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Basic Information
| CAS No.: | 608-31-1 |
|---|---|
| Name: | 2,6-Dichloroaniline |
| Article Data: | 39 |
| Molecular Structure: | |
|
|
|
| Formula: | C6H5Cl2N |
| Molecular Weight: | 162.018 |
| Synonyms: | Aniline,2,6-dichloro- (7CI,8CI);2,6-Dichlorobenzenamine;2,6-Dichlorophenylamine; |
| EINECS: | 210-160-5 |
| Density: | 1.401 g/cm3 |
| Melting Point: | 36-38 °C(lit.) |
| Boiling Point: | 219.9 °C at 760 mmHg |
| Flash Point: | 86.8 °C |
| Solubility: | 1.6 g/L (20 °C) in water |
| Appearance: | white to brown crystalline solid |
| Hazard Symbols: |
 T,  N,  Xi
|
| Risk Codes: | 23/24/25-33-50/53 |
| Safety: | 28-36/37-45-60-61-28A |
| Transport Information: | UN 3442 6.1/PG 2 |
| PSA: | 26.02000 |
| LogP: | 3.15680 |
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Synthetic route
- 22134-75-4
4-amino-3,5-dichloro-benzenesulfonamide
- 608-31-1
2,6-Dichloroaniline
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid at 180℃; | 96.2% |
Conditions
| Conditions | Yield |
|---|---|
| With ammonium formate at 20℃; for 0.75h; Reduction; | 91% |
| With hydrogenchloride; tin | |
| With hydrogen; silver; silica gel In ethanol at 140℃; under 15001.2 Torr; for 3h; | 100 % Chromat. |
Conditions
| Conditions | Yield |
|---|---|
| With methanol; gold; hydrogen; caesium carbonate at 100℃; under 3800.26 Torr; for 72h; | 91% |
| With hydrogen bromide; acetic acid; aniline for 24h; Heating; | 86% |
| With hydrogen bromide; acetic acid; aniline Reflux; | 80% |
- 56961-25-2
4-amino-3,5-dichlorobenzoic acid
- 608-31-1
2,6-Dichloroaniline
Conditions
| Conditions | Yield |
|---|---|
| With copper(I) oxide In quinoline at 220℃; for 6h; Autoclave; | 85% |
| In water | 80% |
- 10286-88-1
N-(2,6-dichlorophenyl)benzamide
- 608-31-1
2,6-Dichloroaniline
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid for 3h; Heating; | 68% |
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate; potassium iodide; Chloroacetamide In N,N-dimethyl-formamide at 90 - 150℃; for 4h; Reagent/catalyst; Smiles Aromatic Rearrangement; | 65% |
Conditions
| Conditions | Yield |
|---|---|
| With chlorine In chlorobenzene at 15℃; for 6h; Solvent; Reagent/catalyst; Temperature; | A 60% B 35% |
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride; potassium permanganate In acetonitrile at 60℃; | A 19% B 29% |
Conditions
| Conditions | Yield |
|---|---|
| With carbon dioxide; water; chlorine Behandeln des Reaktionsprodukts mit 98 prozentiger Schwefelsaeure und Dampf bei 180grad; |
- 56700-68-6
tert-butyl (2,6-dichlorophenyl)carbamate
- 608-31-1
2,6-Dichloroaniline
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In ethanol |
Raw Materials
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2,6-Dichloroaniline
Chemistry
Molecular Formula:C6H5Cl2N
Molar mass:162.0166 g/mol
Structure of 2,6-Dichloroaniline(608-31-1):
Synonyms of 2,6-Dichloroaniline(608-31-1):2,6-dichlorobenzenamine;2,6-Dichloranilin;2,6-DICHLOROANILINE;Benzenamine, 2,6-dichloro-
Density:1.401 g/cm3
Flash Point:118 °C
Boiling Point:228°C
Index of Refraction:1.613
Vapour Pressure: 0.116 mmHg at 25°C
Melting point:35-39°C
Water solubility: 1.6 g/L (20 °C)
Molar mass:162.0166 g/mol
Structure of 2,6-Dichloroaniline(608-31-1):
Synonyms of 2,6-Dichloroaniline(608-31-1):2,6-dichlorobenzenamine;2,6-Dichloranilin;2,6-DICHLOROANILINE;Benzenamine, 2,6-dichloro-
Density:1.401 g/cm3
Flash Point:118 °C
Boiling Point:228°C
Index of Refraction:1.613
Vapour Pressure: 0.116 mmHg at 25°C
Melting point:35-39°C
Water solubility: 1.6 g/L (20 °C)
Uses
2,6-Dichloroaniline(608-31-1) can be used in the pharmaceutical industry for the synthesis of antibacterial agents of lomefloxacin, Lee uric acid and clonidine.
2,6-Dichloroaniline(608-31-1) also can be used in the pesticide industry for the synthesis of herbicides and fungicides.
2,6-Dichloroaniline(608-31-1) also can be used in the pesticide industry for the synthesis of herbicides and fungicides.
Production
1. the right-amino benzene sulfonamide as the raw , chloride by concentrated hydrochloric acid, sulfuric acid hydrolysis and then derived .
2. For amino acid ester method: by chlorination, the water decarboxylation derived.
3. For amino acid method.
Toxicity Data With Reference
Carcinogenicity:2,6-Dichloroaniline(608-31-1)- Not listed as a carcinogen by IARC, NTP,ACGIH, or CA Prop 65.
Other: See actual entry in RTECS for complete information.
Safety Profile
Hazard Codes:T
,N
,Xi
Risk Statements:
23: Toxic by inhalation
24: Toxic in contact with skin
25: Toxic if swallowed
30: Can become highly flammable in use
50: Very Toxic to aquatic organisms
53: May cause long-term adverse effects in the aquatic environment
Safety Statements:
28: After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer)
36: Wear suitable protective clothing
37: Wear suitable gloves
45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
60: This material and/or its container must be disposed of as hazardous waste
61: Avoid release to the environment. Refer to special instructions safety data sheet
,N,XiRisk Statements:
23: Toxic by inhalation
24: Toxic in contact with skin
25: Toxic if swallowed
30: Can become highly flammable in use
50: Very Toxic to aquatic organisms
53: May cause long-term adverse effects in the aquatic environment
Safety Statements:
28: After contact with skin, wash immediately with plenty of ... (to be specified by the manufacturer)
36: Wear suitable protective clothing
37: Wear suitable gloves
45: In case of accident or if you feel unwell, seek medical advice immediately (show label where possible)
60: This material and/or its container must be disposed of as hazardous waste
61: Avoid release to the environment. Refer to special instructions safety data sheet
Specification
Stability and Reactivity of 2,6-Dichloroaniline(608-31-1):
Conditions to Avoid: Incompatible materials, light, exposure to air.
Chemical Stability:Stable under normal temperatures and pressures.
Incompatibilities with Other Materials: Exposure to acids, acid chlorides, acid anhydrides,air.
Hazardous Decomposition Products: carbon dioxide,carbon monoxide,Hydrogen chloride,nitrogen oxides.
Conditions to Avoid: Incompatible materials, light, exposure to air.
Chemical Stability:Stable under normal temperatures and pressures.
Incompatibilities with Other Materials: Exposure to acids, acid chlorides, acid anhydrides,air.
Hazardous Decomposition Products: carbon dioxide,carbon monoxide,Hydrogen chloride,nitrogen oxides.