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765-17-3

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Basic Information
CAS No.: 765-17-3
Name: bombykol
Article Data: 30
Molecular Structure:
Molecular Structure of 765-17-3 (bombykol)
Formula: C16H30 O
Molecular Weight: 238.414
Synonyms: 10,12-Hexadecadien-1-ol,(Z,E)- (8CI); 10,12-Hexadecadien-1-ol, trans-10,cis-12- (7CI);(E,Z)-10,12-Hexadecadien-1-ol; (E,Z)-10,12-Hexadecadienol; Bombycol; Bombykol;Hexadeca-10-trans,12-cis-dien-1-ol
Density: 0.859g/cm3
Boiling Point: 298.3°C at 760 mmHg
Flash Point: 133.5°C
PSA: 20.23000
LogP: 5.01200
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Conditions
ConditionsYield
With pyridinium p-toluenesulfonate In ethanol at 70℃; for 4h;97.7%
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(10E,12Z)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In tetrahydrofuran at 0℃; for 2h; Substitution;93%
With tetrabutyl ammonium fluoride In tetrahydrofuran at 0℃; for 4h;
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(E)-10-hexadecen-12-yn-1-ol

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(10E,12Z)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
With water; silver; copper; zinc In methanol at 60 - 70℃; for 6.5h;90%
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With hydrogen; Lindlar's catalyst In methanol
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(10E,12Z)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium ethanolate In ethanol; benzene for 2.5h; Heating;82%
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(E)-11-hydroxy-1-undecenyl iodide

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(10E,12Z)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
With potassium hydroxide; PdL482%

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(10E,12Z)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
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(bromo-8 octyloxy-1)-1, ethoxy-1 ethane

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acetoxy-1 octadiene-2,4 (E,Z)

A

765-17-3

(10E,12Z)-hexadeca-10,12-dien-1-ol

B

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(10E,12E)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
With magnesium In tetrahydrofuran; diethyl ether at -30℃; for 1.5h;A 75%
B 20%
...Expand
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chloro-8 trimethylsilyl oxy-1 octane

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acetoxy-1 octadiene-2,4 (E,Z)

A

765-17-3

(10E,12Z)-hexadeca-10,12-dien-1-ol

B

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(10E,12E)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
With magnesium In tetrahydrofuran; diethyl ether at -30℃; for 1.5h;A 75%
B 20%
...Expand
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(10E,12Z)-Hexadeca-1,10,12-triene

765-17-3

(10E,12Z)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
Stage #1: (10E,12Z)-Hexadeca-1,10,12-triene With 9-borabicyclo[3.3.1]nonane dimer In tetrahydrofuran for 2h; Addition;
Stage #2: With sodium hydroxide; dihydrogen peroxide In tetrahydrofuran at 25℃; for 2h; Oxidation;		67%
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(10E,12Z)-hexadeca-10,12-dien-1-ol

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium ethanolate In ethanol; benzene for 2.5h; Heating;50%
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