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5467-56-1

Basic Information
CAS No.: 5467-56-1
Name: 1-[4-(PENTYLOXY)PHENYL]ETHANONE
Article Data: 19
Molecular Structure:
Molecular Structure of 5467-56-1 (1-[4-(PENTYLOXY)PHENYL]ETHANONE)
Formula: C13H18O2
Molecular Weight: 206.285
Synonyms: 4-pentyloxyacetophenone;4-pentoxyacetophenone;4-n-pentyloxyacetophenone;4-amyloxyacetophenone;
Density: 0.977g/cm3
Boiling Point: 319.9°Cat760mmHg
Flash Point: 134.4°C
PSA: 26.30000
LogP: 3.45820
Synthetic route
110-53-2

1-Bromopentane

99-93-4

4-Hydroxyacetophenone

5467-56-1

4-pentyloxyacetophenone

Conditions
ConditionsYield
With potassium carbonate In water; ethyl acetate; acetone100%
With potassium carbonate In N,N-dimethyl-formamide for 16h; Reflux;92%
With potassium carbonate; potassium iodide In acetone Inert atmosphere; Reflux;78%
2050-04-6

(pentyloxy)benzene

108-24-7

acetic anhydride

5467-56-1

4-pentyloxyacetophenone

Conditions
ConditionsYield
With zinc(II) chloride
108-95-2

phenol

5467-56-1

4-pentyloxyacetophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: AlCl3; CS2
2: methanol. NaOH
View Scheme
13329-40-3

4-Iodoacetophenone

5467-56-1

4-pentyloxyacetophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: copper(l) iodide; 8-Hydroxyquinoline-N-oxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere
1.2: 28 h / 100 °C / Inert atmosphere
2.1: cesiumhydroxide monohydrate; tetra-(n-butyl)ammonium iodide / water; dimethyl sulfoxide / 12 h / 100 °C / Inert atmosphere
View Scheme
99-90-1

para-bromoacetophenone

5467-56-1

4-pentyloxyacetophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: copper(l) iodide; 8-Hydroxyquinoline-N-oxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere
1.2: 24 h / 110 °C / Inert atmosphere
2.1: cesiumhydroxide monohydrate; tetra-(n-butyl)ammonium iodide / water; dimethyl sulfoxide / 12 h / 100 °C / Inert atmosphere
View Scheme
1-Chloropentane

1-Chloropentane

99-93-4

4-Hydroxyacetophenone

5467-56-1

4-pentyloxyacetophenone

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 60 - 80℃; for 4h; Inert atmosphere;
99-93-4

4-Hydroxyacetophenone

pentyl halide

pentyl halide

5467-56-1

4-pentyloxyacetophenone

Conditions
ConditionsYield
With potassium carbonate In acetone at 20℃;
5467-56-1

4-pentyloxyacetophenone

(R)-1-(4-Pentyloxy-phenyl)-ethanol

Conditions
ConditionsYield
With Trimethyl borate; (S)-diphenylprolinol; dimethylsulfide borane complex In tetrahydrofuran; toluene at 25 - 30℃;99%
5467-56-1

4-pentyloxyacetophenone

177715-63-8

4-pentyloxy-benzoic acid ethyl ester

107265-33-8

1,3-Di-(p-n-pentyloxyphenyl)propane-1,3-dione

Conditions
ConditionsYield
With sodium hydride90%
With sodium hydride
5467-56-1

4-pentyloxyacetophenone

1571-08-0

methyl 4-formylbenzoate

C22H24O4

Conditions
ConditionsYield
With caesium carbonate In ethanol; water at 50℃; for 5h;84.6%
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  • 5467-56-1

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    We are Hebei minshang biotechnology co. LTD., mainly deal in pharmaceutical intermediates and various chemicals. We are manufacturers and have our own factory. Products & Usage Ph

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