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75-00-3

Basic Information
CAS No.: 75-00-3
Name: Ethane, chloro-
Molecular Structure:
Molecular Structure of 75-00-3 (Ethane, chloro-)
Formula: C2H5Cl
Molecular Weight: 64.52
Synonyms: Aethylis;Aethylis chloridum;Anodynon;Chlorethyl;Chloridum;Chloroethane;Chloryl;Chloryl Anesthetic;Chloryle anesthetic;Cloretilo;Dublofix;Ether chloratus;Ether hydrochloric;Ether muriatic;Hydrochloric ether;Kelene;Monochloroethane;Muriaticether;Narcotile;R 160;
EINECS: 200-830-5
Density: 0.884 g/cm3
Melting Point: -139 °C(lit.)
Boiling Point: 12.7 °C at 760 mmHg
Flash Point: <-30 °F
Solubility: 6710 mg/L at 25℃
Appearance: colourless gas
Hazard Symbols: HighlyF+,HarmfulXn,ToxicT,FlammableF
Risk Codes: 45-11-20/21/22-36/37/38-52/53-40-12-39/23/24/25-23/24/25-67-66-22-19
Safety: 9-16-33-36/37-61-45-7-29-36/37/39-26-53
Transport Information: UN 1993 3/PG 2
PSA: 0.00000
LogP: 1.24510
Synthetic route
87463-00-1

O-ethyl N-methyl-N-phenylthiocarbamate

A

75-00-3

chloroethane

B

100244-53-9

(N-methyl-N-phenylcarbamoyl)sulfenyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride In chloroform-d1 at 5℃; for 0.166667h;A 100%
B n/a
With sulfuryl dichloride In chloroform-d1 at 25℃;
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

65039-09-0

1-ethyl-3-methyl-1H-imidazol-3-ium chloride

A

377739-43-0

1-ethyl-3-methyl-imidazolium tris(pentafluoroethyl)trifluorophosphate

B

60-29-7

diethyl ether

C

75-00-3

chloroethane

Conditions
ConditionsYield
at 80℃; for 3h; Product distribution / selectivity;A 98.9%
B n/a
C n/a
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

30388-20-6

N,N,N',N',N'',N''-hexamethylguanidinium chloride

A

hexamethylguanidinium tris(pentafluoroethyl)trifluorophosphate

B

60-29-7

diethyl ether

C

75-00-3

chloroethane

Conditions
ConditionsYield
at 80℃; for 3h;A 98.9%
B n/a
C n/a
762-04-9

phosphonic acid diethyl ester

A

75-00-3

chloroethane

B

phosphorous acid monoethyl ester cobaltous salt

Conditions
ConditionsYield
With CoCl2 at 120℃; Product distribution; the thermal stability of the product was investigated by DTA, DTG and TG;A n/a
B 98%
945614-34-6

triethyloxonium bis(trifluoromethylsulfonyl)imide

65039-09-0

1-ethyl-3-methyl-1H-imidazol-3-ium chloride

A

60-29-7

diethyl ether

B

75-00-3

chloroethane

C

174899-82-2

1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide

Conditions
ConditionsYield
at 80℃; for 3h;A n/a
B n/a
C 97.9%
1825-69-0

dimethyl chloro ethoxy silane

75-36-5

acetyl chloride

A

75-00-3

chloroethane

B

acetoxydimethylsilyl isothiocyanate

Conditions
ConditionsYield
at 30 - 40℃; for 1h;A 97%
B 87%
64-17-5

ethanol

75-00-3

chloroethane

Conditions
ConditionsYield
With hydrogenchloride; aluminum (III) chloride; zinc(II) chloride at 70 - 120℃; under 900.09 - 2625.26 Torr; for 2h; Large scale;96.3%
With hydrogenchloride; zinc(II) chloride at 8 - 130℃;65%
With hydrogenchloride
50966-09-1

diethyl (1-benzamido-2,2-dichlorovinyl)phosphonate

A

75-00-3

chloroethane

B

77113-14-5

azlactone of (1-benzamido-2,2-dichlorovinyl)phosphonochloridic acid

Conditions
ConditionsYield
With phosphorus pentachloride at 110 - 120℃; for 5.5h;A n/a
B 96%

1-(chlorodimethylsilyl)-7-(ethoxydimethylsilyl)-m-carbaborane

A

75-00-3

chloroethane

B

B10H10C2(Si(CH3)2O)(Si(CH3)2)

Conditions
ConditionsYield
iron(III) chloride In neat (no solvent) heating (120 - 130°C), addn. of further FeCl3, heating (180°C); reprecipitation (toluene); elem. anal.;A 96%
B 94.7%
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

