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87120-72-7

Basic Information
CAS No.: 87120-72-7
Name: 1-Piperidinecarboxylicacid, 4-amino-, 1,1-dimethylethyl ester
Molecular Structure:
Molecular Structure of 87120-72-7 (1-Piperidinecarboxylicacid, 4-amino-, 1,1-dimethylethyl ester)
Formula: C10H20N2O2
Molecular Weight: 200.28
Synonyms: 1,1-Dimethylethyl4-amino-1-piperidinecarboxylate;1-(t-Butoxycarbonyl)-4-aminopiperidine;1-tert-Butoxycarbonyl-4-aminopiperidine;4-Amino-1-(tert-butyloxycarbonyl)piperidine;4-Amino-1-piperidinecarboxylic acid 1,1-dimethylethyl ester;4-Amino-1-tert-butoxycarbonylpiperidine;4-Amino-N-Boc-piperidine;4-Aminopiperidine-1-carboxylic acid tert-butyl ester;N-Boc-4-aminopiperidine;N-tert-Butoxycarbonyl-4-aminopiperidine;[N-(tert-Butoxycarbonyl)piperidin-4-yl]amine;tert-Butyl4-aminopiperidine-1-carboxylate;
EINECS: 1312995-182-4
Density: 1.041 g/cm3
Melting Point: 50 °C
Boiling Point: 277.3 °C at 760 mmHg
Flash Point: 121.5 °C
Solubility: Insoluble in water.
Appearance: white to light yellow crystal powder
Hazard Symbols: HarmfulXn, IrritantXi
Risk Codes: 20/21/22-36/37/38
Safety: 22-26-36/37/39
Transport Information:
PSA: 55.56000
LogP: 1.98280
Synthetic route
206273-87-2

4-benzylamino-piperidine-1-carboxylic acid tert-butyl ester

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon In ethanol under 5320.36 Torr;98%
With hydrogen; palladium 10% on activated carbon In ethanol98%
With hydrogen; palladium on activated charcoal In methanol
150008-24-5

tert-butyl 4-(hydroxyimino)piperidine-1-carboxylate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With hydrogen; Raney nickel In ethanol under 2585.81 Torr;98%
With Raney nickel In methanol at 20℃; for 4h;83%
With hydrogen; 5% rhodium on activated aluminium oxide In methanol at 50℃;
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one With hydroxylamine hydrochloride; sodium carbonate In water at 23℃; for 14h;
Stage #2: With hydrogen; Raney Ni In ethanol under 2585.81 Torr; for 3.5h; Solid phase;
96%
In ammonia-saturated methanol; aluminum nickel95.4%
Stage #1: N-tert-butyloxycarbonylpiperidin-4-one With titanium(IV) isopropylate; ammonia In ethanol at 25℃; for 6h;
Stage #2: With sodium tetrahydroborate In ethanol at 25℃; for 3h; Further stages.;
88%

C18H24F3N3O2

A

434-45-7

1,1,1-trifluoroacetophenone

B

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With chloro-trimethyl-silane; lithium chlorideA n/a
B 90%

C18H24F3N3O2

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With chloro-trimethyl-silane; lithium chloride In N,N-dimethyl-formamide at 60℃; for 12h;90%
13035-19-3

4-aminopiperidine

24424-99-5

di-tert-butyl dicarbonate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Stage #1: 4-aminopiperidine; di-tert-butyl dicarbonate In 4-methyl-2-pentanone at 0 - 20℃; for 0.5h; Inert atmosphere; Reflux;
Stage #2: With water In isopropyl alcohol at 50℃;
85%
In dichloromethane at 0℃; for 5h;71.9%
Stage #1: 4-aminopiperidine With benzaldehyde In toluene for 3h; Heating / reflux;
Stage #2: di-tert-butyl dicarbonate In toluene at 20℃;
With triethylamine In 1,4-dioxane; water
With triethylamine In 1,4-dioxane; water
153198-06-2

tert-butyl 4-(2,2,2-trifluoroacetamido)piperidine-1-carboxylate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With ammonium hydroxide In methanol for 2h; Heating;81%
With ammonium hydroxide In methanol for 6h; Heating;5.75 g
With sodium bicarbonate; potassium carbonate In methanol

tert-butyl 4-[(2,4-dimethoxyphenyl)methylamino]piperidine-1-carboxylate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In methanol at 25℃; for 16h;81%
873088-90-5

