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| CAS No.: | 55-81-2 |
|---|---|
| Name: | 4-Methoxyphenethylamine |
| Article Data: | 85 |
| Molecular Structure: | |
|
|
|
| Formula: | C9H13NO |
| Molecular Weight: | 151.208 |
| Synonyms: | Phenethylamine,p-methoxy- (6CI,8CI);2-(4-Methoxyphenyl)ethanamine;2-(4-Methoxyphenyl)ethylamine;2-(p-Methoxyphenyl)ethylamine;4-Methoxy-b-phenethylamine;4-Methoxy-b-phenylethylamine;4-Methoxybenzeneethanamine;4-Methoxyphenethylamine;4-Methoxyphenylethylamine;Homoanisylamine;NSC 43687;O-Methyltyramine;Tyramine, O-methyl-;p-Methoxyphenethylamine; |
| EINECS: | 200-245-5 |
| Density: | 1.008 g/cm3 |
| Melting Point: | 249-251°C |
| Boiling Point: | 255.2 °C at 760 mmHg |
| Flash Point: | 105.3 °C |
| Appearance: | clear colorless to slightly yellow liquid |
| Hazard Symbols: |
 C
|
| Risk Codes: | 34 |
| Safety: | 26-36/37/39-45 |
| Transport Information: | UN 2735 |
| PSA: | 35.25000 |
| LogP: | 1.89670 |
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- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
- 198756-72-8
benzyl 4-methoxyphenethylcarbamate
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 1h; | 100% |
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride; lithium aluminium tetrahydride In diethyl ether at 0 - 20℃; | 96% |
| With lithium borohydride; diisopropopylaminoborane In tetrahydrofuran for 18h; Reflux; | 94% |
| With [Ru(H)(BH4)(CO)(PPh3)(3-(di-tert-butylphosphino)-N-((1-methyl-1H-imidazol-2 yl)methyl)propylamine)]; hydrogen In isopropyl alcohol at 70℃; for 3h; Inert atmosphere; Autoclave; | 94% |
- 31236-71-2
lysichitalexin
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| With samarium diiodide; water; isopropylamine In tetrahydrofuran | 96% |
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| With potassium carbonate; thiophenol In acetonitrile at 50℃; | 95% |
- 1258181-22-4
C12H14Cl3NO3
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| Stage #1: C12H14Cl3NO3 With chloro-trimethyl-silane; mischmetal In tetrahydrofuran for 2h; Inert atmosphere; Reflux; Stage #2: With water In tetrahydrofuran for 0.0833333h; Alkaline conditions; | 87% |
| Conditions | Yield |
|---|---|
| With hydrogenchloride; hydrogen; acetic acid; palladium on activated charcoal for 1h; | 71% |
| With hydrogen; carbon palladium at 85℃; under 37503 Torr; | 70% |
| (catalytic hydrogenation); |
- 91247-71-1
2-4-methoxyphenylethylcarbamic acid methyl ester
A
- 22246-04-4
7-methoxy-3,4-dihydro-2H-isoquinolin-1-one
B
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| With PPA at 145℃; for 0.166667h; | A 59% B 30% |
- 25413-27-8
3-(4-methoxy-phenyl)propionamide
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| With sodium hydroxide; bromine In water at 70 - 80℃; for 0.25h; | 53% |
| With sodium hypobromide | |
| With alkaline sodium hypochlorite |
- 141666-92-4
4-methyl-N-[2-(4-methoxyphenyl)ethyl]benzenesulfonamide
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| With titanium tetrachloride In tetrahydrofuran for 2.5h; Heating; | 40% |
- 3179-10-0, 5576-97-6
(E)-1-methoxy-4-(2-nitrovinyl)benzene
- 55-81-2
4-Methoxyphenethylamine
| Conditions | Yield |
|---|---|
| With samarium diiodide; water; isopropylamine In tetrahydrofuran | 36% |
| With sulfuric acid; palladium; acetic acid Hydrogenation; | |
| bei der elektrochemischen Reduktion; | |
| With lithium aluminium tetrahydride |
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Chemistry
The Molecular Weight of p-METHOXYPHENETHYLAMINE(55-81-2):151.21
The Molecular Structure of p-METHOXYPHENETHYLAMINE(55-81-2) is:
Density:1.008 g/cm3
Melting point:249-251°C
Boiling point:255.2 °C at 760 mmHg
Flash point:105.3 °C
Index of Refraction:1.525
Molar Refractivity:46.01 cm3
Molar Volume:149.9 cm3
Polarizability:18.24 10-24cm3
Surface Tension:36.9 dyne/cm
Enthalpy of Vaporization:49.27 kJ/mol
Vapour Pressure:0.0165 mmHg at 25°C
Appearance:clear colorless to slightly yellow liquid
IUPAC Name:2-(4-methoxyphenyl)ethanamine
Synonyms:4-Methoxy-2-phenethylamine;4-methoxy-benzeneethanamin;2-(4-Methoxyphenyl)ethanamine;4-Methoxybenzeneethanamine;4-Methoxy-beta-phenylethylamine;Homoanisylamine;o-methyltyramine;Phenethylamine, p-methoxy-
Uses
Toxicity Data With Reference
| 1. | ipr-mus LD50:100 mg/kg | NTIS** National Technical Information Service. (Springfield, VA 22161) (Formerly U.S. Clearinghouse for Scientific and Technical Information) No. AD277-689 . |
Consensus Reports
Safety Profile
Poison by intraperitoneal route. When heated to decomposition it emits toxic fumes of NOx.
Hazard Codes:C,T
C:Corrosive
T:Toxic
Risk Statements
R34:Causes burns.
Safety Statements
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S27:Take off immediately all contaminated clothing .
RIDADR:
UN 2735 8/PG 3
WGK Germany:3
RTECS:SH7875000
F:10-23
Hazard Note:Toxic/Corrosive
HS Code:29222900