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| CAS No.: | 52462-29-0 |
|---|---|
| Name: | Dichloro(p-cymene)ruthenium(II) dimer |
| Molecular Structure: | |
|
|
|
| Formula: | C20H28Cl4Ru2 |
| Molecular Weight: | 612.394 |
| Synonyms: | (p-Cymene)ruthenium dichloridedimer;Bis(((h6-4-isopropyltoluene)(chloro)(m-chloro)ruthenium));Bis((dichloro(h6-p-isopropyl(methyl)benzene)ruthenium));Bis((m-chloro)chloro(h6-1-isopropyl-4-methylbenzene)ruthenium);Bis(4-isopropyltoluene)tetrachlorodiruthenium;Bis(dichloro(h6-4-isopropyltoluene)ruthenium);Bis(dichloro(h6-p-isopropyltoluene)ruthenium);Bis(m-chlorochloro(h6-4-cymene)ruthenium); |
| EINECS: | 435-530-5 |
| Melting Point: | 247.0-250.0 °C (dec.)(lit.) |
| Boiling Point: | 173.9oC at 760mmHg |
| Flash Point: | 47.2oC |
| Solubility: | insoluble in water |
| Appearance: | red-orange to red-brown crystals or powder |
| Hazard Symbols: |
 Xn
|
| Risk Codes: | 22-36-52/53 |
| Safety: | 26-61 |
| PSA: | 0.00000 |
| LogP: | 8.99480 |
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(R)-5-isopropyl-2-methylcyclohexa-1,3-diene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In methanol at 140℃; for 0.166667h; Microwave irradiation; | 100% |
| In ethanol at 130℃; for 0.0666667h; Microwave irradiation; | 83% |
| In ethanol for 24h; Reflux; | 76% |
- 99-87-6
4-methylisopropylbenzene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In 2-methoxy-ethanol; water at 120℃; for 4h; Product distribution / selectivity; | 98% |
- 99-83-2
p-mentha-1,5-diene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In ethanol for 17h; Schlenk technique; Reflux; Inert atmosphere; | 98% |
| In ethanol for 4h; Reflux; Inert atmosphere; | 78% |
| In methanol Inert atmosphere; Schlenk technique; Heating; | |
| In ethanol for 12h; Reflux; Inert atmosphere; |
- 99-83-2
p-mentha-1,5-diene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In ethanol for 8h; Reflux; | 96% |
| In methanol for 4h; Schlenk technique; Inert atmosphere; Reflux; | 85% |
- 99-87-6
4-methylisopropylbenzene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| for 15h; Inert atmosphere; Reflux; | 94% |
| In butan-1-ol at 80℃; for 6h; Solvent; Temperature; | 94% |
| In ethanol Reflux; |
- 20759-14-2
ruthenium(III) chloride hydrate
- 99-85-4
crithmene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In ethanol RuCl3*H2O is refluxed in EtOH in presence of the cyclohexadiene under N2 (4 h); ppt. is filtered, a second crop of ppt. is obtained by reducing the filtrate and cooling (-10°C); | 90% |
- 99-87-6
4-methylisopropylbenzene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In ethanol for 24h; Solvent; Inert atmosphere; Reflux; | 90% |
| In ethanol for 24h; Reflux; Inert atmosphere; | 90% |
- 99-86-5
1-methyl-4-isopropyl-1,3-cyclohexadiene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In methanol at 140℃; for 0.00833333h; Inert atmosphere; Microwave irradiation; | 86% |
| In methanol Schlenk technique; Inert atmosphere; Reflux; | |
| In ethanol at 20℃; for 15h; Schlenk technique; |
- 20759-14-2
ruthenium(III) chloride hydrate
- 99-86-5
1-methyl-4-isopropyl-1,3-cyclohexadiene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In ethanol refluxing for 4 h; crystn. on cooling, filtration, washing (cold MeOH), drying (vac.); second crop on crystn. of filtrate after evapn.; elem. anal.; | 77% |
- 99-83-2
p-mentha-1,5-diene
- 52462-29-0
[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2
| Conditions | Yield |
|---|---|
| In ethanol for 4h; Sonication; Reflux; | 76% |
| In ethanol at 79℃; for 4h; Heating / reflux; | 35% |
| Inert atmosphere; Schlenk technique; | |
| Inert atmosphere; Schlenk technique; |
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Specification
The Ruthenium, di-m-chlorodichlorobis[(1,2,3,4,5,6-h)-1-methyl-4-(1-methylethyl)benzene]di-, with CAS registry number 52462-29-0, belongs to the following product categories: (1)Cyclic compounds; (2)Catalysts for Organic Synthesis; (3)Classes of Metal Compounds; (4)Homogeneous Catalysts; (5)Metal Complexes; (6)Ru (Ruthenium) Compounds; (7)Synthetic Organic Chemistry; (8)Transition Metal Compounds; (9)Ru Catalysts; (10)Catalysis and Inorganic Chemistry; (11)Ruthenium. It has the systematic name of ruthenium(2+) chloride - 1-methyl-4-(propan-2-yl)benzene (1:2:1). This chemical is a kind of red-orange to red-brown crystals or powder.
When you are using this chemical, please be cautious about it as the following:
The Ruthenium, di-m-chlorodichlorobis[(1,2,3,4,5,6-h)-1-methyl-4-(1-methylethyl)benzene]di- is harmful if swallowed. And it irritates to eyes. This chemical is also harmful to aquatic organisms, may cause long-term adverse effects in the aquatic environment, so avoid release it to the environment. Refer to special instructions / safety data sheets. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
You can still convert the following datas into molecular structure:
(1)SMILES: Cc1ccc(cc1)C(C)C.Cc1ccc(cc1)C(C)C.[Cl-].[Cl-].[Cl-].[Cl-].[Ru+2].[Ru+2]
(2)InChI: InChI=1/2C10H14.4ClH.2Ru/c2*1-8(2)10-6-4-9(3)5-7-10;;;;;;/h2*4-8H,1-3H3;4*1H;;/q;;;;;;2*+2/p-4
(3)InChIKey: LAXRNWSASWOFOT-XBHQNQODAM
(4)Std. InChI: InChI=1S/2C10H14.4ClH.2Ru/c2*1-8(2)10-6-4-9(3)5-7-10;;;;;;/h2*4-8H,1-3H3;4*1H;;/q;;;;;;2*+2/p-4
(5)Std. InChIKey: LAXRNWSASWOFOT-UHFFFAOYSA-J