1,1-dimethylethyl 4-[bis(phenylmethyl)amino]-1-piperidinecarboxylate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With hydrogen; palladium(II) hydroxide In tetrahydrofuran; ethanol at 23℃; under 760.051 Torr; for 6h; Inert atmosphere;77%
180695-80-1

tert-butyl 4-azidopiperidine-1-carboxylate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With ammonium hydroxide; triphenylphosphine In 1,4-dioxane; methanol at 27 - 28℃; for 0.5h;44%
With hydrogen; palladium on activated charcoal In methanol under 2068.59 Torr;
palladium-carbon In methanol
palladium-carbon In methanol; hexane; ethyl acetate
1044183-50-7

4-(benzylidene-amino)-piperidine-1-carboxylic acid tert-butyl ester

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With acetic acid for 48h;160 mg
With potassium hydrogensulfate for 1.5h;4.76 g
With sodium hydrogen sulfate; water for 2h;
With potassium hydrogensulfate; water In tert-butyl methyl ether at 20℃; for 4h; Inert atmosphere;6.0 g
1029643-92-2

N-phenylmethylidenepiperidinyl-4-amine

A

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

B

(polystyrene-BAL)-NH-CH2-C6H4-p-NO2

(polystyrene-BAL)-NH-CH2-C6H4-p-NO2

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: toluene / 12 h / 25 °C
2: 4.76 g / aq. KHSO4 / 1.5 h
View Scheme
13035-19-3

4-aminopiperidine

A

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

B

(polystyrene-BAL)-NH-CH2-C6H4-p-NO2

(polystyrene-BAL)-NH-CH2-C6H4-p-NO2

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: toluene / 4 h / Heating
2: toluene / 12 h / 25 °C
3: 4.76 g / aq. KHSO4 / 1.5 h
View Scheme
1029643-92-2

N-phenylmethylidenepiperidinyl-4-amine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Et3N / CH2Cl2 / 48 h / 20 °C
2: 160 mg / aq. AcOH / 48 h
View Scheme
Multi-step reaction with 2 steps
1: toluene / 14.08 h / 0 - 20 °C / Inert atmosphere
2: potassium hydrogensulfate; water / tert-butyl methyl ether / 4 h / 20 °C / Inert atmosphere
View Scheme
13035-19-3

4-aminopiperidine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: Na2SO4 / CH2Cl2 / 24 h / 20 °C
2: Et3N / CH2Cl2 / 48 h / 20 °C
3: 160 mg / aq. AcOH / 48 h
View Scheme
Multi-step reaction with 3 steps
1: toluene / 5.5 h / Inert atmosphere; Reflux
2: toluene / 14.08 h / 0 - 20 °C / Inert atmosphere
3: potassium hydrogensulfate; water / tert-butyl methyl ether / 4 h / 20 °C / Inert atmosphere
View Scheme
79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

A

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

B

4-pyrimidinyl-halide

4-pyrimidinyl-halide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaHB(OAc)3 / 1,2-dichloro-ethane
2: H2 / Pd/C / methanol
View Scheme
50541-93-0

4-amino-1-benzylpiperidine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 94 percent / Et3N / CH2Cl2 / 12 h / 20 °C
2: H2 / Pd(OH)2/C / methanol / 12 h / 2585.81 Torr
3: CH2Cl2 / 6 h
4: 5.75 g / aq. NH3 / methanol / 6 h / Heating
View Scheme
Multi-step reaction with 4 steps
1: 94 percent / Et3N / CH2Cl2 / 0.25 h / 0 °C
2: H2 / Pearlman's catalyst / methanol / 48 h / 3102.9 Torr
3: 82 percent / Et3N / CH2Cl2 / 2 h / Ambient temperature
4: 81 percent / 37percent aq. NH4OH / methanol / 2 h / Heating
View Scheme
97181-51-6

4-trifluoromethylcarbonylamino piperidine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: CH2Cl2 / 6 h
2: 5.75 g / aq. NH3 / methanol / 6 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 82 percent / Et3N / CH2Cl2 / 2 h / Ambient temperature
2: 81 percent / 37percent aq. NH4OH / methanol / 2 h / Heating
View Scheme
97181-50-5

