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79099-07-3

Basic Information
CAS No.: 79099-07-3
Name: N-(tert-Butoxycarbonyl)-4-piperidone
Molecular Structure:
Molecular Structure of 79099-07-3 (N-(tert-Butoxycarbonyl)-4-piperidone)
Formula: C10H17NO3
Molecular Weight: 199.25
Synonyms: 1,1-Dimethylethyl4-oxo-1-piperidinecarboxylate;1-(tert-Butoxycarbonyl)-4-oxopiperidine;1-(tert-Butyloxycarbonyl)-4-piperidone;1-BOC-4-piperidone;1-Boc-4-oxopiperidine;4-Oxo-1-(tert-butoxycarbonyl)piperidine;4-Oxopiperidin-1-carboxylic acid tert-butyl ester;N-(tert-Butoxycarbonyl)-4-piperidinone;N-(tert-Butyloxycarbonyl)piperidin-4-one;N-BOC-4-piperidone;N-Boc-4-oxopiperidine;N-Boc-piperidin-4-one;tert-Butyl 4-oxo-1-piperidinecarboxylate;
EINECS: 616-664-5
Density: 1.099 g/cm3
Melting Point: 73-77 ºC
Boiling Point: 289.8 ºC at 760 mmHg
Flash Point: 129.1 ºC
Solubility: slightly soluble in Water
Appearance: light yellow powder
Hazard Symbols: HarmfulXn,IrritantXi
Risk Codes: 36/37/38-20/21/22
Safety: 37/39-26-36
Transport Information:
PSA: 46.61000
LogP: 1.52430
Synthetic route
24424-99-5

di-tert-butyl dicarbonate

41979-39-9

4-piperidone hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With sodium hydrogencarbonate In water 1) 35 deg C, 1 h; 2) 50 deg C, 2.5 h;100%
With sodium hydroxide In tetrahydrofuran; water at 20℃; for 16h;100%
Stage #1: di-tert-butyl dicarbonate; 4-piperidone hydrochloride With triethylamine; dmap In methanol at 20℃; for 20h;
Stage #2: With hydrogenchloride In dichloromethane
100%
24424-99-5

di-tert-butyl dicarbonate

40064-34-4

piperidine-4,4-diol hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With sodium carbonate In tetrahydrofuran; water at 20℃; for 12h;99%
With sodium hydroxide In tetrahydrofuran; water at 20℃; for 16h;98.6%
With potassium hydrogencarbonate In chloroform at 20℃;95%
73390-11-1

4-piperidinone monohydrate

24424-99-5

di-tert-butyl dicarbonate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With sodium hydrogencarbonate In water at 50℃; for 3h;99%
24424-99-5

di-tert-butyl dicarbonate

5174-67-4

piperidin-2-one hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With dmap; N-ethyl-N,N-diisopropylamine In acetonitrile for 2h; Inert atmosphere;99%
4248-19-5

tert-butyl carbamate

41979-39-9

4-piperidone hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
Stage #1: 4-piperidone hydrochloride With sodium hydroxide In water at 0℃;
Stage #2: tert-butyl carbazate In water for 4h;
98.44%
41661-47-6

piperidin-4-one

tert-butyl (3-cyano-4,6-dimethylpyridin-2-yl) carbonate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
In ethanol for 1h; Reflux;96%
41661-47-6

piperidin-4-one

24424-99-5

di-tert-butyl dicarbonate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With triethylamine In methanol; dichloromethane at 0 - 25℃; for 12h; Inert atmosphere;95%
With triethylamine In dichloromethane at 20℃; for 16h;86%
With sodium hydroxide In tetrahydrofuran for 2h; Ambient temperature;
109384-19-2

t-butyl 4-hydroxy piperidine-1-carboxylate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With bis(1,5-cyclooctadiene)nickel(0); potassium tert-butylate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride In 2,4-dichlorotoluene at 25℃; for 0.5h; Inert atmosphere;95%
With sodium hypochlorite; C186H204N12O36; sodium hydrogencarbonate; potassium bromide In dichloromethane; water at 0 - 15℃; for 4h; pH=8.6;95%
With (diacetoxyiodo)benzene In dichloromethane at 20℃; for 3h;95%
24424-99-5