1-decyl-3-methylimidazol-3-ium chloride

A

60-29-7

diethyl ether

B

75-00-3

chloroethane

C

916807-26-6

1-decyl-3-methylimidazolium tris(pentafluoroethyl)trifluorophosphate

Conditions
ConditionsYield
at 80℃; for 3h;A n/a
B n/a
C 96%
78-38-6

ethylphosphonic acid diethyl ester

A

75-00-3

chloroethane

B

1066-50-8

Ethylphosphonic dichloride

Conditions
ConditionsYield
With thionyl chloride; N,N-dimethyl-formamide for 18h; Heating;A n/a
B 95.8%
589-57-1

diethyl phosphorylchloridite

17640-25-4

methyl 2,2-dichloro-2-methoxyacetate

A

5781-53-3

monomethyl oxalyl chloride

B

553-90-2

Dimethyl oxalate

C

75-00-3

chloroethane

D

66298-75-7

phosphonic dichloride

E

74813-29-9

methyl phosphonochloridate

F

74813-30-2

ethyl phosphonochloridate

Conditions
ConditionsYield
With iron(III) chloride at 105 - 110℃; for 1.16667h; Product distribution;A n/a
B n/a
C 95%
D n/a
E n/a
F n/a
589-57-1

diethyl phosphorylchloridite

17640-25-4

methyl 2,2-dichloro-2-methoxyacetate

A

553-90-2

Dimethyl oxalate

B

1498-42-6

phosphorodichloridous acid ethyl ester

C

75-00-3

chloroethane

D

66298-75-7

phosphonic dichloride

E

74813-30-2

ethyl phosphonochloridate

F

phosphonic dichloride

Conditions
ConditionsYield
With iron(III) chloride at 105 - 110℃; for 0.833333h; Product distribution;A n/a
B n/a
C 95%
D n/a
E n/a
F n/a
762-04-9

phosphonic acid diethyl ester

80-10-4

diphenylsilyl dichloride

A

75-00-3

chloroethane

B

90285-15-7

C16H22O6P2Si

Conditions
ConditionsYield
at 102℃;A n/a
B 94.1%
64-17-5

ethanol

7719-12-2, 52843-90-0

phosphorus trichloride

A

75-00-3

chloroethane

B

762-04-9

phosphonic acid diethyl ester

Conditions
ConditionsYield
at 85℃; under 30.003 Torr; Addition of ca.3% diethyl phosphite (triethyl phosphite or ethyl chloride are also possible);A n/a
B 94%
945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

76-83-5

trityl chloride

A

60-29-7

diethyl ether

B

75-00-3

chloroethane

C

tritylium tris(pentafluoroethyl)trifluorophosphate

Conditions
ConditionsYield
at 80℃; for 10h;A n/a
B n/a
C 93.6%
762-04-9

phosphonic acid diethyl ester

A

75-00-3

chloroethane

B

phosphorous acid monoethyl ester calcium salt

Conditions
ConditionsYield
With calcium chloride at 70℃; for 1h; Product distribution; other time; also in the presence of pyridine; the thermal stability of the product was investigated by DTA, DTG and TG;A n/a
B 93.4%
With calcium chloride at 70℃; for 1h;A n/a
B 93.4%
762-04-9

phosphonic acid diethyl ester

A

75-00-3

chloroethane

B

phosphorous acid monoethyl ester manganese salt

Conditions
ConditionsYield
With manganese(II) acetate at 112℃; for 1h; Product distribution; oter time; the thermal stability of the product was investigated by DTA, DTG and TG;A n/a
B 93%
121-44-8

triethylamine

1005-56-7

phenylcarbonochloridothioate

A

75-00-3

chloroethane

B

24486-06-4

O-phenyl-N,N-diethyl thiocarbamate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 1h; Substitution;A n/a
B 93%

N-(n-hexyl)-N-methylpyrrolidinium chloride

945614-32-4

triethyloxonium tris(pentafluoroethyl)trifluorophosphate

A

60-29-7

diethyl ether

B

75-00-3

chloroethane

C

945614-40-4

1-hexyl-1-methylpyrrolidinium tris(pentafluoroethyl)trifluorophosphate

Conditions
ConditionsYield
at 80℃; for 3h;A n/a
B n/a
C 93%

ethyl o-(N-methylcarbamoyl)phenyl sulphoxide

A

2527-66-4

2-methyl-1,2-benzisothiazole-3(2H)-one

B

75-00-3

chloroethane

Conditions
ConditionsYield
With thionyl chloride In tetrachloromethane for 5h; Heating;A 92%
B n/a

