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99-07-0

Basic Information
CAS No.: 99-07-0
Name: 3-Dimethylaminophenol
Article Data: 39
Cas Database
Molecular Structure:
Molecular Structure of 99-07-0 (3-Dimethylaminophenol)
Formula: C8H11NO
Molecular Weight: 137.181
Synonyms: Phenol,m-(dimethylamino)- (6CI,7CI,8CI);(3-Hydroxyphenyl)dimethylamine;3-(Dimethylamino)phenol;3-Hydroxy-N,N-dimethylaniline;3-N,N-Dimethylaminophenol;N,N-Dimethyl-m-aminophenol;NSC 62017;m-(Dimethylamino)phenol;m-(N,N-Dimethylamino)phenol;
EINECS: 202-727-0
Density: 1.089 g/cm3
Melting Point: 82-84 °C(lit.)
Boiling Point: 266.5 °C at 760 mmHg
Flash Point: 132.7 °C
Solubility: slightly soluble in water
Appearance: brown to purple solid
Hazard Symbols: IrritantXi,HarmfulXn
Risk Codes: 26-36-36/37/39-22
Safety: 26-36-36/37/39-22
Transport Information: N/A
PSA: 23.47000
LogP: 1.45820
Synthetic route
15799-79-8

3-methoxy-N,N-dimethylaniline

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With boron trichloride; tetra-(n-butyl)ammonium iodide In dichloromethane at -78 - 0℃; for 1h; dealkylation;95%
124-40-3

dimethyl amine

108-46-3

recorcinol

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With hydrogen In water at 200℃; under 375.038 Torr; for 3h; Reagent/catalyst; Autoclave;93%
626-02-8

3-Iodophenol

124-40-3

dimethyl amine

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With copper(l) iodide; 6,7-dihydro-5H-quinolin-8-one oxime; potassium hydroxide In water at 25℃; for 24h; Inert atmosphere;91%
91240-40-3

methanesulfonic acid 3-dimethylaminophenyl ester

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With lithium diisopropyl amide In tetrahydrofuran at 0℃; for 0.0166667h;89%
591-20-8

3-Bromophenol

124-40-3

dimethyl amine

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With copper(l) iodide; 6,7-dihydro-5H-quinolin-8-one oxime; potassium hydroxide In water at 85℃; for 24h; Inert atmosphere;89%

m-dimethylaminophenylhydroxylamine hydrochloride

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
In water-d2 for 0.5h; Inert atmosphere; Photolysis;89%
121-69-7

N,N-dimethyl-aniline

A

619-60-3

4-(N,N-dimethylamino)phenol

B

3743-22-4

2-hydroxy-N,N-dimethylaniline

C

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With dihydrogen peroxide; antimony pentafluoride In hydrogen fluoride at -20℃; for 0.25h; Mechanism; Product distribution;A 26%
B 14%
C 44%
With hydrogen fluoride; dihydrogen peroxide; antimony pentafluoride at -20℃; for 0.25h;A 26%
B 14%
C 44%
With dihydrogen peroxide; antimony pentafluoride In hydrogen fluoride at -20℃; for 0.25h;A 26%
B 14%
C 44%
50-00-0

formaldehyd

591-27-5

m-Hydroxyaniline

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With hydrogen In methanol at 180℃; under 12751.3 Torr; for 8h; Autoclave;21%
With sodium tetrahydroborate In methanol at 20℃;
67-56-1

methanol

51-81-0

3-aminophenol hydrochloride

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
at 170℃;
87-01-4

7-dimethylamino-4-methyl-chromen-2-one

99-07-0

3-Dimethylaminophenol

Conditions
ConditionsYield
With potassium hydroxide
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Chemistry

IUPAC Name: 3-(dimethylamino)phenol  
Molecular Formula: C8H11NO
Formula Weight: 137.18g/mol
Appearance: gray powder
Density: 1.089 g/cm3
Melting Point: 82 - 84 °C
Boiling Point: 266.5 °C at 760 mmHg
Refractive index: 1.589
Flash point: 132.7 °C 
Vapor Pressure: 0.00524 mmHg at 25°C
Solubility: dissolved in ethanol, ether, benzene, acetone, alkali, and inorganic acid,not almost soluble in water
EINECS: 202-727-0
liansport Information: 70kgs
Freely Rotating Bonds: 2  
Molar Refractivity: 42.44 cm
Molar Volume: 125.8 cm
Polarizability: 16.82 10-24cm
Surface Tension: 44 dyne/cm 
Enthalpy of Vaporization: 52.48 kJ/mol 
Sensitive: Light Sensitive
   The chemical synonyms of  3-Dimethylaminophenol (CAS NO.99-07-0) are (3-Hydroxyphenyl)dimethylamine;3-(dimethylamino)-pheno;3-Hydroxydimethylaminobenzene;3-Hydroxy-N,N-dimethylaniline and 3-n,n-dimethylaminophenol.Its product categories is benzene derivative;Aromatic Phenols;Phenoles and thiophenoles;Amines;Aromatics and Pharmaceutical Intermediate.The molecular structure of 3-Dimethylaminophenol (CAS NO.99-07-0) is.

Uses

It can be used as neostigmine bromide  intermediate and dye intermediate.

Production

It is derived by the Inter-amino-phenol reaction with dimethyl sulfate.

Toxicity Data With Reference

1.    

mma-sat 33 µg/plate

    EMMUEG    Environmental and Molecular Mutagenesis. 11 (Suppl 12)(1988),1.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Mutation data reported. When heated to decomposition it emits toxic vapors of NOx.
Hazard Codes:  Xi,HarmfulXn .
Xn:  Harmful
Xi:  Irritant
Risk Statements:  36/37/38-20/21/22 .
20/21/22:  Harmful by inhalation, in contact with skin and if swallowed.
36/37/38:  Irritating to eyes, respiratory system and skin.
Safety Statements:  26-36-36/37/39-22.
22:  Do not breathe dust.
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
36:  Wear suitable protective clothing.  
36/37/39:  Wear suitable protective clothing, gloves and eye/face protection.