N-(1-benzyl-4-piperidinyl)-2,2,2-trifluoroacetamide

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: H2 / Pd(OH)2/C / methanol / 12 h / 2585.81 Torr
2: CH2Cl2 / 6 h
3: 5.75 g / aq. NH3 / methanol / 6 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: H2 / Pearlman's catalyst / methanol / 48 h / 3102.9 Torr
2: 82 percent / Et3N / CH2Cl2 / 2 h / Ambient temperature
3: 81 percent / 37percent aq. NH4OH / methanol / 2 h / Heating
View Scheme
90633-18-4

4-bromo-1H-piperidine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: DIPEA / CH2Cl2
2: NaN3 / dimethylformamide / 20 °C
3: H2 / 10 percent Pd/C / methanol / 2068.59 Torr
View Scheme
24424-99-5

di-tert-butyl dicarbonate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: DIPEA / CH2Cl2
2: NaN3 / dimethylformamide / 20 °C
3: H2 / 10 percent Pd/C / methanol / 2068.59 Torr
View Scheme
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 16 h / 20 °C
2: palladium on activated charcoal; ammonia; hydrogen / methanol / 20 °C
View Scheme
180695-79-8

tert-butyl 4-bromo-1-piperidinecarboxylate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaN3 / dimethylformamide / 20 °C
2: H2 / 10 percent Pd/C / methanol / 2068.59 Torr
View Scheme
H2 NOH.HCl

H2 NOH.HCl

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

497-19-8

sodium carbonate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
In tetrahydrofuran; EtOH (abs); ethanol
In tetrahydrofuran; EtOH (abs); ethanol
H2 NOH HCl

H2 NOH HCl

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

497-19-8

sodium carbonate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
In tetrahydrofuran; EtOH (abs); ethanol
In tetrahydrofuran
In tetrahydrofuran; EtOH (abs); ethanol
H2NOH HCl

H2NOH HCl

79099-07-3

N-tert-butyloxycarbonylpiperidin-4-one

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
With sodium carbonate In tetrahydrofuran; water

C17H24N2O2

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Stage #1: C17H24N2O2 With potassium hydrogensulfate In water for 1.5h;
Stage #2: With potassium hydroxide In water pH=10;
13035-19-3

4-aminopiperidine

24424-99-5

di-tert-butyl dicarbonate

100-52-7

benzaldehyde

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Stage #1: 4-aminopiperidine; benzaldehyde In toluene for 3h; Heating / reflux;
Stage #2: di-tert-butyl dicarbonate In toluene at 20℃;
41661-47-6

piperidin-4-one

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 16 h / 20 °C
2: palladium on activated charcoal; ammonia; hydrogen / methanol / 20 °C
View Scheme
6295-57-4

2-benzthiazole thioacetic acid

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

701236-99-9

N-(1-tert-butoxycarbonylpiperidin-4-yl)-(2-benzothiazolylthio)acetamide

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In chloroform at 20℃; for 20h;100%
3140-73-6

2-chloro-4,6-dimethoxy-1 ,3,5-triazine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

951004-60-7

4-(4,6-dimethoxy-[1,3,5]triazin-2-ylamino)-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
In acetonitrile at 160℃; for 0.333333h; microwave irradiation;100%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

122805-79-2

(2-formylthiophen-3-yl)carbamic acid ethyl ester

2-[[[1-(1,1-dimethylethoxycarbonyl)-4-piperidinyl]amino]methyl]-3-(ethoxycarbonylamino)-thiophene

Conditions
ConditionsYield
100%
1656-44-6

2,4-dinitrobenzenesulfonyl chloride

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

812690-24-7

tert-butyl 4-{[(2,4-dinitrophenyl)sulfonyl]amino}piperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 2,4-dinitrobenzenesulfonyl chloride; 1-(tert-butoxycarbonyl)-4-aminopiperidine With lutidine In dichloromethane at 0 - 20℃; for 18.5h;
Stage #2: With potassium hydrogensulfate; water for 0.5h; pH=2.5 - 3;
100%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

68282-52-0

2,4-dimethyl-1H-imidazole-5-carbaldehyde

Tert-butyl 4-[(2,4-dimethylimidazol-5-yl)methylamino]piperidin-1-carboxylate

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 0 - 20℃; Cooling with ice;100%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