di-tert-butyl dicarbonate

40064-34-4

4-piperidone monohydrochloride monohydrate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With sodium hydroxide In 1,4-dioxane; water for 12h; Cooling with ice;94%
With sodium hydroxide In 1,4-dioxane92.5%
With triethylamine In dichloromethane; ethyl acetate86%
541-16-2

t-butyl malonate

40064-34-4

piperidine-4,4-diol hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran; water at 0 - 20℃;93%
24424-99-5

di-tert-butyl dicarbonate

piperidin-4-one hydrochloride monohydrate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With sodium hydroxide In 1,4-dioxane93%
With triethylamine In dichloromethane at 20℃;88%
With sodium carbonate In 1,4-dioxane; water at 20℃; for 1h;87%
With sodium carbonate In 1,4-dioxane; water at 20℃; for 1h;87%
152559-29-0

5-tert-butoxycarbonyl-3-hydroxy-4,5,6,7-tetrahyroisoxazolo<4,3-c>pyridine

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With hydrogen; platinum on activated charcoal In ethanol Ambient temperature;86%
3612-20-2

1-phenylmethyl-4-piperidone

24424-99-5

di-tert-butyl dicarbonate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With PMHS; palladium dihydroxide In ethanol at 20℃; for 5h;86%
40064-34-4

4-piperidone monohydrochloride monohydrate

41840-28-2

S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane; water for 6h; Ambient temperature;81.3%
41840-28-2

S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine

40064-34-4

piperidine-4,4-diol hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With triethylamine In 1,4-dioxane; water at 20℃; for 6h;81.3%
856684-31-6

tert-butyl 4-((diphenoxyphosphoryl)oxy)-3,6-dihydropyridine-1(2H)-carboxylate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With triethylsilane; cyclohexa-1,4-diene; oxygen; cobalt acetylacetonate In methanol; nonane at 24℃; under 760.051 Torr; Reagent/catalyst;81%
34619-03-9

tert-butyldicarbonate

41979-39-9

4-piperidone hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With triethylamine In methanol at 20℃; for 2h;75%
With triethylamine In dichloromethane at 0 - 20℃;71%
762-75-4

tert-butyl formate

piperidin-4-one hydrochloride monohydrate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 16h; Inert atmosphere;73%
159635-49-1

tert-butyl 4-methylidenepiperidine-1-carboxylate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With 2,6-dimethylpyridine; sodium periodate; ruthenium(III) chloride trihydrate In dichloromethane; water; acetonitrile at 20℃; for 1h; Inert atmosphere;71%
154775-43-6

3-(1-(tert-butoxycarbonyl)piperidin-4-yl)propanoic acid

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With (2,2'-dipyridyl)bis(5-methyl-2-(4-fluoro)phenylpyridine-N,C)iridium(III) hexafluorophosphate; oxygen; sodium carbonate; 1,1'-diethyl-4,4'-bipyridinium diperchlorate In dimethyl sulfoxide at 20℃; under 760.051 Torr; for 16h; Irradiation;68%
84358-13-4

N-[(tert-butoxy)carbonyl]piperidine-4-carboxylic acid

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With (2,2'-dipyridyl)bis(5-methyl-2-(4-fluoro)phenylpyridine-N,C)iridium(III) hexafluorophosphate; oxygen; sodium carbonate; 1,1'-diethyl-4,4'-bipyridinium diperchlorate In dimethyl sulfoxide at 20℃; under 760.051 Torr; for 16h; Irradiation;67%
157688-46-5