[2,2-Dichloro-1-(4-chloro-benzoylamino)-vinyl]-phosphonic acid diethyl ester

A

75-00-3

chloroethane

B

2-Chloro-5-(4-chloro-phenyl)-3-dichloromethylene-3H-[1,4,2]oxazaphosphole 2-oxide

Conditions
ConditionsYield
With phosphorus pentachloride at 110 - 120℃; for 5.5h;A n/a
B 92%
139535-54-9

N-methyl-N-(2,2-dimethyl-3-chloro-3-ethoxypropyl)methanesulfonamide

A

75-00-3

chloroethane

B

139535-59-4

N-methyl-N-(2,2-dimethyl-3-oxopropyl)methanesulfonamide

Conditions
ConditionsYield
under 9 Torr; Heating;A 91%
B 79%
589-57-1

diethyl phosphorylchloridite

17640-25-4

methyl 2,2-dichloro-2-methoxyacetate

A

75-00-3

chloroethane

B

74813-30-2

ethyl phosphonochloridate

Conditions
ConditionsYield
With iron(III) chloride at 95 - 110℃; for 1.5h;A 90%
B 38%
589-57-1

diethyl phosphorylchloridite

6957-89-7

Ethyl dichloro-(ethoxy)-acetate

A

75-00-3

chloroethane

B

67538-60-7

ethyl phosphonochloridate

C

814-49-3

diethyl chlorophosphate

D

5284-10-6

ethyl ethylphosphonochloridate

Conditions
ConditionsYield
With iron(III) chloride at 95 - 110℃; for 1.5h;A 90%
B 58%
C n/a
D n/a
371-22-2

fluorophosphoric acid diethyl ester

17640-25-4

methyl 2,2-dichloro-2-methoxyacetate

A

75-00-3

chloroethane

B

67538-58-3

ethyl phosphonofluoridate

Conditions
ConditionsYield
With iron(III) chloride at 95 - 110℃; for 1.5h;A 90%
B 45%
371-22-2

fluorophosphoric acid diethyl ester

6957-89-7

Ethyl dichloro-(ethoxy)-acetate

A

75-00-3

chloroethane

B

67538-59-4

ethyl phosphonofluoridate

Conditions
ConditionsYield
With iron(III) chloride at 95 - 110℃; for 1.5h;A 90%
B 50%

[2,2-Dichloro-1-(4-methyl-benzoylamino)-vinyl]-phosphonic acid diethyl ester

A

75-00-3

chloroethane

B

2-Chloro-3-dichloromethylene-5-p-tolyl-3H-[1,4,2]oxazaphosphole 2-oxide

Conditions
ConditionsYield
With phosphorus pentachloride at 110 - 120℃; for 5.5h;A n/a
B 90%
94703-39-6

2,3,3,3-tetrachloro-2-propionitrile

122-52-1

triethyl phosphite

A

75-00-3

chloroethane

B

814-49-3

diethyl chlorophosphate

C

94703-45-4

3,3-dichloro-2-acrylonitrile

Conditions
ConditionsYield
In benzene for 1h; Heating;A n/a
B 90%
C 25%
64317-34-6

N-(pentafluorophenyl)carbonimidoyl dichloride

121-44-8

triethylamine

A

75-00-3

chloroethane

B

120672-75-5

N,N-diethyl-N-pentafluorophenylchloroformamidine

Conditions
ConditionsYield
In diethyl ether at 20℃; for 6h;A n/a
B 90%
616-47-7

1-methyl-1H-imidazole

75-00-3

chloroethane

65039-09-0

1-ethyl-3-methyl-1H-imidazol-3-ium chloride

Conditions
ConditionsYield
In ethanol at 35℃; for 10h; Wavelength; UV-irradiation;100%
79%
In acetonitrile at 70℃; for 168h;71%
75-00-3

chloroethane

7646-78-8

tin(IV) chloride

597-64-8

tetraethyltin

Conditions
ConditionsYield
With magnesium In diethyl ether; toluene at 50℃; Inert atmosphere; Flow reactor;99.4%
75-00-3

chloroethane

62806-88-6

N,N-dipropylcarbamothioate sodium salt

759-94-4

S-ethyl N,N-di-n-propylthiocarbamate

Conditions
ConditionsYield
In water at 80℃; for 0.25h; in ultrasonic field;99.1%
75-00-3

