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99-93-4

Basic Information
CAS No.: 99-93-4
Name: 4'-Hydroxyacetophenone
Article Data: 519
Cas Database
Molecular Structure:
Molecular Structure of 99-93-4 (4'-Hydroxyacetophenone)
Formula: C8H8O2
Molecular Weight: 136.15
Synonyms: Methyl-p-hydroxyphenyl ketone;Phenol, p-acetyl-;USAF KF-15;Methyl p-hydroxyphenyl ketone;p-Oxyacetophenone;Acetophenone, p-hydroxy-;Ethanone, 1- (4-hydroxyphenyl)-;p-Hydroxyphenyl methyl ketone;Ethanone,1-(4-hydroxyphenyl)-;Piceol;Acetophenone, 4-hydroxy- (8CI);p-Hydroxacetophenone;4-Hydroxyacetophenone;4-Acetylphenol;1-(4-Hydroxyphenyl)ethanone;1-(4-Hydroxy-phenyl)-ethanone;4-Hydroksyacetofenol [Polish];p-Acetylphenol;D-Hydroxyacetophehone;Acetophenone, 4-hydroxy-;4'-Hydroxyacetophenone (p-Hydroxyacetophenone);4-Hydroxy acteophenone;p-hydroxyphenethyl alcohol;p-Hydroxy Acetophenone;Para Hydroxy Acetophenone (PHAP);4'-Hydroxyacetophenone (PHAP);4'-hydroxyacetophenone;1-(4-hydroxyphenyl)ethanone;;P-Hydroxyacetophenone;
EINECS: 202-802-8
Density: 1.14 g/cm3
Melting Point: 132-135 °C(lit.)
Boiling Point: 313 °C at 760 mmHg
Flash Point: 121.2 °C
Solubility: methanol: 0.1 g/mL, clear
Appearance: almost white to beige crystalline powder
Hazard Symbols: HarmfulXn,IrritantXi
Risk Codes: 36/37/38-22
Safety: 26-36/37-37/39-24/25-22-36
Transport Information: N/A
PSA: 37.30000
LogP: 1.59480
Synthetic route
149683-53-4

4-(tert-butyldimethylsilyloxy)acetophenone

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With water; potassium carbonate In ethanol at 75℃; for 16h;100%
With water; 1,8-diazabicyclo[5.4.0]undec-7-ene In dimethyl sulfoxide at 20℃; for 0.0166667h; chemoselective reaction;97%
With dichloro bis(acetonitrile) palladium(II) In water; acetone at 75℃; for 16h;96%
2079-53-0

1-(4-(allyloxy)phenyl)ethanone

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With calcium hydride; diphenyldisulfane In 1-methyl-pyrrolidin-2-one at 220℃; for 0.5h;100%
With aniline; (ϖ-allyl)palladium triflate based catalyst at 30℃; for 1h;99%
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 20℃; for 4h; Inert atmosphere;93%
155853-28-4

2-methyl-2-(4-hydroxyphenyl)-1,3-dithiane

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With dihydrogen peroxide; tantalum pentachloride; sodium iodide In water; ethyl acetate at 20℃; for 1h;100%
With dihydrogen peroxide; tantalum pentachloride; sodium iodide In water; ethyl acetate at 20℃; for 1h;100%
With iron(III)-acetylacetonate; dihydrogen peroxide; sodium iodide In water; ethyl acetate at 20℃; for 0.3h;90%
With Amberlite IR-120; palladium on activated charcoal In methanol for 8h; Heating;88%
With β‐cyclodextrin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetone at 20℃; for 2.5h;85%
13329-40-3

4-Iodoacetophenone

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With sodium hydroxide; copper(l) iodide; L-proline In water at 20 - 300℃; microwave irradiation;100%
Stage #1: 4-Iodoacetophenone With copper(l) iodide; tetra(n-butyl)ammonium hydroxide In water at 60℃; for 24h; Inert atmosphere; Sealed tube;
Stage #2: With hydrogenchloride In water; ethyl acetate at 20℃; for 2h; Inert atmosphere; chemoselective reaction;
96%
With copper(l) iodide; potassium hydroxide In water at 100℃; Inert atmosphere;96%

C20H18O3

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In aq. phosphate buffer; dichloromethane at 0 - 20℃; for 22.5h; pH=7;100%
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In aq. phosphate buffer; dichloromethane at 0 - 20℃; for 22.5h;100%
64101-66-2

4’-benzenesulfoxyacetophenone

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With potassium hydroxide In toluene; tert-butyl alcohol at 100℃; for 0.5h; Inert atmosphere;100%
22107-31-9

4-hydroxyacetophenone semicarbazone

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With hydrogenchloride; Tonsil In ethyl acetate for 1.5h; Heating;99.5%
With copper dichloride In acetonitrile for 0.5h; Heating;98%
With ammonium persulfate; montmorrilonite K10 clay In solid for 1h; Irradiation; ultrasound irradiation;94%
93453-79-3

