloro-vinyl)-2,2-dimethyl-cyclopropanecarboxylic acid 1-benzo[1,3]dioxol-5-yl-2,2,2-trichloro-ethyl ester with 1-benzo[1,3]dioxol-5-yl-2,2,2-trichloro-ethanol at temperature of 20 ℃. This reaction will need reagent pyridine and solvent benzene with reaction time of 12 hours. The yield is about 73.9%.

You can still convert the following datas into molecular structure:
(1)SMILES: Cl/C(Cl)=C/C1C(C(Cl)=O)C1(C)C
(2)InChI: InChI=1/C8H9Cl3O/c1-8(2)4(3-5(9)10)6(8)7(11)12/h3-4,6H,1-2H3
(3)InChIKey: CHLAOFANYRDCPD-UHFFFAOYAV
(4)Std. InChI: InChI=1S/C8H9Cl3O/c1-8(2)4(3-5(9)10)6(8)7(11)12/h3-4,6H,1-2H3
(5)Std. InChIKey: CHLAOFANYRDCPD-UHFFFAOYSA-N