chloroethane

methyl 2-((tert-butoxycarbonyl)(hydroxy)amino)acetate

methyl 2-((tert-butoxycarbonyl)(ethoxy)amino)acetate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 3h;99%
75-00-3

chloroethane

121-33-5

vanillin

13184-86-6

phenol, 4-(ethoxymethyl)-2-methoxy-

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol at 30 - 40℃; for 4h;98.56%
75-00-3

chloroethane

sodium hexamethylenethiocarbamate

2212-67-1

S-ethyl N-hexamethylenethiocarbamate

Conditions
ConditionsYield
In water at 70℃; for 0.333333h; in ultrasonic field;98.4%
75-00-3

chloroethane

102-28-3

m-acetamide aniline

6375-46-8

m-acetylamino-N,N-diethylanilne

Conditions
ConditionsYield
With ammonium hydroxide In water at 90 - 98℃; under 7500.75 Torr; for 18h; pH=5 - 7; Temperature; Large scale;98%
75-00-3

chloroethane

21055-93-6

sodium salt of diethylthiocarbamic acid

2941-55-1

S-ethyl N,N-diethylthiocarbamate

Conditions
ConditionsYield
In water at 80℃; for 0.166667h; in ultrasonic field;97.8%
532-32-1

sodium benzoate

75-00-3

chloroethane

93-89-0

benzoic acid ethyl ester

Conditions
ConditionsYield
With tetrabutylammomium bromide In toluene at 40 - 70℃; under 3000.3 - 4500.45 Torr; for 1h; Reagent/catalyst; Autoclave; Inert atmosphere;97.63%
75-00-3

chloroethane

56368-46-8

sodium pentamethylenethiocarbamate

6961-73-5

piperidine-1-carbothioic acid S-ethyl ester

Conditions
ConditionsYield
In water at 70℃; for 0.25h; in ultrasonic field;97.3%
75-00-3

chloroethane

108-10-1

4-methyl-2-pentanone

91-68-9

3-diethylaminophenol

1864-92-2

N,N-diethyl-3-ethoxyaniline

Conditions
ConditionsYield
With sodium hydroxide; sodium carbonate97.1%
78-10-4

tetraethoxy orthosilicate

75-00-3

chloroethane

5021-93-2

diethyldiethoxysilane

Conditions
ConditionsYield
With magnesium at 50 - 100℃;97%
With magnesium at 60℃; for 1h; Temperature;94%
75-00-3

chloroethane

108-18-9

diisopropylamine

7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With lithium chloride; zinc(II) chloride at 190℃; under 16501.7 Torr; for 10h; Catalytic behavior; Temperature; Pressure; Time; Reagent/catalyst; Autoclave;96.7%
17771-33-4

7-hydroxy-2,2-dimethyl-chroman-4-one

75-00-3

chloroethane

76348-94-2

2,2-dimethyl-7-ethoxy-4-chromanone

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 80℃; for 5h;96%
15231-91-1

6-bromo-naphthalen-2-ol

75-00-3

chloroethane

66217-19-4

2-ethoxy-6-bromo-naphthalene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 3.5h;96%
75-00-3

chloroethane

6375-47-9

3-amino-4-methoxyacetanilide

19433-93-3

3-acetylamino-6-methoxy-N,N-diethylaniline

Conditions
ConditionsYield
With sodium hydroxide In water at 80 - 97℃; under 7500.75 Torr; for 22.5h; pH=6.5 - 7;96%
75-00-3

chloroethane

603-35-0

triphenylphosphine

896-33-3

ethyltriphenylphosphonium chloride

Conditions
ConditionsYield
In acetone at 150℃; under 9000.9 Torr; for 40h; Solvent; Temperature; Pressure; Autoclave;95.23%
In acetonitrile for 10h; Inert atmosphere; Reflux;83.2%
108-89-4

picoline

75-00-3

chloroethane

105757-96-8

1-Ethyl-4-methylpyridinium chloride

Conditions
ConditionsYield
In acetonitrile at 80℃; for 5h;95%
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    75-00-3

    MSDS/COA Download

    Ethyl Chloride 99.5% 99.8% 99.9%

    Min.Order: 0 Metric Ton

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  • CHLOROETHANE

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    CHLOROETHANE

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  • 75-00-3               C2H5Cl           CHLOROETHANE

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Consensus Reports

ETHYL CHLORIDE is reported in EPA TSCA Inventory. Community Right-To-Know List.

