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| CAS No.: | 5874-57-7 |
|---|---|
| Name: | D-Serine methyl ester hydrochloride |
| Article Data: | 40 |
| Molecular Structure: | |
|
|
|
| Formula: | C4H10ClNO3 |
| Molecular Weight: | 155.581 |
| Synonyms: | D-Serine,methyl ester, hydrochloride (9CI);Serine, methyl ester, hydrochloride, D-(8CI);(R)-2-Amino-3-hydroxypropionic acid methyl ester hydrochloride;(R)-Methyl 2-amino-3-hydroxypropanoate hydrochloride;Methyl D-serinatehydrochloride;H-D-Ser-OMe·HCl; |
| EINECS: | 611-745-1 |
| Density: | 1.62 g/cm3 |
| Melting Point: | 163-166 °C(lit.) |
| Boiling Point: | 234.7 °C at 760 mmHg |
| Flash Point: | 95.8 °C |
| Appearance: | White Solid |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 26-36 |
| PSA: | 72.55000 |
| LogP: | -0.01870 |
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| Conditions | Yield |
|---|---|
| With acetyl chloride for 2.5h; Heating; | 100% |
| Stage #1: methanol; D-Serine With acetyl chloride at 0℃; Stage #2: In methanol for 3h; Heating; | 100% |
| With hydrogenchloride In water at 55℃; | 100% |
- 67-56-1
methanol
- 312-84-5
D-Serine
- 75-36-5
acetyl chloride
- 5874-57-7
R-(-)-serine methyl ester hydrochloride
| Conditions | Yield |
|---|---|
| Stage #1: methanol; acetyl chloride for 0.0833333h; Cooling with ice; Stage #2: D-Serine for 2h; Reflux; | 97% |
| Conditions | Yield |
|---|---|
| In methanol for 15.5h; Reflux; | 91% |
- 5874-57-7
R-(-)-serine methyl ester hydrochloride
- 501-53-1
benzyl chloroformate
- 93204-36-5
(R)-methyl 2-(((benzyloxy)carbonyl)amino)-3-hydroxypropanoate
| Conditions | Yield |
|---|---|
| With sodium hydrogencarbonate In water; ethyl acetate at 20℃; Cooling with ice; | 100% |
| With sodium hydrogencarbonate In tetrahydrofuran; water at 20℃; for 12h; | 91% |
| With sodium hydrogencarbonate | 80% |
- 24424-99-5
di-tert-butyl dicarbonate
- 5874-57-7
R-(-)-serine methyl ester hydrochloride
- 95715-85-8
2-(tert-butoxycarbonylamino)-3-hydroxypropionic acid methyl ester
| Conditions | Yield |
|---|---|
| Stage #1: R-(-)-serine methyl ester hydrochloride With triethylamine In dichloromethane for 0.5h; Cooling with ice; Stage #2: di-tert-butyl dicarbonate In dichloromethane at 20℃; for 16.5h; Cooling with ice; | 100% |
| With triethylamine In tetrahydrofuran at 0 - 140℃; for 0.333333h; Inert atmosphere; Microwave irradiation; | 99% |
| With triethylamine In tetrahydrofuran at 0 - 50℃; for 17h; Inert atmosphere; | 97% |
- 32315-10-9
bis(trichloromethyl) carbonate
- 5874-57-7
R-(-)-serine methyl ester hydrochloride
- 144542-43-8
(R)-2-oxo-oxazolidine-4-carboxylic acid methyl ester
| Conditions | Yield |
|---|---|
| In tetrahydrofuran for 4h; Heating; | 100% |
| In tetrahydrofuran for 4h; Reflux; Inert atmosphere; | 98% |
| In tetrahydrofuran at 0 - 80℃; for 2h; | 75% |
- 76-83-5
trityl chloride
- 5874-57-7
R-(-)-serine methyl ester hydrochloride
- 116457-91-1
(2R)-3-hydroxy-2-(tritylamino)propanoic acid methyl ester
| Conditions | Yield |
|---|---|
| With triethylamine In chloroform at 0℃; for 1h; | 99% |
| With triethylamine In 1,2-dichloro-ethane at 50℃; for 12h; | 97% |