2-(1-(tert-butoxycarbonyl)piperidin-4-yl)acetic acid

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With (2,2'-dipyridyl)bis(5-methyl-2-(4-fluoro)phenylpyridine-N,C)iridium(III) hexafluorophosphate; oxygen; sodium carbonate; 1,1'-diethyl-4,4'-bipyridinium diperchlorate In dimethyl sulfoxide at 20℃; under 760.051 Torr; for 16h; Irradiation;63%
137076-22-3

tert butyl 4-formylpiperidine-1-carboxylate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With (2,2'-dipyridyl)bis(5-methyl-2-(4-fluoro)phenylpyridine-N,C)iridium(III) hexafluorophosphate; oxygen; sodium carbonate; 1,1'-diethyl-4,4'-bipyridinium diperchlorate In dimethyl sulfoxide at 20℃; under 760.051 Torr; for 16h; Irradiation;17%
188622-27-7

tert-butyl 4-methoxypiperidine-1-carboxylate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
With calcium hypochlorite; acetic acid In water; acetonitrile at 0℃; regioselective reaction;3%
5382-16-1

4-HYDROXYPIPERIDINE

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaOH / tetrahydrofuran; H2O / 1 h / 20 °C
2: SO3*NMe3; triethylamine; DMSO / 18 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: CH2Cl2 / 1 h / 20 °C
2: tetrapropylammoniumperruthenate; NMO; 3 Angstroem molecular sieves / CH2Cl2 / 1 h
View Scheme
Multi-step reaction with 2 steps
1: sodium carbonate / tetrahydrofuran; water / 0 - 20 °C
2: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium carbonate / tetrahydrofuran; water / 0 - 20 °C
2: Dess-Martin periodane / dichloromethane / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium hydroxide; water / 1,4-dioxane / 0 - 20 °C
2: pyridinium chlorochromate; SiO2 / dichloromethane / 2 h / 20 °C
View Scheme
24424-99-5

di-tert-butyl dicarbonate

1.) NaH; 2.) SOCl2

1.) NaH; 2.) SOCl2

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaOH / tetrahydrofuran; H2O / 1 h / 20 °C
2: SO3*NMe3; triethylamine; DMSO / 18 h / 20 °C
View Scheme
24424-99-5

di-tert-butyl dicarbonate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: CH2Cl2 / 1 h / 20 °C
2: tetrapropylammoniumperruthenate; NMO; 3 Angstroem molecular sieves / CH2Cl2 / 1 h
View Scheme
Multi-step reaction with 3 steps
1: 96 percent / NaCO3, NaCl / CHCl3; H2O / 12 h / Heating
2: 59 percent / NaOH, NH2OH*HCl / H2O / 1 h / 0 °C
3: 86 percent / H2 / 10percent Pt/C / ethanol / Ambient temperature
View Scheme
With triethylamine In diethyl ether; dichloromethane
4644-61-5

ethyl 4-piperidone-3-carboxylate hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 96 percent / NaCO3, NaCl / CHCl3; H2O / 12 h / Heating
2: 59 percent / NaOH, NH2OH*HCl / H2O / 1 h / 0 °C
3: 86 percent / H2 / 10percent Pt/C / ethanol / Ambient temperature
View Scheme
1454-53-1

ethyl 1-benzyl-4-oxopiperidine-3-carboxylate hydrochloride

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 99 percent / H2 / 10percent Pd/C / ethanol; H2O / 24 h / 2280 Torr / Ambient temperature
2: 96 percent / NaCO3, NaCl / CHCl3; H2O / 12 h / Heating
3: 59 percent / NaOH, NH2OH*HCl / H2O / 1 h / 0 °C
4: 86 percent / H2 / 10percent Pt/C / ethanol / Ambient temperature
View Scheme
623-73-4

diazoacetic acid ethyl ester

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

141642-82-2

5-oxo-azepane-1,4-dicarboxylic acid 1-tert-butyl ester 4-ethyl ester

Conditions
ConditionsYield
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one With boron trifluoride diethyl etherate In diethyl ether at -30 - -25℃; for 0.333333h;
Stage #2: diazoacetic acid ethyl ester In diethyl ether at -30 - 20℃;
100%
With boron trifluoride diethyl etherate In diethyl ether at -25℃; for 1h; Inert atmosphere;99%
Stage #1: diazoacetic acid ethyl ester; N-tert-butyloxycarbonylpiperidin-4-one With boron trifluoride diethyl etherate In diethyl ether at 0℃; for 2h;
Stage #2: With sodium carbonate In diethyl ether; water at 0℃;
98%
2537-48-6

