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CAS No.: | 5467-56-1 |
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Name: | 1-[4-(PENTYLOXY)PHENYL]ETHANONE |
Article Data: | 19 |
Molecular Structure: | |
Formula: | C13H18O2 |
Molecular Weight: | 206.285 |
Synonyms: | 4-pentyloxyacetophenone;4-pentoxyacetophenone;4-n-pentyloxyacetophenone;4-amyloxyacetophenone; |
Density: | 0.977g/cm3 |
Boiling Point: | 319.9°Cat760mmHg |
Flash Point: | 134.4°C |
PSA: | 26.30000 |
LogP: | 3.45820 |
Conditions | Yield |
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With potassium carbonate In water; ethyl acetate; acetone | 100% |
With potassium carbonate In N,N-dimethyl-formamide for 16h; Reflux; | 92% |
With potassium carbonate; potassium iodide In acetone Inert atmosphere; Reflux; | 78% |
Conditions | Yield |
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With zinc(II) chloride |
Conditions | Yield |
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Multi-step reaction with 2 steps 1: AlCl3; CS2 2: methanol. NaOH View Scheme |
4-Iodoacetophenone
4-pentyloxyacetophenone
Conditions | Yield |
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Multi-step reaction with 2 steps 1.1: copper(l) iodide; 8-Hydroxyquinoline-N-oxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere 1.2: 28 h / 100 °C / Inert atmosphere 2.1: cesiumhydroxide monohydrate; tetra-(n-butyl)ammonium iodide / water; dimethyl sulfoxide / 12 h / 100 °C / Inert atmosphere View Scheme |
Conditions | Yield |
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Multi-step reaction with 2 steps 1.1: copper(l) iodide; 8-Hydroxyquinoline-N-oxide / dimethyl sulfoxide / 0.17 h / 20 °C / Inert atmosphere 1.2: 24 h / 110 °C / Inert atmosphere 2.1: cesiumhydroxide monohydrate; tetra-(n-butyl)ammonium iodide / water; dimethyl sulfoxide / 12 h / 100 °C / Inert atmosphere View Scheme |
Conditions | Yield |
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With potassium carbonate In N,N-dimethyl-formamide at 60 - 80℃; for 4h; Inert atmosphere; |
Conditions | Yield |
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With potassium carbonate In acetone at 20℃; |
4-pentyloxyacetophenone
Conditions | Yield |
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With Trimethyl borate; (S)-diphenylprolinol; dimethylsulfide borane complex In tetrahydrofuran; toluene at 25 - 30℃; | 99% |
4-pentyloxyacetophenone
4-pentyloxy-benzoic acid ethyl ester
1,3-Di-(p-n-pentyloxyphenyl)propane-1,3-dione
Conditions | Yield |
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With sodium hydride | 90% |
With sodium hydride |
Conditions | Yield |
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With caesium carbonate In ethanol; water at 50℃; for 5h; | 84.6% |