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Basic Information
CAS No.: 79-76-5
Name: 4-(2,2-dimethyl-6-methylenecyclohexyl)-3-buten-2-one
Article Data: 3
Molecular Structure:
Molecular Structure of 79-76-5 (4-(2,2-dimethyl-6-methylenecyclohexyl)-3-buten-2-one)
Formula: C13H20 O
Molecular Weight: 192.301
Synonyms: g-Ionone
EINECS: 201-223-8
Density: 0.91 g/cm3
Boiling Point: 267.8 °C at 760 mmHg
Flash Point: 112.3 °C
PSA: 17.07000
LogP: 3.51410
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Synthetic route
472-19-5, 4352-33-4

(2,2-dimethyl-6-methylenecyclohexyl)methanol

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1-triphenylphosphoranylidene-2-propanone

79-76-5

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Conditions
ConditionsYield
Stage #1: 2,2-dimethyl-6-methylenecyclohexanemethanol With oxalyl dichloride; dimethyl sulfoxide In dichloromethane at -78℃; for 3h; Inert atmosphere;
Stage #2: With triethylamine In dichloromethane at -78 - 20℃; Inert atmosphere;
Stage #3: 1-triphenylphosphoranylidene-2-propanone In toluene for 16h; Inert atmosphere; Reflux;		67%
472-76-4

(E)-4-(2,2-Dimethyl-6-methylene-cyclohexyl)-but-3-en-2-ol

79-76-5

γ-ionone

Conditions
ConditionsYield
With manganese(IV) oxide In chloroform for 6h; Heating;

Acetic acid (E)-3-(2,2-dimethyl-6-methylene-cyclohexyl)-1-methyl-allyl ester

79-76-5

γ-ionone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: KOH / methanol / 20 °C
2: MnO2 / CHCl3 / 6 h / Heating
View Scheme
25312-34-9

alpha-ionol

79-76-5

γ-ionone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 91 percent / pyridine / 6 h
2: propan-2-ol; xylene / 480 h / UV-irradiation
3: KOH / methanol / 20 °C
4: MnO2 / CHCl3 / 6 h / Heating
View Scheme
783324-41-4

(2E)-1-methyl-3-(2,6,6-trimethyl-2-cyclohexen-1-yl)-2-propenyl acetate

79-76-5

γ-ionone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: propan-2-ol; xylene / 480 h / UV-irradiation
2: KOH / methanol / 20 °C
3: MnO2 / CHCl3 / 6 h / Heating
View Scheme
81752-87-6

methyl (+/-)-2,2-dimethyl-6-methylene-1-cyclohexanecarboxylate

79-76-5

γ-ionone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 3 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
2.3: 16 h / Inert atmosphere; Reflux
View Scheme
79-76-5

γ-ionone

13720-12-2

4-(2',2'-Dimethyl-6'-methylidenecyclohexyl)butan-2-one

Conditions
ConditionsYield
Stage #1: γ-ionone With water; tri-n-butyl-tin hydride; ammonium chloride; 1-triphenylphosphoranylidene-2-propanone In tetrahydrofuran for 3h; Inert atmosphere;
Stage #2: With sodium fluoride In water; ethyl acetate for 5h; Inert atmosphere;		76%
79-76-5

γ-ionone

74-86-2

acetylene

Ethinyl-Φ-ionol

Conditions
ConditionsYield
(i) naphthalene/Li, THF, (ii) /BRN= 2690409/; Multistep reaction;
79-76-5

γ-ionone

70143-17-8

(E)-4-(5,5-Dimethyl-1-oxa-spiro[2.5]oct-4-yl)-but-3-en-2-one

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0℃; for 4h;
79-76-5

γ-ionone

(+)-7,11-epoxymegastigma-5(6)-en-9-one

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: MCPBA / CH2Cl2 / 4 h / 0 °C
2: 18.9 g / NaOMe / dimethylformamide / 3 h / 20 °C
3: Pseudomonas cepacia lipase PS / various solvent(s)
4: KOH / methanol / 20 °C
5: 93 percent / pyridine*SO3; Et3N / dimethylsulfoxide / 3 h
View Scheme
Multi-step reaction with 5 steps
1: MCPBA / CH2Cl2 / 4 h / 0 °C
2: 18.9 g / NaOMe / dimethylformamide / 3 h / 20 °C
3: 28 percent / NaBH4 / methanol / 2 h / 0 °C
4: Pseudomonas cepacia lipase PS / various solvent(s)
5: pyridine*SO3; Et3N / dimethylsulfoxide / 3 h
View Scheme
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    FOB Price:  USD $ 0.0-0.0

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    Wuhan NewGreat Chemical Co., Ltd. is located in Wuhan Donghu High-tech Development Zone. Wuhan has unique geographical advantages. It is close to Zhengzhou, Changsha, Nanchang and

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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  • (E)-4-(2,2-dimethyl-6-methylidenecyclohexyl)but-3-en-2-one

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-731-85570686

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    China (Mainland)  |  Contact Details

    Business Type:Other

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    Zhejiang Jiuzhou Chemical Co.,Ltd is a market-oriented and innovation-driven biopharmaceutical company. The company is focusing on the R&D, manufacturing and sales of pharmaceutica

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    1,Best Quality: Our products have exported to Germany, Spain, UK, USA, Australia, Middle East, and so on other countries, and we have got very good feedback from our customers.so

    Hubei Jusheng Technology Co., Ltd., is a large group corporation which engaged in the R&D and manufacture of chemicals, Pharmaceuticals and intermediates. We have earned ourselves

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-18871490254

    Address:High-tech Industrial Park,Tianmen city,Hubei province.

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    We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

    Shandong Jiashisheng Biotechnolgy Co.,Ltd is located in high-tech Zone, Liaocheng City, Shandong Province, China, old factory was found in 2008, also named Jiashisheng Group. Here

  • Shandong Jiashisheng Biotechnolgy Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:13165407087

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    Locating in Changchun bonded area, which has absolute advantage of importing and exporting, with the R&D team having more than 10 years experience of OLED material and intermediate

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Min.Order: 0

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    Nanjing Raymon Biotech Co., Ltd. is specialized in developing and marketing middle & high level pharmaceutical intermediates. We are supplying different categories of high-quality

  • Nanjing Raymon Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-025-52181296

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    Shanghai PengMo Biotechnology Co., Ltd. is engaging in researching, developing, manufacturing and exporting advanced pharmaceutical intermediates and other fine chemicals. Our comp

  • Shanghai PengMo Biotechnology Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-13052359378

    Address:No.218 Hai Qu Road.Shanghai.China

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  • 4-(2,2-dimethyl-6-methylenecyclohexyl)-3-Buten-2-one

  • Casno:

    79-76-5

    4-(2,2-dimethyl-6-methylenecyclohexyl)-3-Buten-2-one

    Min.Order: 0

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    1.Fast and safety delivery by well-reputed shipping line;2.we have our own chemical laboratory and factory3.Reasonable price, excellent quality and attentive service.4.prompt reply.we can reply your inquiry within 12 hours.5.sample free(depends on pr

    We are a manufacturer and trader in China, with 10 years of experience in the export of chemical and pharmaceutical raw materials and 320 employees. We are all promoted on Made in

  • Hebei Zhaojun New Material Technology Co., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8617320695765

    Address:Qiu County gucheng ying Town Zhang Zhang Lu villag

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