diethyl 1-cyanomethylphosphonate

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

4-(cyanomethylidene)piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With lithium hexamethyldisilazane In tetrahydrofuran at -70℃; for 0.666667h; Inert atmosphere;100%
With lithium hexamethyldisilazane In tetrahydrofuran at -70℃; for 0.666667h; Inert atmosphere;100%
With lithium bromide In tetrahydrofuran at 20℃; for 3h; Inert atmosphere;100%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

95-55-6

2-amino-phenol

162045-48-9

1-(tert-butoxycarbonyl)-4-[(2-hydroxyphenyl)amino]piperidine

Conditions
ConditionsYield
100%
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; 2-amino-phenol With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 120℃; for 0.0833333h; Microwave irradiation;
Stage #2: With water; sodium hydrogencarbonate
75%
With sodium tris(acetoxy)borohydride
75-77-4

chloro-trimethyl-silane

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

211108-48-4

tert-butyl 4-[(trimethylsilyl)oxy]-3,6-dihydropyridine-1(2H)-carboxylate

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide Inert atmosphere;100%
With sodium hydrogencarbonate; triethylamine In N,N-dimethyl-formamide at 90℃; for 21h; Inert atmosphere;99%
With triethylamine In N,N-dimethyl-formamide at 0 - 90℃;99%
110-91-8

morpholine

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

217807-98-2

4-morpholin-4-yl-3,6-dihydro-2H-pyridine-1-carboxylic acid ter-tbutyl ester

Conditions
ConditionsYield
toluene-4-sulfonic acid In benzene for 24h; Heating / reflux;100%
With toluene-4-sulfonic acid In toluene Reflux;100%
With toluene-4-sulfonic acid In toluene for 16h; Reflux; Inert atmosphere;100%
867-13-0

diethoxyphosphoryl-acetic acid ethyl ester

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

135716-08-4

tert-butyl 4-(2-ethoxy-2-oxoethylidene)piperidine-1-carboxylate

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran at 20℃; for 1h; Horner-Emmons reaction;100%
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran at 0℃; for 0.5h;
Stage #2: N-tert-butyloxycarbonylpiperidin-4-one In tetrahydrofuran at 20℃; for 22h;
100%
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran at 0 - 5℃; for 0.5h;
Stage #2: N-tert-butyloxycarbonylpiperidin-4-one In tetrahydrofuran at 0 - 20℃; for 2h;
100%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

109384-19-2

t-butyl 4-hydroxy piperidine-1-carboxylate

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol100%
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one With sodium tetrahydroborate In ethanol at 0 - 20℃; for 4h;
Stage #2: With water; ammonium chloride In ethanol
100%
With sodium hydroxide; sodium borohydrid In methanol100%
123-75-1

pyrrolidine

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

207691-65-4

N-tert-butoxycarbonyl-4-(tetrahydropyrrole-1-yl)-1,2,3,6-tetrahydropyridine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene for 20h; Heating;100%
In toluene for 6h; Heating / reflux;100%
In toluene at 90℃; for 3h; Dean-Stark;100%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

75-04-7

ethylamine

264905-39-7

4-(N-ethylamino)-1-tert-butoxycarbonylpiperidine

Conditions
ConditionsYield
With hydrogen; platinum on carbon In ethanol; water at 50℃; under 1500.15 Torr; for 4h;100%
With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran; 1,2-dichloro-ethane at 20℃; for 24h; Inert atmosphere;99%
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; ethylamine With acetic acid In tetrahydrofuran for 0.0833333h;
Stage #2: With sodium tris(acetoxy)borohydride In tetrahydrofuran for 24h;
94%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