79-04-9

chloroacetyl chloride

865432-01-5

tert-butyl 4-(2-chloroacetamido)piperidine-1-carboxylate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 1h;100%
With triethylamine In dichloromethane at 0 - 20℃; for 0.333333h; Inert atmosphere;90%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 0.5h;89%
92972-48-0

2,4-dichlorothiazole-5-carboxaldehyde

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

866329-10-4

4-{[(2,4-dichloro-thiazol-5-yl)methyl]-amino}-piperidine-1-carboxylic acid t-butyl ester

Conditions
ConditionsYield
Stage #1: 2,4-dichlorothiazole-5-carboxaldehyde; 1-(tert-butoxycarbonyl)-4-aminopiperidine With acetic acid In 1,2-dichloro-ethane at 21 - 26℃; for 1.5h;
Stage #2: With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20 - 27℃; for 4.46667h;
100%
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 18h;62%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

68282-52-0

2,5(4)-dimethyl-1H-imidazole-4(5)-carboxaldehyde

701298-75-1

tert-butyl 4-{[(2,4-dimethyl-1H-imidazol-5-yl)methyl]amino}piperidine-1-carboxylate

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; acetic acid In methanol at 20℃; for 2h;100%
Stage #1: 1-(tert-butoxycarbonyl)-4-aminopiperidine; 2,5(4)-dimethyl-1H-imidazole-4(5)-carboxaldehyde With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 15h;
Stage #2: With water; potassium carbonate
100%
700-37-8

4-chloro-2-fluoro-nitrobenzene

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

932700-82-8

tert-butyl 4-((5-chloro-2-nitrophenyl)amino)piperidine-1-carboxylate

Conditions
ConditionsYield
With sodium carbonate In N,N-dimethyl-formamide at 80℃; for 1h;100%
With sodium carbonate In N,N-dimethyl-formamide at 80℃; for 1h;100%
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 80℃; for 18h;93.2%
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20 - 80℃; for 1h;
With potassium carbonate In dimethyl sulfoxide at 20℃; Inert atmosphere;
932375-18-3

4-fluoro-2-methyl-5-nitro-benzonitrile

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

932375-19-4

1,1-dimethylethyl 4-[(4-cyano-5-methyl-2-nitrophenyl)amino]-1-piperidinecarboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 80℃;100%
1009-35-4

4-fluoro-3-nitrobenzonitrile

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

320406-05-1

tert-butyl 4-((4-cyano-2-nitrophenyl)amino)piperidine-1-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 72h;100%
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 27℃; Cooling with ice;
125568-71-0

methyl 2,4-difluoro-5-nitrobenzoate

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

1037833-97-8

tert-butyl 4-{[5-fluoro-4-(methoxycarbonyl)-2-nitrophenyl]amino}piperidine-1-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 72h;100%
104-87-0

4-methyl-benzaldehyde

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

359877-52-4

tert-butyl 4-((4-methylphenyl)methyl)aminopiperidine carboxylate

Conditions
ConditionsYield
Stage #1: 4-methyl-benzaldehyde; 1-(tert-butoxycarbonyl)-4-aminopiperidine In ethanol for 4h; Reflux;
Stage #2: With sodium tetrahydroborate; ethanol at 20℃; for 24h;
100%
Stage #1: 4-methyl-benzaldehyde; 1-(tert-butoxycarbonyl)-4-aminopiperidine In ethanol for 4h; Heating / reflux;
Stage #2: With sodium tetrahydroborate In ethanol at 20℃; for 24h;
Stage #3: With water In ethanol
100%
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃;
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

35034-22-1

2-methylimidazole-4(5)-carbaldehyde

1034411-58-9

tert-butyl4-{[(2-methyl-1H-imidazol-5-yl)methyl]amino}piperidine-1-carboxylate

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; acetic acid In methanol at 20℃; for 2h;100%
777-44-6

3-(Trifluoromethyl)benzenesulfonyl chloride

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

884308-82-1

4-(3-trifluoromethylbenzenesulfonylamino)piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane for 2h;100%
1143624-55-8

4,6-bis-benzyloxy-5'-isopropyl-2'-methoxybiphenyl-3-carboxylic acid

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

1143624-64-9

4-[(4,6-bis-benzyloxy-5'-isopropyl-2'-methoxybiphenyl-3-carbonyl)amino]piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h;100%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

