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7149-10-2

Basic Information
CAS No.: 7149-10-2
Name: 4-Hydroxy-3-methoxybenzylamine hydrochloride
Article Data: 11
Molecular Structure:
Molecular Structure of 7149-10-2 (4-Hydroxy-3-methoxybenzylamine hydrochloride)
Formula: C8H12ClNO2
Molecular Weight: 189.642
Synonyms: Creosol, a-amino-, hydrochloride (6CI);Phenol, 4-(aminomethyl)-2-methoxy-, hydrochloride (9CI);p-Cresol, a-amino-2-methoxy-, hydrochloride(8CI);3-Methoxy-4-hydroxybenzylamine hydrochloride;4-(Aminomethyl)-2-methoxyphenol hydrochloride;4-Hydroxy-3-methoxybenzylamine monohydrochloride;Vanillylaminehydrochloride;a-Amino-2-methoxy-p-cresolhydrochloride;a-Aminocreosolhydrochloride;
EINECS: 230-468-3
Melting Point: 219-221 °C (dec.)(lit.)
Boiling Point: 292.9 °C at 760 mmHg
Flash Point: 130.9 °C
Appearance: white to light yellow crystal powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-37/39-36
PSA: 55.48000
LogP: 2.36180
Synthetic route
2874-33-1

vanillin oxime

7149-10-2

vanillylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In ethanol at 20℃; for 3h;100%
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethanol under 760 Torr; for 4h;98%
Stage #1: vanillin oxime With hydrogen In ethanol at 40℃; for 8h;
Stage #2: With hydrogenchloride In ethanol; water pH=1; Temperature;
90.5%
121-33-5

vanillin

7149-10-2

vanillylamine hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol / 6 h / 20 °C
2: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; water / 760.05 Torr
View Scheme
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol / 6 h / 20 °C
2: hydrogenchloride; hydrogen; palladium 10% on activated carbon / ethanol / 760.05 Torr
View Scheme
Stage #1: vanillin With ammonia In methanol at 20℃; for 3h;
Stage #2: With methanol; sodium tetrahydroborate at 45℃;
Stage #3: With hydrogenchloride In water at 0℃; for 3h; Temperature; Concentration;
112 g
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium acetate trihydrate / water / 2 h / 80 °C
2: palladium 10% on activated carbon; hydrogenchloride; hydrogen / ethanol / 24 h / 20 °C / 760.05 Torr
View Scheme
134283-49-1

(E)-4-hydroxy-3-methoxybenzaldehyde oxime

7149-10-2

vanillylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In ethanol at 20℃; under 760.051 Torr; for 24h;74%
93249-67-3

4-hydroxy-3-methoxybenzaldehyde O-methyloxime

7149-10-2

vanillylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; hydrogen; palladium on activated charcoal In ethanol under 760 Torr; for 4h;
121-33-5

vanillin

KOH-solution

KOH-solution

7149-10-2

vanillylamine hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 98 percent / pyridine / Ambient temperature
2: H2, conc. hydrochloric acid / 10percent Pd/C / ethanol / 4 h / 760 Torr
View Scheme
Multi-step reaction with 2 steps
1: 83 percent / NH2OH*HCl, pyridine / ethanol / 24 h / Ambient temperature
2: 98 percent / H2, conc. hydrochloric acid / 10percent Pd/C / ethanol / 4 h / 760 Torr
View Scheme
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Chemistry

IUPAC Name: 4-(Aminomethyl)-2-methoxyphenol hydrochloride
Synonyms of 4-Aminomethyl-2-methoxyphenol hydrochloride (CAS NO.7149-10-2): 4-Aminomethyl-2-methoxyphenol HCl ; EINECS 230-468-3 ; NSC 62020
CAS NO: 7149-10-2
Molecular Formula of 4-Aminomethyl-2-methoxyphenol hydrochloride (CAS NO.7149-10-2): C8H12ClNO2
Molecular Weight: 189.6394
Molecular Structure:

Melting Point: 219-221 °C
ProductCategories: Pharmaceutical Raw Materials ; Chemical intermediate for Capsaicine ; Anilines, Aromatic Amines and Nitro Compounds ; Chemical Amines ; Amines ; Aromatics ; ntermediates & Fine Chemicals ; Metabolites & Impurities ; Pharmaceuticals 
H bond acceptors: 3
H bond donors: 3
Freely Rotating Bonds: 4
Polar Surface Area: 21.7 ?2
Flash Point of 4-Aminomethyl-2-methoxyphenol hydrochloride (CAS NO.7149-10-2): 130.9 °C
Enthalpy of Vaporization: 55.37 kJ/mol
Boiling Point: 292.9 °C at 760 mmHg
Vapour Pressure: 0.00102 mmHg at 25°C

Uses

  4-Aminomethyl-2-methoxyphenol hydrochloride (CAS NO.7149-10-2) is used as Capsaicin.

Safety Profile

  4-Aminomethyl-2-methoxyphenol hydrochloride (CAS NO.7149-10-2): 's Safety Information
Hazard Codes: IrritantXi
Risk Statements: 36/37/38 
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26-37/39-36 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S37/39: Wear suitable gloves and eye/face protection. 
S36: Wear suitable protective clothing.
WGK Germany: 3 
Hazard Note  Irritant

Specification

Handling and Storage 
Handling: Avoid breathing dust, vapor, mist, or gas. Avoid contact with skin and eyes. 
Storage: Store in a cool, dry place. Store in a tightly closed container. 
 4-Aminomethyl-2-methoxyphenol hydrochloride's hazards identification
Eye: Causes eye irritation. 
Skin: Causes skin irritation. May be harmful if absorbed through the skin. 
Ingestion: May cause irritation of the digestive tract. May be harmful if swallowed. 
Inhalation: Causes respiratory tract irritation. May be harmful if inhaled.