107-11-9

1-amino-2-propene

235420-68-5

1-(t-butoxycarbonyl)-4-(N-prop-2-enyl)aminopiperidine

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In dichloromethane at 20℃;100%
With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran at 0 - 20℃;95%
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃;
With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran at 20℃;
With sodium tris(acetoxy)borohydride; acetic acid In tetrahydrofuran at 20℃;
50-00-0

formaldehyd

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

100-46-9

benzylamine

227940-70-7

7-benzyl-9-oxo-3,7-diazabicyclo[3.3.1]nonane-3-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With acetic acid In methanol for 4h; Heating / reflux;100%
With acetic acid In methanol Reflux;100%
With acetic acid In methanol for 5h; Reflux;100%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

156-87-6

propan-1-ol-3-amine

864655-26-5

tert-butyl 4-[(3-hydroxypropyl)amino]piperidine-1-carboxylate

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon In ethanol under 3361.55 Torr; for 1.5h;100%
With hydrogen; palladium on activated charcoal In methanol at 20℃; under 760.051 Torr; for 24h;99%
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane for 2h;
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; propan-1-ol-3-amine With acetic acid In dichloromethane at 20 - 27℃; for 3h;
Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20 - 27℃; Inert atmosphere;
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

100-46-9

benzylamine

206273-87-2

4-benzylamino-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In dichloromethane; acetic acid at 20℃;100%
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; benzylamine With acetic acid In dichloromethane at 20℃; for 1h;
Stage #2: With sodium tris(acetoxy)borohydride In dichloromethane at 20℃; for 16h;
100%
With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; for 16h;98%
496-15-1

1-indoline

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

400828-91-3

tert-butyl 4-(indolin-1-yl) piperidine-1-carboxylate

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 0 - 65℃; for 65h; Product distribution / selectivity;100%
With sodium tris(acetoxy)borohydride; acetic acid at 0 - 25℃; for 1h; Product distribution / selectivity;100%
Stage #1: 1-indoline; N-tert-butyloxycarbonylpiperidin-4-one With acetic acid In 1,2-dichloro-ethane at 0℃; for 0.166667h;
Stage #2: With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 10 - 20℃; for 65h; Product distribution / selectivity;
100%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

13139-86-1

4-methoxyphenyl magnesium bromide

302924-67-0

tert-butyl 4-hydroxy-4-(4-methoxyphenyl)-1-piperidinecarboxylate

Conditions
ConditionsYield
In diethyl ether at 0 - 20℃; for 2h;100%
In diethyl ether at 0 - 20℃; for 2h;100%
In diethyl ether at 0 - 20℃; for 2h;100%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

6146-52-7

5-nitroindole

151273-41-5

tert-butyl 4-(5-nitro-1H-indol-3-yl)-5,6-dihydropyridine-1(2H)-carboxylate

Conditions
ConditionsYield
With pyrrolidine In ethanol at 20℃; for 72h; Heating / reflux;100%
With sodium methylate In methanol for 24h; Reflux;87%
With pyrrolidine In ethanol at 20℃; for 72h;80%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

105-56-6

ethyl 2-cyanoacetate

193537-11-0

tert-butyl 4-(1-cyano-2-ethoxy-2-oxoethylidene)-4-piperidine-1-carboxylate

Conditions
ConditionsYield
With ammonium acetate; acetic acid; benzene100%
With ammonium acetate; acetic acid In benzene for 4h; Reflux; Inert atmosphere;99%
With ammonium acetate In acetic acid; benzene for 4h; Heating / reflux;99%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

141-43-5

ethanolamine

701298-37-5

tert-butyl 4-[(2-hydroxyethyl)amino]piperidine-1-carboxylate

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In methanol at 20℃; under 760.051 Torr; for 24h;100%
With hydrogen; palladium 10% on activated carbon In ethanol under 3361.55 Torr; for 1.5h;100%
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; ethanolamine With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; Inert atmosphere;
Stage #2: With sodium hydroxide In dichloromethane; water pH=10;
94%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

4637-24-5

N,N-dimethyl-formamide dimethyl acetal

157327-41-8

t-butyl-3-[(dimethylamino)methylidene]-4-oxopiperidine-1-carboxylate

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 80℃; for 24h;100%
In N,N-dimethyl-formamide at 80℃; for 24h;100%
at 95℃; for 1.5h;94.4%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