16588-74-2

3,5-ditrifluoromethylisocyanate

1275064-22-6

tert-butyl 4-(3-(3,5-bis(trifluoromethyl)phenyl)ureido)piperidine-1-carboxylate

Conditions
ConditionsYield
In dichloromethane at 20℃;100%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

98-74-8

4-Nitrobenzenesulfonyl chloride

1233952-63-0

4-(4-nitrobenzenesulfonylamino)piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;100%
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 20℃; for 1h; Inert atmosphere;
1365839-19-5

N-(6-chloro-4-((cis-2,6-dimethylmorpholino)methyl)pyridin-2-yl)thiazolo[5,4-b]pyridin-2-amine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

1365839-20-8

1,1-dimethylethyl 4-{[4-{[cis-2,6-dimethyl-4-morpholinyl]methyl}-6-([1,3]thiazolo[5,4-b]pyridin-2-ylamino)-2-pyridinyl]amino}-1-piperidinecarboxylate

Conditions
ConditionsYield
With lithium hexamethyldisilazane; (NHC)Pd(allyl)Cl In tetrahydrofuran at 80℃; for 1h; Microwave irradiation; Inert atmosphere;100%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

82820-87-9

2,4-dibromobutanoyl chloride

1365998-53-3

tert-butyl 4-(2,4-dibromobutanamido)piperidin-1-carboxylate

Conditions
ConditionsYield
Stage #1: 1-(tert-butoxycarbonyl)-4-aminopiperidine; 2,4-dibromobutanoyl chloride With triethylamine In dichloromethane at 0℃;
Stage #2: With sodium hydrogencarbonate In dichloromethane Product distribution / selectivity;
100%
With triethylamine In tetrahydrofuran at 20℃; for 0.5h;
With triethylamine In tetrahydrofuran at 20℃; for 0.5h;
1245649-52-8

1-(benzenesulfonyl)-4-chloro-5-nitro-1H-pyrrolo[2,3-b]pyridine

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

1315495-05-6

4-(1-benzenesulphonyl-5-nitro-1H-pyrrolo[2,3-b]pyridine-4ylamino)piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In isopropyl alcohol for 2h; Reflux;100%
With N-ethyl-N,N-diisopropylamine In isopropyl alcohol Inert atmosphere; Heating;
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

5332-06-9

4-bromobutanenitrile

4-(3-cyano-propylamino)-piperidine-1-carboxylic acid tert-butyl ester

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 48h; Reflux;100%

3-(6-chloropyridin-3-yl)-6-fluoro-1-(phenylsulfonyl)-1H-indole

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

1-(5-(6-fluoro-1-(phenylsulfonyl)-1H-indol-3-yl)pyridin-2-yl)piperidin-4-amine

Conditions
ConditionsYield
In 1-methyl-pyrrolidin-2-one at 180℃; for 2h; Time; Microwave irradiation;100%

4-((4-(4-(trifluoromethoxy)phenyl)-5-(trifluoromethyl)pyrimidin-2-yl)amino)benzoic acid

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

N-(1-Boc-4-piperidyl)-4-((4-(6-(trifluoromethoxy)pyridin-3-yl)-5-(trifluoromethyl)pyrimidin-2-yl)amino)benzamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 15h; Inert atmosphere;100%
87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

57489-77-7

5,7-dichloropyrazolo[1,5-a]pyrimidine

tert-butyl 4-(5-chloropyrazolo[1,5-a]pyrimidin-7-ylamino)piperidine-1-carboxylate

Conditions
ConditionsYield
With triethylamine In acetonitrile at 100℃; for 12h;100%
With triethylamine In acetonitrile at 100℃; for 12h;

4-((4-(6-methoxy-3-pyridyl)-5-trifluoromethylpyrimidin-2-yl)amino)benzoic acid

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

tert-butyl 4-(4-{[4-(6-methoxypyridin-3-yl)-5-(trifluoromethyl)pyrimidin-2-yl]amino}benzamido)piperidine-1-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 15h;100%
331-41-9