1-(4-hydroxyphenyl)ethanol

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With silica-supported Jones reagent In dichloromethane for 0.00269444h;99.3%
With bismuth (III) nitrate pentahydrate; cellulose supported copper(0); oxygen In acetonitrile at 60℃; for 0.5h;96%
With N-Bromosuccinimide; β‐cyclodextrin In methanol; water; acetone at 20℃; for 10h;95%
75-36-5

acetyl chloride

108-95-2

phenol

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With trifluorormethanesulfonic acid at 0 - 20℃; for 1h; Friedel-Crafts acylation; regiospecific reaction;99%
With iron(III) chloride; lithium chloride In 1,2-dichloro-benzene at 70℃; for 5h; Reagent/catalyst; Temperature;90%
Stage #1: phenol With aluminum (III) chloride In dichloromethane for 1h; Friedel Crafts acylation;
Stage #2: acetyl chloride In dichloromethane for 14h; Friedel Crafts acylation;
73.5%
54696-05-8

4'-benzyloxy-acetophenone

99-93-4

4-Hydroxyacetophenone

Conditions
ConditionsYield
With cyclohexa-1,4-diene; polymer-CH2NMe3Cl; palladium In ethanol at 55℃; for 1.5h;99%
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 25℃; for 1h; Inert atmosphere;99%
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 50℃; for 5h; Inert atmosphere;99%
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    4 '- hydroxyacetophenone CAS No.: 99-93-4 Molecular formula: C8H8O2 Molecular weight: 136.15 Melting point 132-135 ° C (lit.) Boiling point 147-148 ° c3mmhg (lit.) Density 1.109fema4330|4-hydroxyacetophenone Refractive index 1.557

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    1.Prompt Goods; 2.Flexible payment terms; 3.Documents & Certificate support. Name:1-(4-hydroxyphenyl)-ethanon Molecular Structure: Formula: C8H8O2 Molecular Weight : 136.15 Synonyms: 1-(4-hydroxyphenyl)-ethanon;4’-hydroxy-acetopheno

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Consensus Reports

Reported in EPA TSCA Inventory.

Specification

4'-Hydroxyacetophenone, its CAS NO. is 99-93-4, and the synonyms are 1-(4-Hydroxyphenyl)ethanone; 4-Acetylphenol; 4-Hydroksyacetofenol; Acetophenone, 4'-hydroxy-; Acetophenone, p-hydroxy-; Methyl p-hydroxyphenyl ketone; Phenol, p-acetyl-; Piceol; p-Acetylphenol; p-Hydroxyacetophenone; p-Hydroxyphenyl methyl ketone; p-Oxyacetophenone. It is a clear liquid or crystals; melting point 19 - 20 C; boiling point 202 C; very slightly soluble in water. It is used as a polymerization catalyst for the manufacture of olefins. It is used as an intermediate for pharmaceuticals, agrochemicals and other organic compounds.

Physical properties about 4'-Hydroxyacetophenone are: (1)ACD/LogP: 1.399; (2)ACD/LogD (pH 5.5): 1.40; (3)ACD/LogD (pH 7.4): 1.32; (4)ACD/BCF (pH 5.5): 6.80; (5)ACD/BCF (pH 7.4): 5.72; (6)ACD/KOC (pH 5.5): 137.14; (7)ACD/KOC (pH 7.4): 115.44; (8)#H bond acceptors: 2; (9)#H bond donors: 1; (10)#Freely Rotating Bonds: 2; (11)Index of Refraction: 1.552; (12)Molar Refractivity: 38.162 cm3; (13)Molar Volume: 119.394 cm3; (14)Polarizability: 15.129 10-24cm3; (15)Surface Tension: 43.9830017089844 dyne/cm; (16)Density: 1.14 g/cm3; (17)Flash Point: 121.232 °C; (18)Enthalpy of Vaporization: 57.61 kJ/mol; (19)Boiling Point: 312.975 °C at 760 mmHg

When you are using this chemical, please be cautious about it as the following:|
1. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice;
2. Wear suitable protective clothing and gloves;
3. Wear suitable gloves and eye/face protection;
4. Avoid contact with skin and eyes;
5. Do not breathe dust;
6. Wear suitable protective clothing;

You can still convert the following datas into molecular structure:
(1)InChI=1S/C8H8O2/c1-6(9)7-2-4-8(10)5-3-7/h2-5,10H,1H3;
(2)InChIKey=TXFPEBPIARQUIG-UHFFFAOYSA-N;
(3)Smilesc1(C(C)=O)ccc(O)cc1;

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
mouse LD50 intraperitoneal 200mg/kg (200mg/kg)   National Technical Information Service. Vol. AD277-689,
mouse LD50 oral 1500mg/kg (1500mg/kg)   Medicina Experimentalis. Vol. 11, Pg. 137, 1964.