| With triethylamine In dichloromethane at 0 - 25℃; for 16h; | 95% |
- 5874-57-7
R-(-)-serine methyl ester hydrochloride
- 100-52-7
benzaldehyde
- 123639-56-5, 131110-76-4, 144001-42-3
methyl (2R)-2-(benzylamino)-3-hydroxypropanoate
| Conditions | Yield |
|---|---|
| Stage #1: R-(-)-serine methyl ester hydrochloride; benzaldehyde With magnesium sulfate; triethylamine In dichloromethane at 20℃; for 24h; Stage #2: With sodium tetrahydroborate In methanol at 0℃; for 3h; Further stages.; | 99% |
| Stage #1: R-(-)-serine methyl ester hydrochloride With triethylamine In methanol at 0℃; for 0.25h; Inert atmosphere; Stage #2: benzaldehyde In methanol at 20℃; for 2h; Inert atmosphere; Stage #3: With sodium tetrahydroborate In methanol at 0℃; Inert atmosphere; | 99% |
| Stage #1: R-(-)-serine methyl ester hydrochloride; benzaldehyde With triethylamine Stage #2: With sodium tetrahydroborate | 79% |
- 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
- 5874-57-7
R-(-)-serine methyl ester hydrochloride
- 874817-14-8
2-(9H-fluoren-9-ylmethoxycarbonylamino)-3-hydroxypropionic acid methyl ester
| Conditions | Yield |
|---|---|
| With sodium hydrogencarbonate In 1,4-dioxane; water cooling; | 99% |
| With sodium hydrogencarbonate In 1,4-dioxane; water at 0 - 20℃; for 4.33333h; | 95% |
| Conditions | Yield |
|---|---|
| With triethylamine In chloroform at 0 - 20℃; Inert atmosphere; | 99% |
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Chemistry
Molecular Structure of D-Serine methyl ester hydrochloride (CAS NO.5874-57-7):
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The Molecular formula of D-Serine methyl ester hydrochloride (CAS NO.5874-57-7): C4H10ClNO3
The Molecular Weight of D-Serine methyl ester hydrochloride (CAS NO.5874-57-7): 155.58
IUPAC Name: (E)-2-cyano-3-(1-phenyl-3-thiophen-2-ylpyrazol-4-yl)prop-2-enamide
H bond acceptors: 4
H bond donors: 3
Freely Rotating Bonds: 5
Polar Surface Area: 38.77Å2
Melting point: 163-166 °C(lit.)
Boiling Point: 234.7 °C at 760 mmHg
Flash Point: 95.8 °C
Enthalpy of Vaporization: 54.8 kJ/mol
Vapour Pressure: 0.00953 mmHg at 25°C
Appearance: White Solid
Storage temp: -15°C
Product Categories: Amino Acids series; Amino Acids; Amino Acids and Derivatives; All Aliphatics; Amino hydrochloride; Aliphatics; Amino Acids & Derivatives; Amino Acid Derivatives; Peptide Synthesis; Serine
Safety Profile
The Hazard Codes of D-Serine methyl ester hydrochloride (CAS NO.5874-57-7): 
Xi
The Risk Statements information of D-Serine methyl ester hydrochloride (CAS NO.5874-57-7):
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of D-Serine methyl ester hydrochloride (CAS NO.5874-57-7):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
36: Wear suitable protective clothing
WGK Germany: 3
Specification
D-Serine methyl ester hydrochloride , with CAS number of 5874-57-7, can be called (R)-2-Amino-3-hydroxypropionic acid methyl ester hydrochloride ; (R)-Methyl 2-amino-3-hydroxypropanoate hydrochloride ; Methyl D-serinatehydrochloride ; DL-Serine, methyl ester, hydrochloride ; L-Serine, methyl ester, hydrochloride ; L-serine, methyl ester, hydrochloride (1:1) ; Methyl L-serinate hydrochloride (1:1) . It is a white solid.