2-(4-chloro-3-fluorophenoxy)acetic acid

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

tert-butyl 4-[[2-(4-chloro-3-fluorophenoxy)acetyl]amino]piperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 2-(4-chloro-3-fluorophenoxy)acetic acid; 1-(tert-butoxycarbonyl)-4-aminopiperidine With HATU In N,N-dimethyl-formamide at 20℃; for 0.166667h;
Stage #2: With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃;
100%
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 25℃; for 12h;
59394-30-8

6-chloro-2-quinolinecarboxylic acid

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

tert-butyl 4-[(6-chloroquinoline-2-carbonyl)amino]piperidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 6-chloro-2-quinolinecarboxylic acid; 1-(tert-butoxycarbonyl)-4-aminopiperidine With HATU In N,N-dimethyl-formamide at 20℃; for 0.166667h;
Stage #2: With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide
100%

N-(2,4-dimethoxybenzyl)-5-fluoro-N-(6-fluoropyridin-2-yl)-4-(trifluoromethyl)pyridine-2-sulfonamide

87120-72-7

1-(tert-butoxycarbonyl)-4-aminopiperidine

tert-butyl 4-((6-(N-(2,4-dimethoxybenzyl)-N-(6-fluoropyridin-2-yl)sulfamoyl)-4-(trifluoromethyl)pyridin-3-yl)amino)piperidine-1-carboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 70℃; for 2h;100%
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Specification

The 4-Amino-1-boc-piperidine is the chemical compound with the formula C10H20N2O2. Its molecular weight is 200.28. It is white to light yellow crystal powder. With cas registry number of 87120-72-7, it belongs to the categories of (1)Amino acid; (2)Amines; (3)blocks; (4)Amines and Anilines; (5)Piperidines, Piperidones,Piperazines; (6)pharmacetical; (7)Pyrans, Piperidines & Piperazines; (8)API intermediates; (9)Piperidines; (10)Piperazine; (11)Pyrans, Piperidines & Piperazines.

Physical properties of 4-Amino-1-boc-piperidine are: (1) ACD/LogP: 1.09 ; (2) # of Rule of 5 Violations: 0 ; (3) ACD/LogD (pH 5.5): ; (4) ACD/LogD (pH 7.4): ; (5) ACD/BCF (pH 5.5): 1 ; (6) ACD/BCF (pH 7.4): 1 ; (7) ACD/KOC (pH 5.5): 1 ; (8) ACD/KOC (pH 7.4): 1.004 ; (9) #H bond acceptors: 4 ; (10) #H bond donors: 2 ; (11) #Freely Rotating Bonds: 3 ; (12) Index of Refraction: 1.484 ; (13) Molar Refractivity: 54.993 cm3 ; (14) Molar Volume: 192.269 cm3 ; (15) Surface Tension: 37.816 dyne/cm ; (16) Density: 1.042 g/cm3 ; (17) Flash Point: 121.509 °C ; (18) Enthalpy of Vaporization: 51.586 kJ/mol ; (19) Boiling Point: 277.303 °C at 760 mmHg ; (20) Vapour Pressure: 0.005 mmHg at 25°C.

Preparation of 4-Amino-1-boc-piperidine : This chemical can be prepared by 4-(2,2,2-trifluoro-acetylamino)-piperidine-1-carboxylic acid tert-butyl ester .


The reaction will use reagent aq. NH3, solvent Methanol and other conditions like heating. The reaction time is about 6 hours. Yield is about 5.75 g.

Uses of 4-Amino-1-boc-piperidine : It is used to prepare other chemicals. Here is a example below.


The reaction occurs at the temperature of 120 ℃ using reagents of K2CO3, KI, solvent of dimethylformamide for 24 hours. The yield is 58%.

When you are using this chemical, please be cautious about it as the following:
This chemical is sensitive to CO2. It is harmful by inhalation, in contact with skin and if swallowed and irritating to eyes, respiratory system and skin. Wear suitable protective clothing, gloves and eye/face protection before use it. During use it, do not breathe dust. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. Keep it under argon.

You can still convert the following datas into molecular structure:
(1) SMILES:CC(C)(C)OC(=O)N1CCC(CC1)N;
(2) InChI:InChI=1/C10H20N2O2/c1-10(2,3)14-9(13)12-6-4-8(11)5-7-12/h8H,4-7,11H2,1-3H3;
(3) InChIKey:LZRDHSFPLUWYAX-UHFFFAOYAC