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778-09-6

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Basic Information
CAS No.: 778-09-6
Name: N-Acetyl DeMethyl MeMantine
Article Data: 13
Molecular Structure:
Molecular Structure of 778-09-6 (N-Acetyl DeMethyl MeMantine)
Formula: C13H21NO
Molecular Weight: 207.316
Synonyms: 1-methyl-3-acetylaminoadamantane;N-acetyl-3-methyl-1-aminoadamantane;1-N-acetylamino-3-methyladamantane;1-acetylamino-3-methyladamantane;N-acetyl-1-amino-3-methyladamantane;
Density: 1.06g/cm3
Melting Point: 111-113°C
Boiling Point: 349.9°Cat760mmHg
Flash Point: 209.5°C
PSA: 29.10000
LogP: 2.87230
Related products
Synthetic route
702-77-2

1-bromo-3-methyladamantane

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acetonitrile

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
With sulfuric acid at 20℃; for 12h; Ritter Amidation;90%
With sulfuric acid
Stage #1: 1-bromo-3-methyladamantane; acetonitrile With phosphoric acid at 20 - 87℃; for 18.5h;
Stage #2: With sodium hydroxide; water; butan-1-ol In toluene at 20 - 45℃; pH=6 - 7;
768-91-2

1-methyl-adamantane

75-05-8

acetonitrile

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
Stage #1: 1-methyl-adamantane With sulfuric acid; nitric acid at 0℃; for 6h;
Stage #2: acetonitrile at 0℃; for 6h; Ritter-type reaction; Further stages.;		41.6%
(anodic oxidation);
60-35-5

acetamide

768-91-2

1-methyl-adamantane

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
With nitric acid at 120℃; for 2h;70%
770-14-9

3,7-dimethylenebicyclo[3.3.1]nonane

2261-02-1

acetylium tetrafluoroborate

75-05-8

acetonitrile

A

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

B

118647-96-4

1-acetonyl-3-acetylaminoadamantane

Conditions
ConditionsYield
In dichloromethane at -40℃; for 0.25h;A 15%
B 75%
...Expand
702-81-8

3-methyl-1-adamantanol

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 85 percent / Ph3P, Br2 / acetonitrile / 30 h / Heating
2: 78 percent / Heating
View Scheme
60-35-5

acetamide

702-77-2

1-bromo-3-methyladamantane

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
Heating;78%
101974-65-6

3-methyl-1-adamantanol nitrate

75-05-8

acetonitrile

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
With sulfuric acid for 3h;75.8%
768-91-2

1-methyl-adamantane

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Br2
2: H2SO4
View Scheme
Multi-step reaction with 2 steps
1: bromine / 20 °C / Reflux
2: sulfuric acid / 12 h / 20 °C
View Scheme
770-14-9

3,7-dimethylenebicyclo[3.3.1]nonane

75-05-8

acetonitrile

778-09-6

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane

Conditions
ConditionsYield
With sulfuric acid
Raw Materials
770-14-9
702-77-2
75-05-8
768-91-2
702-81-8
60-35-5
2261-02-1
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78056-28-7
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