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927-83-3

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Basic Information

CAS No.:

927-83-3

Name:

AZO-TERT-BUTANE

Article Data:

17

Molecular Structure:

Molecular Structure of 927-83-3 (AZO-TERT-BUTANE)

Formula:

C8H18 N2

Molecular Weight:

142.244

Synonyms:

Azoethane,1,1,1',1'-tetramethyl- (6CI,7CI,8CI); Diazene, bis(1,1-dimethylethyl)- (9CI);2,2'-Azobis(2-methylpropane); 2,2'-Azobis-tert-butane; 2,2'-Azoisobutane;Bis(tert-butyl)diimine; Di-tert-butyldiazene

Density:

0.8g/cm³

Melting Point:

-14.5°C

Boiling Point:

150.5°Cat760mmHg

Flash Point:

36°C

Hazard Symbols:

Risk Codes:

11-20/22-36/37/38

Safety:

Hazard Codes	F,Xn
Risk Statements	11-20/22-36/37/38
Safety Statements	16-26-36
RIDADR	UN 1993 3/PG 2
WGK Germany	3
F	10

PSA:

24.72000

LogP:

3.03560

Synthetic route

: 13952-69-7
1,2-di-tert-butylhydrazine

: 927-83-3
di-t-butyldiazene

Conditions	Yield
at 20℃; for 72h; Air; Darkness;	66%

: 13463-40-6
iron pentacarbonyl

: 917-95-3
t-butylnitrite

A: 927-83-3
di-t-butyldiazene

B: 691-24-7
1,3-di-tert-butylcarbodiimide

C: 5336-24-3
1,3-di-tert-butylurea

D: 16649-52-8, 54168-23-9, 87339-11-5
di-t-butyldiazene N-oxide

Conditions	Yield
In tetrahydrofuran Irradiation (UV/VIS); Stirring of nitroso compound in THF under N2, metal carbonyl in THF is added, the soln. is irradiated for 1 h (sunlamp photolysis) at 30°C.; addn. of naphthalene as internal standard, Gc-anal.;	A 1% B 1% C 13% D 4%

: 51655-37-9
N-bromo-2-methylpropan-2-amine

: 927-83-3
di-t-butyldiazene

Conditions	Yield
With silver(l) oxide

: 594-19-4
tert.-butyl lithium

: 927-83-3
di-t-butyldiazene

Conditions	Yield
With diethyl ether; dinitrogen monoxide

: 98-95-3
nitrobenzene

: 75-64-9
tert-butylamine

A: 927-83-3
di-t-butyldiazene

B: 100-65-2
N-Phenylhydroxylamine

C: 495-48-7
azoxybenzene

Conditions	Yield
Mechanism; Rate constant; Irradiation; reaction also in presence of biacetyl and benzophenone or O2;

: 75-64-9
tert-butylamine

A: 927-83-3
di-t-butyldiazene

B: 100-65-2
N-Phenylhydroxylamine

C: 495-48-7
azoxybenzene

Conditions	Yield
With nitrobenzene Irradiation; also in presence of biacetyl and benzophenone;

: 3376-24-7
N-tert-butyl-α-phenylnitrone

: 19028-38-7
1,3,5-trimethyl hexachloro cyclotrigermazane

A: 120347-53-7
(Cl2GeO)3

B: 927-83-3
di-t-butyldiazene

C: 622-29-7
N-Benzylidenemethylamine

Conditions	Yield
Kinetics; react. of germazane with nitron with and without catalysis;

: 3376-24-7
N-tert-butyl-α-phenylnitrone

: 17394-49-9
nonamethyl cyclotrigermazane

A: 927-83-3
di-t-butyldiazene

B: 16090-53-2
2,2,4,4,6,6-hexamethyl-1,3,5-trioxa-2,4,6-trigermacyclohexane

C: 622-29-7
N-Benzylidenemethylamine

Conditions	Yield
Kinetics; react. of germazane with nitron, depending on catalysator;

: (tert-butyl)(1,2-di-tert-butyldiaziridin-3-ylidene)amine

A: 630-18-2
tert-butyl isocyanide

B: 927-83-3
di-t-butyldiazene

C: 119072-55-8, 7188-38-7
tert-butylisonitrile

Conditions	Yield
In Cyclohexane-d12 at 180℃; for 0.133333h;

: Li3Mn4Li(μ3-NtBu)6(μ-NtBu)3(NtBu)(N)

A: 927-83-3
di-t-butyldiazene

B: 1537901-02-2
Mn4IV(μ3-NtBu)4(NtBu)4

Conditions	Yield
With tetraethylammonium chloride Inert atmosphere;

Raw Materials

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