107-91-5

cyanoacetic acid amide

1001020-08-1

tert-butyl 2-amino-3-carbamoyl-4,5-dihydrothieno[2,3-c]pyridine-6(7H)-carboxylate

Conditions
ConditionsYield
With morpholine; sulfur In ethanol at 20℃;100%
With morpholine; sulfur In ethanol for 4h; Gewald Aminoheterocycles Synthesis; Reflux; Inert atmosphere;95%
With sulfur; diethylamine In ethanol at 20℃;93%
13472-85-0

2-methoxy-5-bromopyridine

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

850141-84-3

4-(2-methoxy-5-pyridinyl)-4-hydroxy-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 12h;100%
Stage #1: 2-methoxy-5-bromopyridine With n-butyllithium In tetrahydrofuran; hexanes at -78℃; for 0.0833333h;
Stage #2: N-tert-butyloxycarbonylpiperidin-4-one In tetrahydrofuran; hexanes at -78 - 0℃;
44%
With n-butyllithium In diethyl ether; hexane at -78 - 20℃;42%
Stage #1: 2-methoxy-5-bromopyridine With n-butyllithium In diethyl ether; hexane at -78℃; for 0.5h;
Stage #2: N-tert-butyloxycarbonylpiperidin-4-one In diethyl ether; hexane at -78 - 25℃;
42%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

41661-47-6

piperidin-4-one

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 0 - 20℃; for 3h;100%
With trifluoroacetic acid In dichloromethane at 20℃;100%
With trifluoroacetic acid In dichloromethane
With trifluoroacetic acid In 1,2-dichloro-ethane
With hydrogenchloride In 1,4-dioxane at 20℃; for 4h;6.5 g
372-19-0

meta-fluoroaniline

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

679409-18-8

tert-butyl 4-((3-fluorophenyl)amino)piperidine-1-carboxylate

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃;100%
With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; for 2h; Cooling with ice;98.1%
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 0 - 20℃; for 2h;91%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

2516-47-4

cyclopropanemethylamine

710973-92-5

4-(cyclopropylmethylamino)piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon In tetrahydrofuran under 2068.65 Torr; for 1h;100%
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; Acidic conditions;74%
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 25℃;
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; cyclopropanemethylamine With sodium acetate; acetic acid In tetrahydrofuran at 20℃; for 1h;
Stage #2: With sodium tris(acetoxy)borohydride In tetrahydrofuran at 20℃; for 15h;
Stage #3: With hydrogenchloride In diethyl ether; water
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; cyclopropanemethylamine With sodium acetate; acetic acid In tetrahydrofuran at 20℃; for 1h;
Stage #2: With sodium tris(acetoxy)borohydride In tetrahydrofuran for 15h;
Stage #3: With sodium hydroxide; water
107-85-7

1-amino-3-methylbutane

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

710974-71-3

4-(3-methyl-butylamino)-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon In ethanol under 3102.97 Torr;100%
With hydrogen; palladium 10% on activated carbon In ethanol under 3102.97 Torr;100%
With hydrogen; palladium on activated carbon In ethanol under 3102.97 Torr;100%
With hydrogen; palladium on activated carbon In ethanol under 3102.97 Torr;100%
With sodium tris(acetoxy)borohydride In dichloromethane at 20℃;
5813-64-9

2,2-dimethylpropylamine

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

710976-87-7

tert-butyl 4-[(2,2-dimethylpropyl)amino]piperidine-1-carboxylate

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon In ethanol under 3102.97 Torr; for 3h;100%
Stage #1: 2.2-dimethylpropylamine; N-tert-butyloxycarbonylpiperidin-4-one With triethylamine; zinc(II) chloride In methanol at 65℃; for 6h;
Stage #2: With sodium cyanoborohydride In methanol at 0 - 25℃; for 17h;
88%
With sodium tetrahydroborate In methanol at 0 - 20℃; for 42h;
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

