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68592-15-4

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Basic Information
CAS No.: 68592-15-4
Name: 4'-Methoxy-3',5-di-2-propenyl-(1,1'-biphenyl)-2-ol
Article Data: 11
Molecular Structure:
Molecular Structure of 68592-15-4 (4'-Methoxy-3',5-di-2-propenyl-(1,1'-biphenyl)-2-ol)
Formula: C19H20O2
Molecular Weight: 280.367
Synonyms: methoxyhonokiol;4'-O-Methylhonokiol;METHYLHONOKIOL;4-methoxyhonokiol;3,5'-diallyl-2'-hydroxy-4-methoxy-1,1'-biphenyl;3,5'-diallyl-2'-hydroxy-4-methoxybiphenyl;
Density: 1.054g/cm3
Boiling Point: 396.5oC at 760 mmHg
Flash Point: 176.2oC
PSA: 29.46000
LogP: 4.52480
Related products
Synthetic route

potassium 3-allyl-4-methoxyphenyltrifluoroborate

17269-79-3

4-allyl-2-bromo-phenol

68592-15-4

methylhonokiol

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate; ruphos In 1,2-dimethoxyethane; water at 130℃; for 0.166667h; Suzuki-Miyaura coupling; Microwave irradiation;72%
With palladium diacetate; potassium carbonate; ruphos In 1,2-dimethoxyethane; water at 130℃; Reagent/catalyst; Solvent; Temperature; Suzuki-Miyaura Coupling; Sealed tube; Microwave irradiation;72%
17269-79-3

4-allyl-2-bromo-phenol

1378871-34-1

4-methoxy-3-allyl-1-phenylboronic acid

68592-15-4

methylhonokiol

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); caesium carbonate In 1,2-dimethoxyethane; water Suzuki coupling; Reflux; Inert atmosphere;52%
114303-65-0

2-allyl-4-bromo-1-methoxybenzene

108886-90-4

1-allyl-4-oxocyclohexa-2,5-dienylethanoate

68592-15-4

methylhonokiol

Conditions
ConditionsYield
Stage #1: 2-allyl-4-bromo-1-methoxybenzene With magnesium; ethylene dibromide In diethyl ether for 1h; Reflux;
Stage #2: 1-allyl-4-oxocyclohexa-2,5-dienylethanoate In diethyl ether at 0℃; for 0.5h;		50%
35354-74-6

Honokiol

74-88-4

methyl iodide

A

68592-19-8

3,5′-diallyl-2′-methoxy-[1,1′-biphenyl]-4-ol

B

68592-15-4

methylhonokiol

C

68592-18-7

Dimethylhonokiol

Conditions
ConditionsYield
With potassium carbonate In water; dimethyl sulfoxide at 60℃;A 50%
B 20%
C 15%
With sodium hydroxide In water; dimethyl sulfoxide at 60℃;A 46%
B 20%
C 30%
With caesium carbonate In water; dimethyl sulfoxide at 60℃; Reagent/catalyst;A 21%
B 35%
C 15%
...Expand
35354-74-6

Honokiol

18107-18-1

diazomethyl-trimethyl-silane

A

68592-19-8

3,5′-diallyl-2′-methoxy-[1,1′-biphenyl]-4-ol

B

68592-15-4

methylhonokiol

C

68592-18-7

Dimethylhonokiol

Conditions
ConditionsYield
In methanolA 13%
B 13%
C 47%
...Expand
35354-74-6

Honokiol

74-88-4

methyl iodide

68592-15-4

methylhonokiol

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃;41%
143051-79-0

2-[(2R,4aR,8R,8aR)-8-(5,3'-Diallyl-4'-methoxy-biphenyl-2-yloxy)-4a,8-dimethyl-decahydro-naphthalen-2-yl]-propan-2-ol

A

68592-15-4

methylhonokiol

B

13902-07-3, 15051-81-7, 72173-98-9, 98683-12-6, 117066-77-0, 1209-71-8

eudesm-4-en-11-ol

Conditions
ConditionsYield
With trifluoroacetic acid In benzene for 10h; Ambient temperature;A 6 mg
B 2 mg
133056-10-7

eudeshonokiol B

68592-15-4

methylhonokiol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diethyl ether / 36 h / Ambient temperature
2: 6 mg / CF3COOH / benzene / 10 h / Ambient temperature
View Scheme
140-67-0

Estragole

68592-15-4

methylhonokiol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: boron trichloride-dimethyl sulfide / trans-1,2-dichloroethylene; dichloromethane / 18 h / Reflux
2.1: acetic acid / 8 h
3.1: magnesium; ethylene dibromide / diethyl ether / 1 h / Reflux
3.2: 0.5 h / 0 °C
View Scheme
Multi-step reaction with 3 steps
1: methyl magnesium iodide / 180 °C
2: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; isopropylmagnesium chloride / diethyl ether / 24 h / -78 - 20 °C
3: palladium diacetate; potassium carbonate; ruphos / 1,2-dimethoxyethane; water / 0.17 h / 130 °C / Microwave irradiation
View Scheme
Multi-step reaction with 3 steps
1.1: boron tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere
2.1: isopropylmagnesium chloride / diethyl ether / 1.05 h / -78 °C / Inert atmosphere
2.2: 21 h / -78 - 20 °C
3.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere
View Scheme
501-92-8

4-(prop-2-enyl)phenol

68592-15-4

methylhonokiol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: acetic acid / 8 h
2.1: magnesium; ethylene dibromide / diethyl ether / 1 h / Reflux
2.2: 0.5 h / 0 °C
View Scheme
Multi-step reaction with 2 steps
1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; isopropylmagnesium chloride / diethyl ether / 24 h / -78 - 20 °C
2: palladium diacetate; potassium carbonate; ruphos / 1,2-dimethoxyethane; water / 0.17 h / 130 °C / Microwave irradiation
View Scheme
Multi-step reaction with 2 steps
1.1: isopropylmagnesium chloride / diethyl ether / 1.05 h / -78 °C / Inert atmosphere
1.2: 21 h / -78 - 20 °C
2.1: tetrakis(triphenylphosphine) palladium(0); caesium carbonate / 1,2-dimethoxyethane; water / Reflux; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: isopropylmagnesium chloride / diethyl ether / 0.67 h / -78 °C / Inert atmosphere
1.2: 2.5 h / 20 °C / Inert atmosphere
2.1: potassium carbonate; palladium diacetate; ruphos / 1,2-dimethoxyethane; water / 130 °C / Sealed tube; Microwave irradiation
View Scheme
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