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| CAS No.: | 693-07-2 |
|---|---|
| Name: | 2-Chloroethyl ethyl sulfide |
| Article Data: | 16 |
| Molecular Structure: | |
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|
|
| Formula: | C4H9ClS |
| Molecular Weight: | 124.634 |
| Synonyms: | Sulfide,2-chloroethyl ethyl (6CI,7CI,8CI);1-Chloro-2-(ethylsulfanyl)ethane;1-Chloro-2-(ethylthio)ethane;2-(Ethylthio)chloroethane;2-Chlorodiethylsulfide;2-Chloroethyl ethyl sulfide;2-Chloroethyl ethyl thioether;2-Ethylthioethyl chloride;Ethyl 2-chloroethyl sulfide;H-MG;Half-sulfurmustard;NSC 10977; |
| EINECS: | 211-742-1 |
| Density: | 1.07 |
| Boiling Point: | 156-157 ºC |
| Flash Point: | 52 ºC |
| Solubility: | insoluble |
| Appearance: | clear colourless to light yellow liquid |
| Hazard Symbols: |
|
| Risk Codes: | R10;R22;R36/37/38;R40 |
| Safety: | Poison by ingestion and subcutaneous routes. Mutation data reported. A severe skin and eye irritant. See also ETHERS and SULFIDES. When heated to decomposition it emits very toxic fumes of Cl− and SOx. |
| Transport Information: | UN 1992 |
| PSA: | 25.30000 |
| LogP: | 1.97830 |
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- 107-06-2
1,2-dichloro-ethane
- 75-08-1
ethanethiol
A
- 5395-75-5
1,2-bis(ethylthio)ethane
B
- 693-07-2
2-Chloroethyl ethyl sulfide
| Conditions | Yield |
|---|---|
| Stage #1: ethanethiol With potassium hydroxide; hydrazine hydrate for 1h; Stage #2: 1,2-dichloro-ethane at 50℃; for 2h; | A 68% B 6% |
| Conditions | Yield |
|---|---|
| at -10 - -5℃; |
| Conditions | Yield |
|---|---|
| With hydrogenchloride | |
| With thionyl chloride; chloroform | |
| With phosphorus trichloride | |
| With thionyl chloride In chloroform Heating; | |
| With thionyl chloride |
- 860213-87-2
1-ethylsulfanyl-2-butoxy-ethane
- 693-07-2
2-Chloroethyl ethyl sulfide
| Conditions | Yield |
|---|---|
| With 1,4-dioxane; hydrogenchloride |
| Conditions | Yield |
|---|---|
| With methanol |
A
- 5395-75-5
1,2-bis(ethylthio)ethane
B
- 75-00-3
chloroethane
C
- 110-77-0
2-(ethylsulfanyl)ethanol
D
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6-oxa-3,9-dithiaundecane
E
- 693-07-2
2-Chloroethyl ethyl sulfide
| Conditions | Yield |
|---|---|
| With hydrogenchloride In water at 90℃; for 1h; Product distribution; Mechanism; | A 2.4 % Chromat. B 2.3 % Chromat. C 44.9 % Chromat. D 2.9 % Chromat. E 44.9 % Chromat. |
- 7719-09-7
thionyl chloride
- 57830-41-8
3,6-dithiaoctan-1-ol
A
- 505-29-3
1,4-Dithiane
B
- 693-07-2
2-Chloroethyl ethyl sulfide
| Conditions | Yield |
|---|---|
| at 100℃; |
- 7719-09-7
thionyl chloride
- 57830-41-8
3,6-dithiaoctan-1-ol
A
- 505-29-3
1,4-Dithiane
B
- 92569-22-7
1-chloro-3,6-dithiaoctane
C
- 693-07-2
2-Chloroethyl ethyl sulfide
| Conditions | Yield |
|---|---|
| at 35℃; |
| Conditions | Yield |
|---|---|
| With potassium hydroxide; triisopropylsilanol In N,N-dimethyl-formamide Ambient temperature; | 100% |
| With potassium tert-butylate Kinetics; | |
| With potassium hydroxide; triisopropylsilanol In N,N-dimethyl-formamide at 25℃; | 100 % Chromat. |
- 693-07-2
2-Chloroethyl ethyl sulfide
- 27998-62-5
2-chloroethyl ethyl sulfoxide
| Conditions | Yield |
|---|---|
| With methanesulfonic acid; urea hydrogen peroxide adduct In methanol Flow reactor; | 98% |
| With N-(tert-butyl)-N-chloro-cyanamide In water; acetonitrile | 97% |
| With 1,8-diazabicyclo[5.4.0]undec-7-ene hydrobromide-perbromide In water; acetonitrile at 20℃; for 0.0166667h; | 94% |
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Specification
The IUPAC name of 2-Chloroethyl ethyl sulfide is 1-Chloro-2-ethylsulfanylethane , with the CAS registry number 693-07-2, it is also named as 1-Chloro-2-(ethylthio)ethane ; 2-(Ethylthio)chloroethane ; 2-Chloroethyl ethyl sulfide ; 2-Chloroethyl ethyl thioether ; 2-Chloroethyl(ethyl)sulfide ; 2-Ethylthioethyl chloride ; Chlordiethylsulfid ; Ethane, 1-chloro-2-(ethylthio)- . It belongs to the following product categories, such as Organic Building Blocks. This product must store at 0-6 °C. 2-Chloroethyl ethyl sulfide is clear colourless to light yellow liquid and is insoluble in water.
2-Chloroethyl ethyl sulfide is harmful by inhalation, in contact with skin and if swallowed so we should rinse immediately with plenty of water and seek medical advice if contact with eyes. We must keep away from sources of ignition and no smoking because it is flammable. 2-Chloroethyl ethyl sulfide is also irritating to eyes, respiratory system and skin so we must wear suitable protective clothing, gloves and eye/face protection when contect with it .
Toxicity of 2-Chloroethyl ethyl sulfide is following:
| Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
|---|---|---|---|---|---|
| mouse | LDLo | subcutaneous | 25mg/kg (25mg/kg) | National Technical Information Service. Vol. PB158-507, | |
| rat | LD50 | oral | 252mg/kg (252mg/kg) | "Sbornik Vysledku Toxixologickeho Vysetreni Latek A Pripravku," Marhold, J.V., Institut Pro Vychovu Vedoucicn Pracovniku Chemickeho Prumyclu Praha, Czechoslovakia, 1972Vol. -, Pg. 170, 1972. |