150008-24-5

tert-butyl 4-(hydroxyimino)piperidine-1-carboxylate

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium hydroxide In ethanol; water for 0.5h; Reflux;100%
With hydrogenchloride; hydroxylamine In ethanol for 1.5h; Reflux;100%
With hydroxylamine hydrochloride; sodium acetate In methanol; water Reflux;100%
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

74-89-5

methylamine

147539-41-1

4-methylamino-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one; methylamine In methanol for 1h; pH=5 - 6;
Stage #2: With methanol; sodium cyanoborohydride for 12h; Cooling with ice;
100%
With formic acid; palladium 10% on activated carbon; hydrogen In ethanol at 50℃; under 30003 Torr; Autoclave;99%
With formic acid; palladium 10% on activated carbon; hydrogen In ethanol at 50℃; under 30003 Torr; Autoclave;99%
558-13-4

carbon tetrabromide

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

305794-65-4

tert-butyl 4-(dibromomethylidene)piperidine-1-carboxylate

Conditions
ConditionsYield
With triphenylphosphine In dichloromethane at 0 - 20℃; for 72h; Inert atmosphere;100%
With triphenylphosphine In acetonitrile at 0 - 25℃; for 2.25h;56%
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0 - 20℃; for 0.5h;
Stage #2: N-tert-butyloxycarbonylpiperidin-4-one In dichloromethane at -78 - 20℃;
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0 - 20℃;
Stage #2: N-tert-butyloxycarbonylpiperidin-4-one In dichloromethane at -78 - 20℃;
Stage #1: carbon tetrabromide With triphenylphosphine In dichloromethane at 0 - 20℃;
Stage #2: N-tert-butyloxycarbonylpiperidin-4-one In dichloromethane at -78 - 20℃;
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    D - glucuronic acid and N - acetyl glucosamine disaccharides unit composed of hyaluronic acid (Hyaluronan), also called uronic acid, hyaluronic acid, basic structure is made up of two disaccharides unit D - glucuronic acid and N - acetyl glucosamin

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    79099-07-3

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  • N-(tert-Butoxycarbonyl)-4-piperidone/ LIDE PHARMA- Factory supply / Best price

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    79099-07-3

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Chemistry

Molecular Structure:

Molecular Formula: C10H17NO3
Molecular Weight: 199.2469
IUPAC Name: tert-Butyl 4-oxopiperidine-1-carboxylate
Synonyms of N-(tert-Butoxycarbonyl)-4-piperidone (CAS NO.79099-07-3): BOC-Piperidone ; tert-Butyl 4-oxopiperidine-1-carboxylate ; 1-Piperidinecarboxylicacid, 4-oxo-, 1,1-dimethylethyl ester
CAS NO: 79099-07-3
Classification Code: Amines; blocks; Carbonyl Compounds; Heterocycles; Miscellaneous Biochemicals; pharmacetical; Pyrans, Piperidines &Piperazines; Piperidine; Piperidines; Amino Acids & Derivatives; Pyrans, Piperidines & Piperazines
Melting point: 73-77 °C 
Index of Refraction: 1.481
Molar Refractivity: 51.57 cm3
Molar Volume: 181.1 cm3
Surface Tension: 39.5 dyne/cm
Density: 1.099 g/cm3
Flash Point: 129.1 °C
Enthalpy of Vaporization: 52.92 kJ/mol
Boiling Point: 289.8 °C at 760 mmHg
Vapour Pressure: 0.00215 mmHg at 25 °C

Uses

  N-(tert-Butoxycarbonyl)-4-piperidone (CAS NO.79099-07-3) is used as a pharmaceutical intermediates.

Safety Profile

Hazard Codes of N-(tert-Butoxycarbonyl)-4-piperidone (CAS NO.79099-07-3): HarmfulXn,IrritantXi
Risk Statements: 36/37/38-20/21/22 
R36/37/38: Irritating to eyes, respiratory system and skin. 
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed.
Safety Statements: 37/39-26-36 
S37/39: Wear suitable gloves and eye/face protection. 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S36: Wear suitable protective clothing.
WGK Germany: 3
Hazard Note: Irritant

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