Standards and Recommendations

OSHA PEL: TWA 1000 ppm
ACGIH TLV: TWA 1000 ppm
DFG MAK: Confirmed Animal Carcinogen with Unknown Relevance to Humans
NIOSH REL: (Chloroethane) Handle with caution
DOT Classification:  2.1; Label: Flammable Gas

Specification

The Ethane, chloro-, with the CAS registry number 75-00-3, is also known as Octamethylsilanetetramine. It belongs to the product categories of Refrigerants; Organics; Halides (Low Boiling point); Alkyl Chlorides; Gas Cylinders; Monofunctional & alpha,omega-Bifunctional Alkanes; Monofunctional Alkanes; Synthetic Organic Chemistry. Its EINECS number is 200-830-5. This chemical's molecular formula is C2H5Cl and molecular weight is 64.51. What's more, its systematic name is chloroethane. (1)Anesthetic [topical]; (2)Anesthetics; (3)Anesthetics, local; (4)Central Nervous System Agents; (5)Central Nervous System Depressants; (6)Drug / Therapeutic Agent; (7)Mutation data; (8)Peripheral Nervous System Agents; (9)Reproductive Effect; (10)Sensory System Agents; (11)TSCA Flag T [Subject to the Section 4 test rule under TSCA]; (12)Tumor data. It is stable at common pressure and temperature, and it should be sealed and stored in a cool and dry place. Moreover, it should be protected from oxides and water. It is used as a refrigerant, an aerosol spray propellant, an anesthetic, and a blowing agent for foam packaging. 

Physical properties of Ethane, chloro- are: (1)ACD/LogP: 1.50; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 1.5; (4)ACD/LogD (pH 7.4): 1.5; (5)ACD/BCF (pH 5.5): 8.14; (6)ACD/BCF (pH 7.4): 8.14; (7)ACD/KOC (pH 5.5): 156.06; (8)ACD/KOC (pH 7.4): 156.06; (9)Index of Refraction: 1.361; (10)Molar Refractivity: 16.16 cm3; (11)Molar Volume: 72.9 cm3; (12)Polarizability: 6.4×10-24cm3; (13)Surface Tension: 17.9 dyne/cm; (14)Density: 0.884 g/cm3; (15)Enthalpy of Vaporization: 24.97 kJ/mol; (16)Boiling Point: 12.7 °C at 760 mmHg; (17)Vapour Pressure: 1170 mmHg at 25°C.

Preparation: this chemical can be prepared by ethylphosphonic acid diethyl ester by heating. This reaction will need reagent SOCl2 with the reaction time of 18 hours. This reaction will also need catalyst DMF. The yield is about 95.8%.

Ethane, chloro- can be prepared by ethylphosphonic acid diethyl ester by heating

Uses of Ethane, chloro-: it can be used to produce 1-Ethyl-4-methylpyridinium chloride at the temperature of 80 °C. It will need solvent acetonitrile with the reaction time of 5 hours. The yield is about 95%.

Ethane, chloro- can be used to produce 1-Ethyl-4-methylpyridinium chloride at the temperature of 80 °C

When you are using this chemical, please be cautious about it as the following:
This chemical is extremely flammable, so you should keep it away from sources of ignition - No smoking. It has a limited evidence of a carcinogenic effect. It is harmful to aquatic organisms as it may cause long-term adverse effects in the aquatic environment. You should keep the container in a well-ventilated place and take precautionary measures against static discharges. When using it, you need wear suitable protective clothing and gloves. You must avoid releasing it to the environment just refering to special instructions/safety data sheet.

You can still convert the following datas into molecular structure:
(1)SMILES: ClCC
(2)Std. InChI: InChI=1S/C2H5Cl/c1-2-3/h2H2,1H3
(3)Std. InChIKey: HRYZWHHZPQKTII-UHFFFAOYSA-N

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
guinea pig LCLo inhalation 40000ppm/45M (40000ppm) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

BEHAVIORAL: EXCITEMENT

LUNGS, THORAX, OR RESPIRATION: ACUTE PULMONARY EDEMA
U.S. Public Health Service, Public Health Bulletin. Vol. 185, Pg. 1, 1929.
mouse LC50 inhalation 146gm/m3/2H (146000mg/m3)   "Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects, GKNT, 1982Vol. -, Pg. 66, 1982.
rat LC50 inhalation 152gm/m3/2H (152000mg/m3) BRAIN AND COVERINGS: OTHER DEGENERATIVE CHANGES

BEHAVIORAL: GENERAL ANESTHETIC

BLOOD: HEMORRHAGE
Toksikologiya Novykh Promyshlennykh Khimicheskikh Veshchestv. Toxicology of New Industrial Chemical Substances. For English translation, see TNICS*. Vol. 6, Pg. 45, 1964.